IP Library Granted Patent US 11,591,918
Granted Patent B2
US 11,591,918 · App. 16/270,680 · Granted Feb 28, 2023

Article with ceramic barrier coating and layer of networked ceramic nanofibers

Inventors: Zhongfen Ding (South Windsor, CT); Elisa M. Zaleski (Manchester, CT)
Assignee: RAYTHEON TECHNOLOGIES CORPORATION
F01D5/288C04B35/48C04B35/6225C04B35/62222C23C28/3215C23C28/3455F01D5/284C04B2235/3244C04B2235/3246C04B2235/3248C04B2235/5236C04B2235/5264C23C30/00F05D2220/32F05D2230/90F05D2240/24F05D2300/2118F05D2300/5023F05D2300/614
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Quick Facts
Patent No.
US 11,591,918
App. No.
16/270,680
Granted
Feb 28, 2023
Kind
B2
Abstract

An article includes a substrate, a ceramic barrier coating, and a layer of networked ceramic nanofibers. The ceramic barrier coating is disposed on the substrate and has a porous columnar microstructure. The layer of networked ceramic nanofibers is disposed on the ceramic barrier layer and seals the pores of the porous columnar microstructure.

Claims (22)

1. An article comprising:

a substrate;

a ceramic barrier coating disposed on the substrate, the ceramic barrier coating having a porous columnar microstructure; and

a layer of networked ceramic nanofibers disposed on the ceramic barrier coating and sealing the pores of the porous columnar microstructure, the ceramic nanofibers are selected from the group consisting of yttria stabilized zirconia, gadolinia zirconate, zirconium oxide, and combinations thereof, and the layer of networked ceramic nanofibers includes filaments that are randomly oriented in the pores of the porous columnar microstructure.

2. The article as recited in claim 1 , wherein the substrate is a metal alloy.

3. The article as recited in claim 1 , wherein the layer has a thickness of 1 micrometer to 50 micrometers.

4. The article as recited in claim 3 , wherein the thickness is from 1 micrometer to 5 micrometers.

5. The article as recited in claim 1 , wherein the ceramic barrier coating has a thickness t1 and the layer has a thickness t2, and t2 is less than t1 by a factor of at least 5.

6. The article as recited in claim 1 , further comprising an additional ceramic barrier coating disposed on the layer of the networked ceramic nanofibers.

7. The article as recited in claim 6 , wherein the additional ceramic barrier coating includes zirconia stabilized with an element selected from the group consisting of cesium, titanium, and combinations thereof.

8. The article as recited in claim 1 , wherein the ceramic nanofibers are yttria stabilized zirconia.

9. The article as recited in claim 1 , wherein the ceramic nanofibers are gadolinia zirconate.

10. The article as recited in claim 1 , wherein the ceramic nanofibers are intertwined.

11. An airfoil comprising:

An airfoil section;

a porous ceramic barrier coating disposed on the airfoil section, the porous ceramic barrier coating having a porous columnar microstructure; and

a layer of networked ceramic nanofibers disposed on the porous ceramic barrier coating and sealing the pores of the porous ceramic barrier coating, the ceramic nanofibers are selected from the group consisting of yttria stabilized zirconia, gadolinia zirconate, zirconium oxide, and combinations thereof, and the layer of networked ceramic nanofibers includes filaments that are randomly oriented in the pores of the porous columnar microstructure.

12. The airfoil as recited in claim 11 , further comprising an additional ceramic barrier coating disposed on the layer of the networked ceramic nanofibers.

13. The airfoil as recited in claim 12 , wherein the additional ceramic barrier coating includes zirconia stabilized with an element selected from the group consisting of cesium, titanium, and combinations thereof, and the layer has a thickness of 1 micrometer to 5 micrometers.

14. A method of fabricating an article, the method comprising:

providing a substrate and a ceramic barrier coating disposed on the substrate, the ceramic barrier coating having a porous columnar microstructure; and

depositing by blow-spinning a layer of networked ceramic nanofibers on the ceramic barrier coating to seal the pores of the porous columnar microstructure, the ceramic nanofibers are selected from the group consisting of yttria stabilized zirconia, gadolinia zirconate, zirconium oxide, and combinations thereof, and the layer of networked ceramic nanofibers includes filaments that are randomly oriented in the pores of the porous columnar microstructure.

Assignments (4)
CHANGE OF NAME Recorded Jul 27, 2023
From: RAYTHEON TECHNOLOGIES CORPORATION
To: RTX CORPORATION
Reel/Frame 064714/0001 →
CORRECTIVE ASSIGNMENT TO CORRECT THE SPELLING ON THE ADDRESS 10 FARM SPRINGD ROAD FARMINGTONCONNECTICUT 06032 PREVIOUSLY RECORDED ON REEL 057190 FRAME 0719. ASSIGNOR(S) HEREBY CONFIRMS THE CORRECT SPELLING OF THE ADDRESS 10 FARM SPRINGS ROAD FARMINGTON CONNECTICUT 06032. Recorded Aug 19, 2021
From: UNITED TECHNOLOGIES CORPORATION
To: RAYTHEON TECHNOLOGIES CORPORATION
Reel/Frame 057226/0390 →
CHANGE OF NAME Recorded Aug 16, 2021
From: UNITED TECHNOLOGIES CORPORATION
To: RAYTHEON TECHNOLOGIES CORPORATION
Reel/Frame 057190/0719 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Feb 8, 2019
From: DING, ZHONGFEN; ZALESKI, ELISA M.
To: UNITED TECHNOLOGIES CORPORATION
Reel/Frame 048273/0405 →