Methods for X-ray inspection of PDC tooling and parts
View Patent ↗Embodiments disclosed herein are directed to methods and systems for X-ray imaging and/or inspection of a PCD element in a protective leaching cup, which may be placed in a tray. Embodiments include inspection of one or more characteristics between the protective leaching cup and the PCD element prior to and/or after leaching of the PCD element. Embodiments also include using X-ray imaging to assist with positioning the PCD element in the protective leaching cup. Embodiments further include inspection of one or more defects in the PCD element during processing and/or after usage by X-ray technique.
1. A method of leaching a polycrystalline diamond (“PCD”) element and inspecting a leached PCD element, the method comprising:
positioning a PCD element in a predetermined position at least partially within a protective leaching cup;
at least partially leaching the PCD element to form a leach profile therein;
capturing an X-ray of the PCD element in the leaching cup;
analyzing the X-ray of the PCD element to determine at least one characteristic of the leach profile; and
if the leach profile of the PCD element is satisfactory at least partially based on the at least one characteristic, removing the PCD element from the protective leaching cup.
2. The method of claim 1 , wherein positioning a PCD element in a predetermined position at least partially within a protective leaching cup includes positioning the PCD element in the predetermined position such that a seal region of the protective leaching cup seals against the PCD element.
3. The method of claim 2 , wherein positioning the PCD element in the predetermined position such that a seal region of the protective leaching cup seals against the PCD element includes positioning the PCD element in the predetermined position such that the seal region of the protective leaching cup seals against a PCD table of the PCD element at or near a bottom of a chamfer of the PCD table.
4. The method of claim 2 , wherein positioning the PCD element in the predetermined position such that a seal region of the protective leaching cup seals against the PCD element includes positioning the PCD element in the predetermined position such that the seal region of the protective leaching cup seals against a side surface of a PCD table of the PCD element.
5. The method of claim 2 , wherein positioning the PCD element in the predetermined position such that a seal region of the protective leaching cup seals against the PCD element includes positioning the PCD element in the predetermined position such that the seal region of the protective leaching cup seals against an interface between a PCD table and a substrate of the PCD element.
6. The method of claim 1 , wherein positioning a PCD element in a predetermined position at least partially within a protective leaching cup includes:
determining one or more trapped gases are present between the PCD element and the protective leaching cup;
aligning an expansion apparatus with the protective leaching cup; and
forcing the expansion apparatus against the PCD element to enable removal of the one or more trapped gases.
7. The method of claim 6 , wherein determining one or more trapped gases are present between the PCD element the protective leaching cup includes capturing an initial X-ray of the PCD element positioned in the protective leaching cup.
8. The method of claim 6 , wherein forcing the expansion apparatus against the PCD element to enable removal of the one or more trapped gases includes temporarily expanding or deforming outwardly at least a portion of the protective leaching cup using the expansion apparatus.
9. The method of claim 1 , wherein:
positioning a PCD element in a predetermined position at least partially within a protective leaching cup includes positioning the PCD element in the protective leaching cup to expose a selected portion of the PCD element to a leaching agent; and
at least partially leaching the PCD element to form a leach profile therein includes leaching the selected portion of the PCD element with the leaching agent to form the leach profile in the PCD element.
10. The method of claim 1 , wherein positioning a PCD element in a predetermined position at least partially within a protective leaching cup includes positioning the PCD element in the protective leaching cup such that the protective leaching cup protects at least one sidewall and a bottom portion of the PCD element from leaching.
11. The method of claim 1 , further comprising, if the leach profile of the PCD element is not satisfactory at least partially based on the at least one characteristic, re-leaching the PCD element.
12. The method of claim 1 , further comprising, if the leach profile of the PCD element is not satisfactory at least partially based on the at least one characteristic, rejecting at least one of the PCD element or the protective leaching cup.
13. A method of leaching a polycrystalline diamond (“PCD”) element and inspecting a leached PCD element, the method comprising:
positioning a PCD element in a protective leaching cup to expose a selected portion of the PCD element to a leaching agent during leaching;
leaching the selected portion of the PCD element with the leaching agent to form a leach profile in the PCD element;
capturing an X-ray of the PCD element in the leaching cup to determine at least one characteristic of the leach profile in the PCD element formed during leaching of the selected portion of the PCD element; and
if the leach profile of the PCD element is satisfactory at least partially based on the at least one characteristic, removing the PCD element from the protective leaching cup.
14. The method of claim 13 , wherein positioning a PCD element in a protective leaching cup to expose a selected portion of the PCD element to a leaching agent during leaching includes positioning the PCD element in the protective leaching cup such that a seal region of the protective leaching cup seals against the PCD element to expose the selected portion of the PCD element to the leaching agent and protect at least a portion of the PCD element from the leaching agent.
15. The method of claim 14 , wherein positioning the PCD element in the protective leaching cup such that a seal region of the protective leaching cup seals against the PCD element to expose the selected portion of the PCD element to the leaching agent and protect at least a portion of the PCD element from the leaching agent includes positioning the PCD element in the protective leaching cup such that a seal region of the protective leaching cup seals against the PCD element to expose the selected portion of the PCD element to the leaching agent and protect at least one sidewall and a bottom portion of the PCD element from leaching.
16. The method of claim 13 , wherein positioning a PCD element in a protective leaching cup to expose a selected portion of the PCD element to a leaching agent during leaching includes:
determining one or more trapped gases are present between the PCD element and the protective leaching cup;
aligning an expansion apparatus with the protective leaching cup; and
forcing the expansion apparatus against the PCD element to enable removal of the one or more trapped gases.
17. The method of claim 13 , further comprising, if the leach profile of the PCD element is not satisfactory at least partially based on the at least one characteristic, re-leaching the PCD element or rejecting at least one of the PCD element or the protective leaching cup.
18. A method of leaching a polycrystalline diamond (“PCD”) element and inspecting a leached PCD element, the method comprising:
leaching a selected portion of a PCD element with a leaching agent to form a leach profile in the PCD element, the PCD element being positioned at least partially within a protective leaching to expose the selected portion of the PCD element to the leaching agent and protect at least a portion of the PCD element from the leaching agent;
capturing an X-ray of the PCD element in the leaching cup to determine at least one characteristic of the leach profile in the PCD element; and
if the leach profile of the PCD element is satisfactory at least partially based on the at least one characteristic, removing the PCD element from the protective leaching cup.
19. The method of claim 18 , further comprising positioning the PCD element in the protective leaching cup such that a seal region of the protective leaching cup seals against the PCD element to expose the selected portion of the PCD element to the leaching agent and protect at least one sidewall and a bottom portion of the PCD element from the leaching agent.
20. The method of claim 18 , further comprising:
determining one or more trapped gases are present between the PCD element and the protective leaching cup;
aligning an expansion apparatus with the protective leaching cup; and
forcing the expansion apparatus against the PCD element to enable removal of the one or more trapped gases.