IP Library Granted Patent US 10,968,320
Granted Patent B2
US 10,968,320 · App. 16/238,735 · Granted Apr 6, 2021

Thermal interface materials including polymeric phase-change materials

Inventors: Dylan J. Boday (Tucson, AZ); Joseph Kuczynski (North Port, FL); Timothy C. Mauldin (San Diego, CA)
Assignee: International Business Machines Corporation
C08G81/021C08F299/0485C08G63/676C08G65/3322C09K5/00C09K5/02C09K5/06H01L23/3737H01L23/4275H01L24/29H01L24/32H01L24/83H01L2224/2919H01L2224/83201
View Patent ↗
Loading inventors, assignments & file history…
Monitor This Case
Get email alerts when status or documents change.
Order Certified Copies
Most orders are placed with the USPTO same day — all within 24 business hours.
Order via The Patent Place →
Pre-filled with this patent's details
Quick Facts
Patent No.
US 10,968,320
App. No.
16/238,735
Granted
Apr 6, 2021
Kind
B2
Abstract

In an example, a thermal interface material includes a polymeric phase-change material.

Claims (31)

1. A thermal interface material, comprising:

a polymeric phase-change material, the polymeric phase-change material comprising a block copolymer formed from a diene, the diene formed from a vinyl-terminated fatty acid monomer and an ethylene glycol monomer.

2. The thermal interface material of claim 1 , wherein the vinyl-terminated fatty acid monomer has a chemical formula C 2 H 4 —R—C(O)OH and the ethylene glycol monomer has a chemical formula C 2n H 4n+2 O n+1 , wherein:

R corresponds to a chain length (x) of at least 8 carbon atoms between a terminal vinyl group and a carbonyl group, and

n is greater than or equal to 1.

3. The thermal interface material of claim 2 , wherein n is equal to 1.

4. The thermal interface material of claim 2 , wherein n is 2 or more.

5. The thermal interface material of claim 4 , wherein the ethylene glycol monomer includes tetraethylene glycol.

6. The thermal interface material of claim 1 , wherein the polymeric phase-change material has a melting transition temperature (T m ) in a range of 0° C. to 100° C.

7. The thermal interface material of claim 1 , wherein the polymeric phase-change material has a melting enthalpy in a range of 200 J/g to 400 J/g.

8. The thermal interface material of claim 1 , wherein the polymeric phase-change material has a thermal stability parameter (T d ) of 5% mass loss at a temperature that is in a range of 250° C. to 450° C.

9. The thermal interface material of claim 1 , wherein the thermal interface material has a structure represented by:

wherein x is at least 8 carbon atoms and n is greater than or equal to 1.

10. A thermal interface material, comprising:

a polymeric phase-change material, the polymeric phase-change material comprising a block copolymer formed from a diene, the diene being formed from a vinyl-terminated fatty acid monomer and an ethylene glycol monomer, the vinyl-terminated fatty acid monomer having a chemical formula of C 2 H 4 —R—C(O)OH and the ethylene glycol monomer having the chemical formula C 2n H 4n+2 O n+1 , wherein:

R corresponds to a chain length (x) of at least 8 carbon atoms between a terminal vinyl group and a carbonyl group, and

n is greater than 2.

11. The thermal interface material of claim 10 , wherein the ethylene glycol monomer includes tetraethylene glycol.

12. The thermal interface material of claim 10 , wherein the polymeric phase-change material has a melting transition temperature (T m ) in a range of 0° C. to 100° C.

13. The thermal interface material of claim 10 , wherein the polymeric phase-change material has a melting enthalpy in a range of 200 J/g to 400 J/g.

14. The thermal interface material of claim 10 , wherein the polymeric phase-change material has a thermal stability parameter (T d ) of 5% mass loss at a temperature that is in a range of 250° C. to 450° C.

15. The thermal interface material of claim 10 , wherein n is equal to 4.

16. The thermal interface material of claim 10 , wherein the thermal interface material has a structure represented by:

wherein x us at least 8 carbon atoms and n is greater than 2.

17. A thermal interface material, comprising:

a polymeric phase-change material, the polymeric phase-change material comprising a block copolymer formed from a diene, and the diene being formed from a vinyl-terminated fatty acid monomer and an ethylene glycol monomer, the vinyl-terminated fatty acid monomer having a chemical formula of C 2 H 4 —R—C(O)OH and the ethylene glycol monomer having the chemical formula C 2n H 4n+2 O n+1 , wherein:

R corresponds to a chain length (x) of at least 8 carbon atoms between a terminal vinyl group and a carbonyl group,

n is greater than or equal to 1, and

the polymeric phase-change material has one or more of a melting transition temperature (T m ) in a range of 0° C. to 100° C., a melting enthalpy in a range of 200 J/g to 400 J/g, or a thermal stability parameter (T d ) of 5% mass loss at a temperature that is in a range of 250° C. to 450° C.

18. The thermal interface material of claim 17 , wherein the thermal interface material has a structure represented by:

wherein x is at least 8 carbon atoms and n is greater than or equal to 1.

Assignments (1)
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Jan 3, 2019
From: BODAY, DYLAN J.; KUCZYNSKI, JOSEPH; MAULDIN, TIMOTHY C.
To: INTERNATIONAL BUSINESS MACHINES CORPORATION
Reel/Frame 047889/0923 →
Continuity (2)
Division 14954409 · Nov 30, 2015
Related Publication 20190135987A1 · May 9, 2019