IP Library Granted Patent US 10,814,304
Granted Patent B2
US 10,814,304 · App. 16/219,678 · Granted Oct 27, 2020

Carbon-based compositions with highly efficient volumetric gas sorption

Inventors: Henry R. Costantino (Woodinville, WA); Alan Tzu-Yang Chang (Renton, WA); Chad Goodwin (Seattle, WA); Cory Mekelburg (Hagerstown, MD); Liam Cover (Seattle, WA); Benjamin E. Kron (Seattle, WA); Katharine Geramita (Seattle, WA); Aaron M. Feaver (Seattle, WA); Leah A. Thompkins (Seattle, WA)
Assignee: Group14 Technologies, Inc.
B01J20/20B01J20/28004B01J20/28011B01J20/28016B01J20/28066B01J20/28073C01B3/0021C01B3/0084C01B32/30C10L3/06C10L3/10Y02E60/325
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Quick Facts
Patent No.
US 10,814,304
App. No.
16/219,678
Granted
Oct 27, 2020
Kind
B2
Abstract

The present application is generally directed to gas storage materials such as activated carbon comprising enhanced gas adsorption properties. The gas storage materials find utility in any number of gas storage applications. Methods for making the gas storage materials are also disclosed.

Claims (30)

1. A composition comprising a gas and a carbon material having:

i) a specific gravimetric methane adsorption of 0.13 g/g or greater at room temperature and 50 bar pressure;

ii) a tap density of 0.6 g/cm 3 or greater;

iii) a mass average surface area of 1500 m 2 /g or greater; and

iv) a mass average total pore volume of 0.7 cm 3 /g or greater.

2. The composition of claim 1 , wherein the gas comprises methane, ethane, hydrogen or natural gas or a combination thereof.

3. The composition of claim 1 , wherein the carbon material is in the form of a pellet.

4. The composition of claim 1 , wherein the carbon material is in the form of a pyrolyzed monolith.

5. The composition of claim 1 , wherein the carbon material is in the form of an activated monolith.

6. The composition of claim 1 , wherein the specific gravimetric methane adsorption is 0.17 g/g or greater.

7. The composition of claim 1 , wherein the carbon material comprises a mixture of two or more populations of particles, wherein from 5%-30% of the particles have a surface area below 1500 m 2 /g, from 10%-80% of the particles have a surface area of from 1500 m 2 /g to 1800 m 2 /g and from 5-30% of the particles have a surface area greater than 1800 m 2 /g.

8. The composition of claim 1 , wherein the carbon material comprises a mixture of two or more populations of particles, wherein from 20-80% of the particles have a surface area of 1600 m 2 /g or lower and from 20-80% of the particles have a surface area of 2000 m 2 /g or higher.

9. The composition of claim 1 , wherein the carbon material comprises a pore volume and from 1-40% of the pore volume resides in mesopores, and from 1-50% of the pore volume resides in macropores.

10. The composition of claim 1 , wherein the carbon material comprises silicon.

11. A composition comprising a gas and a carbon material having a specific gravimetric methane adsorption of 0.13 g/g or greater at room temperature and 50 bar pressure, wherein the carbon material comprises a mixture of two or more populations of particles, wherein from 5%-30% of the particles have a surface area below 1500 m 2 /g, from 10%-80% of the particles have a surface area of from 1500 m 2 /g to 1800 m 2 /g and from 5-30% of the particles have a surface area greater than 1800 m 2 /g.

12. The composition of claim 11 , wherein the gas comprises methane, ethane, hydrogen or natural gas or a combination thereof.

13. The composition of claim 11 , wherein the carbon material is in the form of a pellet.

14. The composition of claim 11 , wherein the carbon material is in the form of a pyrolyzed monolith.

15. The composition of claim 11 , wherein the carbon material is in the form of an activated monolith.

16. The composition of claim 11 , wherein the specific gravimetric methane adsorption is 0.17 g/g or greater.

17. The composition of claim 11 , wherein the carbon material comprises a pore volume and from 1-40% of the pore volume resides in mesopores, and from 1-50% of the pore volume resides in macropores.

18. The composition of claim 11 , wherein the carbon material comprises silicon.

19. A composition comprising a gas and a carbon material having a specific gravimetric methane adsorption of 0.13 g/g or greater at room temperature and 50 bar pressure, wherein the carbon material comprises a mixture of two or more populations of particles, wherein from 20-80% of the particles have a surface area of 1600 m 2 /g or lower and from 20-80% of the particles have a surface area of 2000 m 2 /g or higher.

20. The composition of claim 19 , wherein the gas comprises methane, ethane, hydrogen or natural gas or a combination thereof.

21. The composition of claim 19 , wherein the carbon material is in the form of a pellet.

22. The composition of claim 19 , wherein the carbon material is in the form of a pyrolyzed monolith.

23. The composition of claim 19 , wherein the carbon material is in the form of an activated monolith.

24. The composition of claim 19 , wherein the specific gravimetric methane adsorption is 0.17 g/g or greater.

25. The composition of claim 19 , wherein the carbon material comprises a pore volume and from 1-40% of the pore volume resides in mesopores, and from 1-50% of the pore volume resides in macropores.

26. The composition of claim 19 , wherein the carbon material comprises silicon.

Continuity (3)
Division 14533956 · Nov 5, 2014
Provisional Application 61900310 · Nov 5, 2013
Related Publication 20190358607A1 · Nov 28, 2019
Cited By (6)
US 12,537,192 US 12,562,381 US 12,577,114 US 12,577,657 US 12,597,597 US 12,606,443