IP Library Granted Patent US 11,513,046
Granted Patent B2
US 11,513,046 · App. 16/270,890 · Granted Nov 29, 2022

Flowability testing systems and methods

Inventors: Theophilus Edovia (Richmond, TX); Vittoria Balsamo-Hernandez (Fulshear, TX); Marcus D. Faust, Jr. (Naperville, IL); Rogelio Banda (Houston, TX); Wilfredis Medina-Melendez (Richmond, TX); Kenneth W. Dorris (Richmond, TX); Tyler D. Boyd (Houston, TX)
Assignee: CHAMPIONX USA Inc.
G01N11/06G01F1/74G01G17/04G01N2011/002
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Quick Facts
Patent No.
US 11,513,046
App. No.
16/270,890
Granted
Nov 29, 2022
Kind
B2
Abstract

Systems and methods for assessing flowability of a multiphase fluid are provided. The method includes agitating a sample of the multiphase fluid contained in a container while controlling an agitation force applied to the sample; pouring the sample, after it has been agitated, into a viscosity cup having an opening at its upper end and an orifice at its lower end and thereby causing the multiphase fluid to flow out of the viscosity cup through the orifice; weighing an amount of the multiphase fluid that has flowed through the orifice and into a receiving vessel over a period of time; and assessing flowability of the multiphase fluid sample using the weight of the multiphase fluid sample in the receiving vessel as a function of time.

Claims (28)

1. A method of assessing flowability of a multiphase fluid produced from a petroleum well or oilfield, the method comprising:

adding a candidate chemical treatment agent to a sample of the multiphase fluid produced from a petroleum well or oilfield contained in a container to form a treated sample;

agitating the treated sample of the multiphase fluid produced from a petroleum well or oilfield contained in a container while controlling an agitation force applied to the treated sample, wherein agitation of the sample has an initial phase where vigorous agitation and a temperature of from about 50° F. to about 162° F. is used and a second phase of agitation wherein less vigorous agitation as compared to the initial phase is used or in the second phase of agitation a temperature of about 50° F. to about 106° F. is used;

pouring the treated sample, after it has been agitated, into a viscosity cup having an opening at its upper end and an orifice at its lower end and thereby causing the multiphase fluid produced from a petroleum well or oilfield to flow out of the viscosity cup through the orifice;

weighing an amount of the multiphase fluid produced from a petroleum well or oilfield that has flowed through the orifice and into a receiving vessel over a period of time;

weighing the container after the treated sample has been poured out into the viscosity cup as a measure of a deposition characteristic of the treated multiphase fluid sample;

assessing flowability of the treated multiphase fluid sample produced from a petroleum well or oilfield using the weight of the treated multiphase fluid sample in the receiving vessel as a function of time and assessing the deposition of the treated multiphase fluid sample; and

comparing the flowability and deposition of the treated multiphase fluid sample with an otherwise identical multiphase fluid sample that did not have the candidate chemical treatment agent added before agitation.

2. The method of claim 1 further comprising controlling a temperature of the viscosity cup while the sample is in the viscosity cup.

3. The method of claim 2 wherein controlling the temperature of the viscosity cup comprises controlling the temperature of the viscosity cup independently of the temperature of the sample while it is being agitated.

4. The method of claim 1 wherein the multiphase fluid comprises production petroleum fluids from a petroleum well.

5. The method of claim 1 wherein the candidate chemical treatment agent comprises a flow improver, a paraffin inhibitor, or a combination thereof.

6. The method of claim 1 wherein assessing flowability of the multiphase fluid sample using the weight of the multiphase fluid sample in the receiving vessel as a function of time comprises determining a maximum flow rate into the receiving vessel.

7. The method of claim 6 wherein the flowability of the treated multiphase fluid sample is compared with the flowability of the untreated multiphase fluid sample.

