IP Library Granted Patent US 10,774,168
Granted Patent B2
US 10,774,168 · App. 16/297,651 · Granted Sep 15, 2020

Composition including silane-grafted polyolefin

Inventors: Krishnamachari Gopalan (Troy, MI); Robert J. Lenhart (Fort Wayne, IN); Gending Ji (Waterloo, CA)
Assignee: COOPER-STANDARD AUTOMOTIVE, INC.
C08F255/04B60J10/15B60J10/16B60J10/17C08F255/00
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Quick Facts
Patent No.
US 10,774,168
App. No.
16/297,651
Granted
Sep 15, 2020
Kind
B2
Abstract

A silane-grafted polyolefin composition is disclosed and includes a desired reduced specific weight material. The composition finds application in a wide array of uses, and in particular automotive and uses such as windshield wipers, where this composition is used in place of conventional materials such as TPV and EPDM rubber formulations.

Claims (28)

1. A windshield wiper comprising a windshield wiper composition, the windshield wiper composition consisting of:

a silane-grafted polyolefin having a density of from about 0.84 g/cm 3 to about 0.96 g/cm 3 ; and

one or more additives selected from the group consisting of polypropylenes, thermoplastic vulcanizates (TPV), olefinic block copolymers, ethylene propylene diene terpolymers (EPDM), ethylene vinyl acetate (EVA) copolymers, ethylene n-butyl acrylate copolymers, and ethylene methacrylate copolymers;

wherein the polyolefin is selected from the group consisting of a blend of propylene/α-olefin copolymer with an ethylene/α-olefin copolymer, and a propylene/α-olefin copolymer.

2. A method for manufacturing a windshield wiper, comprising:

grafting silanes to a polyolefin to form a silane-grafted polyolefin;

extruding a composition comprising the silane-grafted polyolefin having a density of from about 0.84 g/cm 3 to about 0.96 g/cm 3 , a condensation catalyst, and optionally one or more fillers selected from the group consisting of polypropylenes, thermoplastic vulcanizates (TPV), ethylene propylene diene terpolymers (EPDM), ethylene vinyl acetate (EVA) copolymers, ethylene n-butyl acrylate copolymers, and ethylene methacrylate copolymers; and

molding the extruded composition into the windshield wiper;

wherein the polyolefin is selected from the group consisting of a blend of propylene/α-olefin copolymer with an ethylene/α-olefin copolymer, and a propylene/α-olefin copolymer.

3. The method of claim 2 , wherein the grafting is performed in a melt.

4. The method of claim 2 , wherein the grafting is performed in solution.

5. The method of claim 2 , wherein the grafting is performed in a solid-state.

6. The method of claim 2 , wherein the grafting is performed in a swollen-state.

7. The method of claim 2 , wherein the composition further comprises:

one or more fillers selected from the group consisting of antistatic agents, dyes, pigments, UV light absorbers, nucleating agents, fillers, slip agents, plasticizers, fire retardants, lubricants, processing aides, smoke inhibitors, anti-blocking agents, and viscosity control agents.

8. A windshield wiper comprising:

a windshield wiper composition that comprises:

a silane-grafted polyolefin having a density of from about 0.84 g/cm 3 to about 0.96 g/cm 3 ,

wherein the polyolefin is a blend of propylene/α-olefin copolymer and an ethylene/aα-olefin copolymer.

9. The windshield wiper of claim 8 , wherein the windshield wiper further comprises:

one or more additives selected from the group consisting of polypropylenes, thermoplastic vulcanizates (TPV), ethylene propylene diene terpolymers (EPDM), ethylene vinyl acetate (EVA) copolymers, ethylene n-butyl acrylate copolymers, and ethylene methacrylate copolymers.

10. The windshield wiper of claim 8 , wherein the windshield wiper further comprises:

one or more additives selected from the group consisting of antistatic agents, dyes, pigments, UV light absorbers, nucleating agents, fillers, slip agents, plasticizers, fire retardants, lubricants, processing aides, smoke inhibitors, anti-blocking agents, and viscosity control agents.

11. The windshield wiper of claim 8 , wherein the windshield wiper further comprises:

one or more fillers selected from the group consisting of metal oxides, metal hydroxides, metal carbonates, metal sulfates, metal silicates, clays, talcs, carbon black, and silicas.

