IP Library Granted Patent US 10,626,075
Granted Patent B2
US 10,626,075 · App. 16/207,635 · Granted Apr 21, 2020

Process for oxidation of alcohols using oxygen-containing gases

Inventors: Wenjuan Zhou (Shanghai, CN); Wenhao Fang (Shanghai, CN); Armin T. Liebens (Shanghai, CN)
Assignee: RHODIA OPERATIONS
C07C51/235B01J21/04B01J21/10B01J23/06B01J23/10B01J23/894B01J23/8926B01J35/002B01J35/006B01J35/0013B01J37/035B01J37/16C07C51/23C07C51/245C07C59/125C07C231/12C07C231/14C07C233/46B01J2231/70
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Quick Facts
Patent No.
US 10,626,075
App. No.
16/207,635
Granted
Apr 21, 2020
Kind
B2
Abstract

The present invention concerns a process of oxidizing an alcohol for the production of its corresponding carbonyl compounds wherein the oxidation is performed with oxygen or gases containing oxygen in the presence of a catalyst comprising at least a gold compound and a copper compound. Said alcohol oxidation by gaseous oxidant can achieve a high yield and selectivity with minimized degradation products or waste organic solvents.

Claims (12)

1. A composition comprising an ethoxylated alcohol of formula (II)

R 1 (OCH 2 CHR 2 ) n OCH 2 CH 2 OH  (II)

wherein R 1 represents an alkyl radical having 1 to 22 carbon atoms or a monounsaturated or polyunsaturated linear or branched alkenyl radical having 2 to 22 carbon atoms, optionally comprising at least a substituent and/or a heteroatom; R 2 represents a hydrogen atom or a methyl group or a mixture thereof in the individual molecule; and n has an average number between 2 and 20;

or

an acid monoethanolamide of formula (IV)

wherein R′ represents a saturated, linear or branched alkyl radical having from 4 to 25 carbon atoms or a monounsaturated or polyunsaturated linear or branched alkenyl radical having from 4 to 25 carbon atoms;

and a catalyst comprising at least a gold compound and a copper compound.

2. The composition of claim 1 , wherein R 1 is selected from a group consisting of methyl, butyl and lauryl.

3. The composition of claim 1 , wherein R 1 is an alkyl group substituted with at least one substituent selected from a group consisting of —OR 3 , —CH 3 , —CH 2 CH 3 , —COOH, —CONH 2 and —COOR 3 , wherein R 3 represents an alkyl or aryl group.

4. The composition according to claim 1 , wherein the acid monoethanolamide of formula (IV) is lauric acid monoethanolamide.

5. The composition according to claim 1 , wherein the catalyst is applied to a support selected from the group consisting of activated carbon and oxide supports.

6. The composition according to claim 5 , wherein the support is an oxide support selected from the group consisting of zinc oxide, magnesium oxide, cerium dioxide and aluminium oxide.

Assignments (2)
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Jan 26, 2024
From: RHODIA OPERATIONS
To: SPECIALTY OPERATIONS FRANCE
Reel/Frame 066374/0642 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Nov 7, 2023
From: RHODIA OPERATIONS
To: SPECIALTY OPERATIONS FRANCE
Reel/Frame 065488/0365 →