IP Library Granted Patent US 10,641,691
Granted Patent B2
US 10,641,691 · App. 16/372,715 · Granted May 5, 2020

Polymer total dissolved solids vessel

Inventors: Edward Jino Kim (Riverdale, GA); Joseph Martin Boyd (Mount Pleasant, SC); David Alan Smith (Mount Pleasant, SC)
Assignee: Environmental Express, Inc.
G01N5/045B01L3/505G01N5/04B01L7/00B01L2300/028B01L2300/123Y10T29/49776
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Quick Facts
Patent No.
US 10,641,691
App. No.
16/372,715
Granted
May 5, 2020
Kind
B2
Abstract

A thin film vessel useable in gravimetric methods for measuring the total dissolved solids or total solids in a liquid sample, or the moisture content of a solid sample. The vessel includes a main body formed of a thin walled polymeric material having a melting temperature greater than 180° C. The main body comprises an open top edge and a sealed bottom edge which define an inner cavity configured to hold a volume of liquid, and indicia applied to a portion of the main body, wherein the indicia include a tare weight of the vessel.

Claims (28)

1. A method for testing total dissolved solids in a liquid sample, the method comprising:

placing a volume of liquid into a testing vessel, wherein the testing vessel comprises:

a main body comprising an open top end and a sealed bottom end to define an inner cavity configured to hold a volume of liquid, wherein the main body comprises a thin walled polymeric material having a melting temperature greater than 180° C.; and

an indicia applied to a portion of the main body indicating a tare weight of the testing vessel, wherein the tare weight of the testing vessel comprises a weight of the testing vessel measured after at least one preconditioning step, wherein the at least one preconditioning step comprises heating the testing vessel to at least 180° C. for a first length of time,

heating the testing vessel containing the liquid sample for a time sufficient to evaporate the volume of liquid;

heating the testing vessel at 180° C. for a second length of time and weighing the testing vessel; and

repeating the step of heating the testing vessel at 180° C. for the second length of time and weighing the testing vessel until a subsequently recorded weight of the testing vessel varies by less than 0.5 mg from a previously recorded weight.

2. The method of claim 1 , wherein the second length of time comprise a time of one hour.

3. The method of claim 1 , wherein the first length of time comprises a time of at least one hour.

4. The method of claim 1 , wherein the volume of liquid comprises a volume of less than 150 ml.

5. The method of claim 1 , wherein the weight of the testing vessel comprises a weight of between 0.5 grams and 5.0 grams.

6. The method of claim 1 , wherein the polymeric material comprises nylon, polyethylene terephthalate, polyethylene, polypropylene, or a combination thereof.

7. The method of claim 1 , wherein the wall thickness of the thin walled polymeric material is less than 0.008 inches.

8. A method of producing a vessel useful for gravimetric testing, the method comprising:

performing at least one preconditioning step on the vessel, wherein the at least one preconditioning step comprises heating the vessel to at least 180° C. for a specified time and weighing the vessel to obtain a tare weight of the vessel, wherein the vessel comprises:

a main body having an open top end and a sealed bottom end to define an inner cavity configured to hold a volume of liquid, wherein the main body comprises a thin walled polymeric material having a melting temperature greater than 180° C.; and

applying an indicia to a portion of the main body of the vessel, wherein the indicia include the tare weight of the vessel.

9. The method of claim 8 , further comprising:

repeating the preconditioning step until subsequent recorded weights of the vessel vary by less than 0.5 mg.

10. The method of claim 8 , wherein the tare weight of the vessel comprises a weight of between 0.5 grams and 5.0 grams.

11. The method of claim 8 , wherein the vessel has a wall thickness of less than 0.008 inches.

12. The method of claim 1 , wherein a value of the tare weight may be subtracted from a value of the subsequently recorded weight to determine a weight of the total dissolved solids in the volume of liquid.

13. A method of producing a vessel useful for gravimetric testing, the method comprising:

performing a preconditioning step on the vessel, wherein the preconditioning step comprises heating the vessel to at least 180° C. for a specified time and weighing the vessel, wherein the vessel comprises:

a main body having an open top end and a sealed bottom end to define an inner cavity configured to hold a volume of liquid, wherein the main body comprises a thin walled polymeric material having a melting temperature greater than 180° C.;

repeating the preconditioning step until a subsequently recorded weight of the vessel varies by less than 0.5 mg from a previously recorded weight, wherein the subsequently recorded weight of the vessel is a tare weight of the vessel; and

applying an indicia to a portion of the main body of the vessel, wherein the indicia include the tare weight of the vessel.

14. The method of claim 13 , wherein the tare weight of the vessel is a weight of 0.5 grams to 5.0 grams.

Assignments (5)
RELEASE OF SECURITY INTEREST Recorded Nov 10, 2021
From: CORTLAND CAPITAL MARKET SERVICES LLC, AS COLLATERAL AGENT
To: CONTROL 3, LLC; COLE-PARMER INSTRUMENT COMPANY LLC; ENVIRONMENTAL EXPRESS, INC.
Reel/Frame 058073/0499 →
RELEASE OF FIRST LIEN SECURITY INTEREST (REEL/FRAME 050926/0279) Recorded Nov 1, 2021
From: JEFFERIES FINANCE LLC
To: COLE-PARMER INSTRUMENT COMPANY LLC; ENVIRONMENTAL EXPRESS, INC.; CONTROL 3, LLC
Reel/Frame 057988/0267 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Mar 27, 2020
From: KIM, EDWARD J; BOYD, JOSEPH M; SMITH, DAVID A
To: ENVIRONMENTAL EXPRESS, INC.
Reel/Frame 052241/0880 →
FIRST LIEN SECURITY AGREEMENT Recorded Nov 4, 2019
From: COLE-PARMER INSTRUMENT COMPANY LLC; ENVIRONMENTAL EXPRESS, INC.; CONTROL 3, LLC
To: JEFFERIES FINANCE LLC
Reel/Frame 050926/0279 →
SECOND LIEN SECURITY AGREEMENT Recorded Nov 4, 2019
From: COLE-PARMER INSTRUMENT COMPANY LLC; ENVIRONMENTAL EXPRESS, INC.; CONTROL 3, LLC
To: CORTLAND CAPITAL MARKET SERVICES LLC
Reel/Frame 050926/0318 →