12. The windshield wiper of claim 11 wherein the one or more fillers are present in an amount from about 1 wt % to about 20 wt %.

13. The windshield wiper of claim 8 , wherein the windshield wiper further comprises:

one or more tackifying resins selected from the group consisting of aliphatic hydrocarbons, aromatic hydrocarbons, modified hydrocarbons, terpenes, modified terpenes, hydrogenated terpenes, rosins, hydrogenated rosins, and combinations thereof.

Assignments (10)
RELEASE OF SECURITY INTEREST IN PATENTS PREVIOUSLY RECORDED REEL/FRAME (062544/0357) Recorded Mar 4, 2026
From: U.S. BANK TRUST COMPANY, NATIONAL ASSOCIATION, AS COLLATERAL AGENT
To: COOPER-STANDARD AUTOMOTIVE INC.; COOPER-STANDARD INDUSTRIAL AND SPECIALTY GROUP, LLC
Reel/Frame 075022/0543 →
RELEASE OF SECURITY INTEREST IN PATENTS PREVIOUSLY RECORDED AT REEL/FRAME (062545/0715) Recorded Mar 4, 2026
From: U.S. BANK TRUST COMPANY, NATIONAL ASSOCIATION, AS COLLATERAL AGENT
To: COOPER-STANDARD AUTOMOTIVE INC.; COOPER-STANDARD INDUSTRIAL AND SPECIALTY GROUP, LLC
Reel/Frame 075022/0267 →
PATENT SECURITY AGREEMENT (1ST LIEN) Recorded Jan 30, 2023
From: COOPER-STANDARD AUTOMOTIVE INC.; COOPER-STANDARD INDUSTRIAL AND SPECIALTY GROUP, LLC
To: U.S. BANK TRUST COMPANY, NATIONAL ASSOCIATION, AS COLLATERAL AGENT
Reel/Frame 062544/0357 →
PATENT SECURITY AGREEMENT (3RD LIEN) Recorded Jan 30, 2023
From: COOPER-STANDARD AUTOMOTIVE INC.; COOPER-STANDARD INDUSTRIAL AND SPECIALTY GROUP, LLC
To: U.S. BANK TRUST COMPANY, NATIONAL ASSOCIATION, AS COLLATERAL AGENT
Reel/Frame 062545/0715 →
TERMINATION AND RELEASE OF SECURITY INTEREST PREVIOUSLY RECORDED AT REEL/FRAME (052788/0158) Recorded Jan 29, 2023
From: DEUTSCHE BANK AG NEW YORK BRANCH, AS COLLATERAL AGENT
To: COOPER-STANDARD AUTOMOTIVE INC.
Reel/Frame 062539/0706 →
TERMINATION AND RELEASE OF SECURITY INTEREST PREVIOUSLY RECORDED AT REEL/FRAME (052788/0392) Recorded Jan 27, 2023
From: U.S. BANK TRUST COMPANY, NATIONAL ASSOCIATION (SUCCESSOR IN INTEREST TO U.S. BANK NATIONAL ASSOCIATION), AS COLLATERAL AGENT
To: COOPER-STANDARD AUTOMOTIVE INC
Reel/Frame 062540/0108 →
PATENT SECURITY AGREEMENT Recorded May 31, 2020
From: COOPER-STANDARD AUTOMOTIVE INC.
To: BANK OF AMERICA, N.A., AS ADMINISTRATIVE AGENT
Reel/Frame 052797/0812 →
PATENT SECURITY AGREEMENT Recorded May 29, 2020
From: COOPER-STANDARD AUTOMOTIVE INC.
To: U.S. BANK NATIONAL ASSOCIATION, AS COLLATERAL AGENT
Reel/Frame 052788/0392 →
SECURITY AGREEMENT Recorded May 29, 2020
From: COOPER-STANDARD AUTOMOTIVE INC.
To: DEUTSCHE BANK AG NEW YORK BRANCH
Reel/Frame 052788/0158 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Mar 9, 2019
From: GOPALAN, KRISHNAMACHARI; LENHART, ROBERT J; JI, GENDING
To: COOPER-STANDARD AUTOMOTIVE, INC
Reel/Frame 048553/0860 →
Continuity (4)
Continuation 15978919 · May 14, 2018
Continuation 14305918 · Jun 16, 2014
Provisional Application 61835157 · Jun 14, 2013
Related Publication 20190202957A1 · Jul 4, 2019