IP Library Granted Patent US 11,161,952
Granted Patent B2
US 11,161,952 · App. 16/286,229 · Granted Nov 2, 2021

Methods of insulating piping and other materials using high temperature non-crosslinked polyethylene-based foam

Inventor: Debabrata Kundu (Charlotte, NC)
Assignee: Hickory Springs Manufacturing Company
C08J9/00B29C44/50B29C44/56C08J3/28C08J9/141B29K2023/06B29K2023/0625B29K2995/0063C08J2201/03C08J2203/14C08J2323/06C08J2323/08
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Quick Facts
Patent No.
US 11,161,952
App. No.
16/286,229
Granted
Nov 2, 2021
Kind
B2
Abstract

A linear low density polyethylene (LLDPE) foam and methods of making the same are described. The LLDPE foam has a maximum operating temperature of about 220° F. The LLDPE foam can also have a density in the range of from 0.6 to 10.0 lbs/ft 3 . The LLDPE foam can be manufactured in part by processing an LLDPE resin in order to create a long branch molecular structure in the LLDPE resin without crosslinking or otherwise adversely affecting the thermoplastic properties of the LLDPE resin.

Claims (22)

1. A method of insulating a pipe with foam insulation, comprising:

obtaining a resin consisting essentially of a non-crosslinked linear low density polyethylene resin having an initial melt index between 15 and 20 at 190° C.;

causing the linear low density polyethylene resin to be irradiated to form an irradiated, non-crosslinked linear low density polyethylene resin having a final melt index between 0.7 and 5.0 at 190° C. and having the long chain branch structure;

adding one or more additives selected from the group consisting of flame retardants, color pigments, nucleating agents, diffusion blockers, and blowing agents to the irradiated, non-crosslinked linear low density polyethylene resin;

foaming the irradiated, non-crosslinked linear low density polyethylene resin with the one or more additives to obtain a foam, wherein the foam forms a foam pipe insulation material to be applied to a surface of a pipe such that the foam pipe insulation material meets the ASTM C411 standard for hot-surface performance of high-temperature thermal insulation when tested at 220° F.;

applying to the surface of the pipe the foam pipe insulation material; and

wherein the pipe is configured for passing media through the portion of the pipe on which the foam pipe insulation material is applied.

2. The method of claim 1 , wherein the foam pipe insulation material does not exhibit any cracking, delamination or warpage after 96 hours.

3. The method of claim 1 , wherein the foam pipe insulation material does not exhibit any cracking, delamination or warpage after 683 hours.

4. The method of claim 1 , wherein the foam has a density in the range of from 0.6 to 10.0 lbs/ft3.

5. The method of claim 4 , wherein the foam has a density in the range of from 1.0 to 2.0 lbs/ft3.

6. The method of claim 1 , wherein the irradiation is carried out without eliminating the thermoplastic property of the linear low-density polyethylene resin.

7. A method of insulating a pipe with foam insulation comprising:

manufacturing a foam insulation, comprising:

irradiating a resin wherein the resin consists essentially of a non-crosslinked linear low-density polyethylene resin having an initial melt index in the range of from 15 to 20 at 190° C. until the melt index is reduced to in the range of from 0.7 to 5.0 at 190° C. and having a long chain branch structure;

mixing the irradiated liner low-density polyethylene resin with one or more foam additives;

heating the mixture of the irradiated liner low-density polyethylene resin and the one or more foam additives to thereby form a melt;

injecting a blowing agent into the melt;

cooling the melt; and

passing the cooled melt through a die to thereby form a foam insulation such that the foam insulation meets the ASTM C411 standard for hot-surface performance of high-temperature thermal insulation when tested at 220° F.;

applying to a surface of a pipe the foam insulation; and

passing media through the portion of the pipe on which the foam insulation is applied.

Assignments (3)
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Jul 31, 2026
From: HICKORY SPRINGS MANUFACTURING COMPANY
To: PTI LLC
Reel/Frame 075478/0219 →
SECURITY INTEREST Recorded Mar 9, 2023
From: HICKORY SPRINGS MANUFACTURING COMPANY; HSM TRANSPORTATION, LLC
To: WELLS FARGO BANK, NATIONAL ASSOCIATION
Reel/Frame 062928/0460 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Aug 27, 2019
From: KUNDU, DEBABRATA
To: HICKORY SPRINGS MANUFACTURING COMPANY
Reel/Frame 050178/0714 →