IP Library Granted Patent US 11,479,675
Granted Patent B2
US 11,479,675 · App. 16/370,303 · Granted Oct 25, 2022

Coated solar reflective granules and methods of manufacturing the same

Inventors: Rhonda Jenree (Berkeley Springs, WV); Dale Addison Grove (Hagerstown, MD)
Assignee: U.S. Silica Company
C09C3/10C09C1/42C09C3/063C09C3/12F26B1/00F26B3/084F26B25/007E04D7/005
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Quick Facts
Patent No.
US 11,479,675
App. No.
16/370,303
Granted
Oct 25, 2022
Kind
B2
Abstract

A reflective particulate material comprises a particulate substrate, and a coating on the particulate substrate. The coated reflective particulate material may have a relative error of an amount of the coating on the particulate substrate of about 5% to about 15%, and/or a dust index of about 5 or lower, and/or a staining loss of about 8% to about 11%. A method of manufacturing the reflective particulate material comprises mixing the particulate substrate with a liquid coating composition to form a wet particulate mixture, passing the wet particulate mixture through at least one heat zone to remove water and/or moisture, and curing the coating material in the coating composition.

Claims (28)

1. A reflective particulate material, comprising:

a particulate substrate comprising particles; and

a coating on the particles of the particulate substrate, the reflective particulate material having:

a relative error of an amount of the coating on the particles particulate substrate of from about 5% to about 15%; and a standard deviation of the amount of coating on the particles particulate substrate of from about 0.05% to about 0.10%; and

a dust index of less than 2; and

a staining loss when applied to an asphalt substrate of less than 10%.

2. The reflective particulate material according to claim 1 , wherein the coating comprises a fluoropolymer, fluorosilane, silane, siloxane, polysiloxane, organo-polysiloxane, silicate, organic silicate, silicone resin, acrylic, urethane, polyurethane, and/or glycol ether.

3. The reflective particulate material according to claim 1 , wherein the coating comprises a silane and siloxane mixture.

4. The reflective particulate material according to claim 1 , wherein the coating is present in an amount of about 3 wt % or less based on a total weight of the reflective particulate material.

5. The reflective particulate material according to claim 1 , wherein the relative error of the amount of the coating on the particle is from about 5% to about 7%.

6. The reflective particulate material according to claim 1 , wherein the particulate substrate comprises a clay.

7. A method of manufacturing the reflective particulate material of claim 1 , the method comprising:

mixing the particulate substrate with a liquid coating composition to form a wet particulate mixture, the coating composition comprising a coating material;

passing the wet particulate mixture through at least one heat zone to remove water and to at least partially cure the coating material in the coating composition.

8. The method according to claim 7 , wherein the mixing the particulate substrate with a liquid coating composition comprises:

metering an amount of the particulate substrate into a mixer;

metering an amount of the liquid coating composition into the mixer; and

mixing the particulate substrate and the liquid coating composition in the mixer.

9. The method according to claim 8 , wherein the mixer comprises a paddle mixer comprising an elongated chamber housing a rotating barrel having a plurality of paddles extending radially from the barrel.

10. The method according to claim 7 , wherein the passing the wet particulate mixture through at least one heat zone comprises passing the wet particulate mixture through at least first and second heat zones, the first heat zone being maintained at a lower temperature than the second heat zone.

11. The method according to claim 7 , wherein the passing the wet particulate mixture through the at least one heat zone comprises delivering the wet particulate mixture to a fluidized bed dryer, the fluidized bed dryer comprising an elongated chamber into which air is introduced to convey the wet particulate mixture along a length of the elongated chamber past the at least one heat zone.

12. The method according to claim 11 , wherein the at least one heat zone comprises at least first and second heat zones, the first heat zone being maintained at a lower temperature than the second heat zone, and the air first conveying the wet particulate mixture past the first heat zone and then past the second heat zone.

13. The method according to claim 11 , wherein the fluidized bed dryer is coupled to a heater via at least one conduit, the at least one conduit delivering heated air from the heater to the at least one heat zone of the fluidized bed dryer.

14. The method according to claim 13 , wherein the at least one conduit comprises at least first and second conduits and the at least one heat zone comprises at least first and second heat zones, the first conduit delivering first heated air to the first heat zone to maintain the first heat zone at a first temperature, and the second conduit delivering second heated air to the second heat zone to maintain the second heat zone at a second temperature, the first temperature being lower than the second temperature.

15. The method according to claim 7 , wherein the passing the wet particulate mixture through the at least one heat zone generates an exhaust stream, the method further comprising filtering the exhaust stream.

16. The method according to claim 15 , wherein the filtering the exhaust stream comprises delivering the exhaust stream to at least one dust collection device.

17. The method according to claim 16 , wherein the at least one dust collection device comprises at least first and second dust collection devices.

18. The method according to claim 17 , wherein the first dust collection device comprises a cyclone collector, and the second dust collection device comprises a baghouse dust collector.

Assignments (2)
NOTICE OF GRANT OF SECURITY INTEREST IN INTELLECTUAL PROPERTY (FIRST LIEN) Recorded Jul 31, 2024
From: U.S. SILICA COMPANY
To: WILMINGTON TRUST, NATIONAL ASSOCIATION, AS COLLATERAL AGENT
Reel/Frame 068307/0349 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded May 16, 2019
From: GROVE, DALE ADDISON; JENREE, RHONDA
To: U.S. SILICA COMPANY
Reel/Frame 049202/0093 →
Continuity (1)
Related Publication 20200308413A1 · Oct 1, 2020