IP Library Granted Patent US 11,377,628
Granted Patent B2
US 11,377,628 · App. 16/258,942 · Granted Jul 5, 2022

Solidifying liquid anionic surfactants

Inventors: Wendy Lo (Saint Paul, MN); Erik C. Olson (Saint Paul, MN); Jon D. Hansen (Saint Paul, MN); Katherine J. Molinaro (Saint Paul, MN); Corey Rosenthal (Saint Paul, MN)
Assignee: ECOLAB USA INC.
C11D11/0082C11D1/143C11D1/146C11D1/22C11D1/24C11D1/29C11D3/046C11D3/10C11D3/2075C11D3/2079C11D3/222C11D3/323C11D3/3418C11D3/3707C11D3/3749C11D3/3761C11D3/38C11D11/02C11D1/37
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Quick Facts
Patent No.
US 11,377,628
App. No.
16/258,942
Granted
Jul 5, 2022
Kind
B2
Abstract

The invention relates to solidification of liquid anionic surfactants with a binder, carrier, or both binder and carrier to form a solidified surfactant composition. In particular, the invention relates to solidification of liquid surfactants utilizing drying device(s), wherein the feed composition contains at least one liquid surfactant and the binder, carrier, or binder and carrier to form a solidified surfactant composition. The solidified surfactant compositions can be useful in various cleaning compositions.

Claims (16)

1. A method of preparing a solidified surfactant composition comprising:

adding to a drying device:

a liquid anionic surfactant comprising a sulfate surfactant, a sulfonate surfactant, or a combination thereof; and one or more of

a solid binder comprising a natural polymer, a urea derivative, a polyacrylate, a polyethylene glycol (PEG), or a combination thereof; wherein the solid binder is dissolved with the liquid surfactant in a ratio of between about 4:1 to about 1:60 by actives, and

a solid carrier comprising an alpha olefin sulfonate, linear alkyl sulfonate, sodium lauryl sulfate, sodium alkyl sulfate, sodium carbonate, magnesium carbonate, sodium acetate, magnesium acetate, sodium sulfate, magnesium sulfate, sodium chloride, or combination thereof, wherein the carrier and the liquid surfactant are in a ratio of between about 5:1 to about 1:30 by actives, and wherein the carrier is a solid component when added to the drying device;

drying the liquid surfactant and one or more of binder and solid carrier to form a solidified surfactant composition;

wherein the drying device comprises a spray dryer; wherein the spray dryer has an inlet and an outlet wherein the inlet temperature is between about 20° C. and about 250° C.; and wherein the outlet temperature is less than about 150° C.; and

wherein the liquid surfactant is solidified in the solidified surfactant composition, and wherein the solidified surfactant composition has less than about 5 wt-% water.

2. The method of claim 1 , wherein the liquid surfactant is a C4-C18 alkyl sulfate, a C4-C18 alkyl ether sulfate, an alkyl benzene sulfonate, an ammonium lauryl sulfate, a linear alkyl benzene sulfonate, a linear alkyl benzene sulfonic acid, an isopropylamine dodecylbenzene sulfonate, or a combination thereof.

3. The method of claim 1 , wherein the liquid surfactant is a sodium lauryl ether sulfate.

4. The method of claim 1 , wherein the method comprises the binder and wherein the binder is a PEG having a melting point of at least about 40° C., a gum, a cellulose, a cellulose ester, a chitin, a chitosan, a starch, protein, a lignin, a natural rubber, or a combination thereof.

5. The method of claim 1 , wherein the method comprises the carrier.

6. The method of claim 1 , wherein the solidified surfactant composition contains at least about 10 wt. % active surfactants.

7. The method of claim 1 , wherein the drying process is performed in a batch system.

8. The method of claim 1 , wherein the drying process is performed in a continuous system.

9. The method of claim 1 , wherein the method comprises the binder and the carrier.

Assignments (1)
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Feb 1, 2019
From: LO, WENDY; OLSON, ERIK C.; HANSEN, JON D.; MOLINARO, KATHERINE J.; ROSENTHAL, COREY
To: ECOLAB USA INC.
Reel/Frame 048222/0618 →
Continuity (2)
Provisional Application 62622545 · Jan 26, 2018
Related Publication 20190233772A1 · Aug 1, 2019
Cited By (1)
US 12,359,147