IP Library Granted Patent US 11,073,515
Granted Patent B2
US 11,073,515 · App. 16/192,805 · Granted Jul 27, 2021

Method for photobleaching stained cells

Inventors: Jonathan Fauerbach (Rösrath, DE); Christian Dose (Kürten, MA); Thomas Rockel (Düsseldorf, DE); Veronika Rudolf (Bergisch Gladbach, DE)
Assignee: Miltenyi Biotec GmbH
G01N33/54353G01N33/5306G01N33/542G01N33/582
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Quick Facts
Patent No.
US 11,073,515
App. No.
16/192,805
Granted
Jul 27, 2021
Kind
B2
Abstract

The invention is directed to a method for detecting a target moiety in a sample of biological specimens by: a) providing at least one conjugate with the general formula (I) X n —P—Y m , b) contacting the sample of biological specimens with at least one conjugate, thereby labeling the target moiety recognized by the antigen recognizing moiety Y with the conjugate c) exciting the labelled target moieties with light having a wavelength within the absorbance spectrum of fluorescent moiety X d) detecting the labelled target moieties by detecting the fluorescence radiation and e) degrading the fluorescent moiety X of the labelled target moieties by irradiating the conjugate with light having a wavelength within the absorbance spectrum of fluorescent moiety X Use of the method in fluorescence microscopy, flow cytometer, spectrofluorometry, cell separation, pathology or histology.

Claims (12)

1. A method for detecting a target moiety in a sample of biological specimens comprising:

a) providing at least one conjugate with the general formula III:

wherein Z is at least one fluorescent moiety X and at least one antigen recognizing moiety Y; and p is an integer ranging from 27 through 112;

b) contacting the sample of biological specimens with the at least one conjugate, thereby labelling the target moiety recognized by the at least one antigen recognizing moiety Y with the conjugate;

c) exciting the labelled target moieties with light having a wavelength within the absorbance spectrum of the at least one fluorescent moiety X;

d) detecting the labelled target moieties by detecting the fluorescence radiation emitted by the at least one fluorescent moiety X; and

e) degrading the at least one fluorescent moiety X of the labelled target moieties by irradiating the conjugate with light having a wavelength within the absorbance spectrum of the at least one fluorescent moiety X for a time sufficient to deliver enough energy to reduce the fluorescence radiation emitted by the at least one fluorescent moiety X at least by 75% of the initial fluorescence radiation.

2. The method according to claim 1 , wherein the at least one fluorescent moiety X is selected from the group consisting of xanthene dyes, rhodamine dyes, coumarine dyes, cyanine dyes, pyrene dyes, oxazine dyes, pyridyl oxazole dyes and pyrromethene dyes.

3. The method according to claim 1 , wherein the at least one fluorescent moiety X is substituted with one more water solubility imparting substituents selected from the group consisting of sulfonates, phosphonates, phosphates, sulfonamides, polyethers and carbonates.

4. The method according to claim 1 , wherein the at least one antigen recognizing moiety Y is at least one biomolecule selected from group consisting of an immunoglobulin, antibody, fragmented antibody, Fab, Fab′, F(ab′) 2 , sdAb, scFv, and di-scFv, each of naturally or recombinant origin.

5. The method according to claim 1 , wherein the at least one antigen recognizing moiety Y is at least one biomolecule selected from the group consisting of peptide/MHC-complexes, receptors for cell adhesion or costimulatory molecules, receptor ligands, antigens, hapten binders, avidin, streptavidin, neutravidin, aptamers, primers and ligase substrates.

6. The method according to claim 1 , wherein the at least one antigen recognizing moiety Y is an antibody, an fragmented antibody, an fragmented antibody derivative, peptide/MHC-complexes targeting TCR molecules, cell adhesion receptor molecules, receptors for costimulatory molecules or artificial engineered binding molecules.

Assignments (1)
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Dec 29, 2019
From: MILTENYI BIOTEC GMBH
To: MILTENYI BIOTEC B.V. & CO. KG
Reel/Frame 051443/0669 →