IP Library Granted Patent US 10,900,109
Granted Patent B2
US 10,900,109 · App. 16/306,998 · Granted Jan 26, 2021

Titanium sheet and method for manufacturing the same

Inventors: Koji Mitsuda (Tokyo, JP); Kazuhiro Takahashi (Tokyo, JP); Hideto Seto (Tokyo, JP)
Assignee: NIPPON STEEL CORPORATION
C22F1/183C22F1/02C22F1/18C22C14/00C22F1/00
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Quick Facts
Patent No.
US 10,900,109
App. No.
16/306,998
Granted
Jan 26, 2021
Kind
B2
Abstract

To provide a titanium sheet excellent in formability and a method for manufacturing the same. A titanium sheet, wherein, when a carbon concentration of a base material is C b (mass %) and a carbon concentration at a depth d μm from a surface is C d (mass %), the depth d (carbon concentrated layer thickness) satisfying C d /C b >1.5 is 1.0 μm or more and less than 10.0 μm or less, wherein a Vickers hardness HV 0.025 at a load of 0.245 N in the surface is 200 or more, a Vickers hardness HV 0.05 at a load of 0.49 N in the surface is lower than HV 0.025 , and a difference between HV 0.025 and HV 0.05 is 30 or more, wherein a Vickers hardness HV 1 at a load of 9.8 N in the surface is 150 or less, and wherein an average interval between cracks generated in the surface when a strain of 25% is given in a rolling direction in a bulging forming process is less than 50 μm and a depth thereof is 1 μm or more and less than 10 μm.

Claims (10)

1. A titanium sheet,

wherein, when a carbon concentration of a base material is C b (mass %) and a carbon concentration at a depth d μm from a surface is C d (mass %), the depth d (carbon concentrated layer thickness) satisfying C d /C b >1.5 is 3.0 μm or more and less than 10.0 μm,

wherein a Vickers hardness HV 0.025 at a load of 0.245 N in the surface is 200 or more, a Vickers hardness HV 0.05 at a load of 0.49 N in the surface is lower than HV 0.025 , and a difference between HV 0.025 and HV 0.05 is 30 or more,

wherein a Vickers hardness HV 1 at a load of 9.8 N in the surface is 150 or less, and

wherein an average interval between cracks generated in the surface when a strain of 25% is given in a rolling direction in a bulging forming process is less than 50 μm and a depth thereof is 1 μm or more and less than 10 μm.

2. A method for manufacturing the titanium sheet according to claim 1 , the manufacturing method comprising:

after performing hot-rolling and descaling, forming an oxide coating film of 20 to 200 nm in thickness in a titanium sheet;

performing cold-rolling to the titanium sheet by using mineral oil as lubricant oil at a reduction ratio of 15% or more per each pass until a rolling ratio of 70% is reached; thereafter,

performing cold-rolling at a reduction ratio of 5% or less at least in a final pass; and

performing annealing to the cold-rolled titanium sheet by holding in a temperature range of 750 to 810° C. for 0.5 to 5 minutes in a vacuum or Ar gas atmosphere.

Assignments (2)
CHANGE OF NAME Recorded May 14, 2019
From: NIPPON STEEL & SUMITOMO METAL CORPORATION
To: NIPPON STEEL CORPORATION
Reel/Frame 049257/0828 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Dec 31, 2018
From: MITSUDA, KOJI; TAKAHASHI, KAZUHIRO; SETO, HIDETO
To: NIPPON STEEL & SUMITOMO METAL CORPORATION
Reel/Frame 047875/0791 →