8. The method of claim 1 wherein the candidate chemical treatment agent comprises a flow improver.

9. The method of claim 1 wherein the multiphase fluid comprises a paraffinic crude oil.

10. The method of claim 9 wherein the candidate chemical treatment agent comprises a flow improver, a paraffin inhibitor, or a combination thereof.

11. The method of claim 1 wherein the sample of the multiphase fluid is prepared by mixing oil from an oilfield with a synthetic brine.

12. The method of claim 11 wherein the candidate chemical treatment agent is added to the brine before the brine is mixed with the oil.

13. A method of assessing flowability of a multiphase fluid produced from a petroleum well or oilfield, the method comprising:

adding a candidate chemical treatment agent to a sample of the multiphase fluid produced from a petroleum well or oilfield contained in a container to form a treated sample;

agitating the treated sample of the multiphase fluid produced from a petroleum well or oilfield contained in a container while controlling an agitation force applied to the treated sample;

pouring the treated sample, after it has been agitated, into a viscosity cup having an opening at its upper end and an orifice at its lower end and thereby causing the multiphase fluid produced from a petroleum well or oilfield to flow out of the viscosity cup through the orifice;

weighing an amount of the multiphase fluid produced from a petroleum well or oilfield that has flowed through the orifice and into a receiving vessel over a period of time;

weighing the container after the treated sample has been poured out into the viscosity cup as a measure of a deposition characteristic of the treated multiphase fluid sample;

assessing flowability of the treated multiphase fluid sample produced from a petroleum well or oilfield using the weight of the treated multiphase fluid sample in the receiving vessel as a function of time and assessing the deposition of the treated multiphase fluid sample; and

comparing the flowability and deposition of the treated multiphase fluid sample with an otherwise identical multiphase fluid sample that did not have the candidate chemical treatment agent added before agitation, wherein a surface cleaning efficiency is calculated as a percentage reduction in the amount of material deposited on the container as compared to an untreated control under the same conditions.

14. The method of claim 13 wherein the surface cleaning efficiency of the treated multiphase fluid sample is compared with the surface cleaning efficiency of the untreated multiphase fluid sample.

Assignments (8)
RELEASE OF SECURITY INTEREST IN PATENTS Recorded Jul 17, 2025
From: JPMORGAN CHASE BANK, N.A.
To: CHAMPIONX LLC; APERGY ESP SYSTEMS, LLC; APERGY BMCS ACQUISITION CORP; HARBISON-FISCHER, INC.; NORRIS RODS, INC.,; NORRIS RODS, INC.,; NORRISEAL-WELLMARK, INC.; PCS FERGUSON, INC.; QUARTZDYNE, INC.; US SYNTHETIC CORPORATION
Reel/Frame 072004/0019 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Oct 20, 2022
From: EDOVIA, THEOPHILUS; DORRIS, KENNETH W.
To: ECOLAB USA INC.
Reel/Frame 061481/0270 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Oct 7, 2022
From: BOYD, TYLER D.
To: CHAMPIONX USA INC.
Reel/Frame 061346/0137 →
RELEASE OF SECURITY INTEREST Recorded Jun 7, 2022
From: BANK OF AMERICA, N.A.
To: CHAMPIONX USA INC.
Reel/Frame 060304/0267 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Sep 22, 2020
From: ECOLAB USA INC.
To: CHAMPIONX USA INC.
Reel/Frame 053849/0537 →
SECURITY INTEREST Recorded Jun 5, 2020
From: CHAMPIONX USA INC.
To: BANK OF AMERICA, N.A.
Reel/Frame 052848/0368 →
SECURITY INTEREST Recorded Jun 5, 2020
From: CHAMPIONX USA INC.
To: JPMORGAN CHASE BANK, N.A.
Reel/Frame 053250/0001 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Apr 4, 2019
From: BALSAMO-HERNANDEZ, VITTORIA; FAUST, MARCUS D., JR.; BANDA, ROGELIO; MEDINA-MELENDEZ, WILFREDIS
To: ECOLAB USA INC.
Reel/Frame 048794/0735 →