IP Library Granted Patent US 11,419,769
Granted Patent B2
US 11,419,769 · App. 16/409,257 · Granted Aug 23, 2022

Sublingual films

Inventors: Nathan John Bryson (Toronto, CA); Anthony John Giovinazzo (Caledon, CA); Scott David Barnhart (York, PA); Michael Clinton Koons (York, PA)
Assignee: Sunovion Pharmaceuticals Inc.
A61F13/00063A61J1/03A61J7/0053A61K9/006A61K9/7007A61K31/381A61K31/4045A61K31/428A61K31/4415A61K31/473A61K31/48A61K31/485A61K31/4985A61K31/506A61K45/06A61K47/02A61K47/10A61K47/12A61K47/14A61K47/22A61K47/36A61K47/38A61P25/16B29C39/18B29C39/38B29C43/305B29C43/52B29C65/70B29C66/45B65D65/38A61K9/209A61K2300/00B29K2001/00B29L2007/008B29L2009/00B29L2031/753B29L2031/755
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Quick Facts
Patent No.
US 11,419,769
App. No.
16/409,257
Granted
Aug 23, 2022
Kind
B2
Abstract

The invention features sublingual film formulations of dopamine agonists and methods of treating Parkinson's disease, tremors, restless leg syndrome, sexual dysfunction, and depressive disorders therewith.

Claims (25)

1. A pharmaceutical composition in unit dosage form formulated for sublingual administration, wherein said unit dosage form is a film comprising:

(i) 30 to 75% (w/w) of an acid addition salt of apomorphine,

(ii) 0.5 to 10% (w/w) of a low molecular weight polymer having a weight average molecular weight of 5 kDa to 50 kDa selected from the group consisting of hydroxypropyl cellulose, hydroxypropyl methyl cellulose, hydroxyethyl cellulose, carboxymethyl cellulose, and methyl cellulose; and

(iii) 4 to 20±6% (w/w) of a high molecular weight polymer having a weight average molecular weight of greater than 60 kDa selected from the group consisting of hydroxypropyl cellulose, hydroxypropyl methyl cellulose, hydroxyethyl cellulose, carboxymethyl cellulose, and methyl cellulose; and

wherein said film is a bilayer film comprising a first layer comprising said acid addition salt of apomorphine and a second layer comprising a pH neutralizing agent that is pyridoxine.

2. The pharmaceutical composition of claim 1 , further comprising from 0.2 to 5% (w/w) of permeation enhancer.

3. The pharmaceutical composition of claim 1 , further comprising from 0.2 to 5% (w/w) of glycerol monostearate.

4. The pharmaceutical composition of claim 1 , further comprising from 3 to 12% (w/w) of plasticizing agent.

5. The pharmaceutical composition of claim 4 , wherein said plasticizing agent is a polyol, oleic acid, or triacetin.

6. The pharmaceutical composition of claim 5 , wherein said plasticizing agent is a polyol selected from the group consisting of sorbitol, mannitol, maltitol, xylitol, glycerol, propylene glycol, and polyethylene glycol.

7. The pharmaceutical composition of claim 1 , further comprising from 1 to 50% (w/w) of a hydrolyzed starch.

8. The pharmaceutical composition of claim 7 , wherein said hydrolyzed starch is a dextrin.

9. The pharmaceutical composition of claim 7 , wherein said hydrolyzed starch is a maltodextrin.

10. The pharmaceutical composition of claim 1 , further comprising an antioxidant.

11. The pharmaceutical composition of claim 1 , further comprising said pharmaceutical composition further comprises from 0.05 to 2.5% (w/w) of a metabisulfite.

12. The pharmaceutical composition of claim 1 , wherein said unit dosage form is stable for a period of at least 2 months at 40° C., when packaged in a sealed plastic-lined aluminum foil.

13. The pharmaceutical composition of claim 1 , wherein said film comprises particles of said acid addition salt of apomorphine.

14. The pharmaceutical composition of claim 13 , wherein said acid addition salt of apomorphine is apomorphine hydrochloride.

15. The pharmaceutical composition of claim 13 , wherein said particles have an effective particle size of from 20 nm to 10 μm.

16. The pharmaceutical composition of claim 1 , wherein said unit dosage form when placed in 1 mL of unbuffered water at pH 7 results in a solution having a pH of between 4.5 and 8.5.

17. The pharmaceutical composition of claim 1 , wherein said film comprises 12±3 mg of apomorphine hydrochloride.

18. The pharmaceutical composition of claim 1 , wherein said film comprises 22±4 mg of apomorphine hydrochloride.

19. The pharmaceutical composition of claim 1 , wherein said film comprises 30±5 mg of apomorphine hydrochloride.

20. A method of treating Parkinson's disease in a subject, said method comprising sublingual administration of a pharmaceutical composition of claim 1 in an amount effective to treat said subject.

21. The method of claim 20 , wherein said treating comprises alleviating an OFF episode associated with Parkinson's disease in said subject.

Assignments (6)
MERGER Recorded Feb 27, 2020
From: PROJECT PEGASUS SUB ACQUISITION ULC
To: SUNOVION CNS DEVELOPMENT CANADA ULC
Reel/Frame 052885/0366 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Feb 27, 2020
From: BRYSON, NATHAN JOHN; GIOVINAZZO, ANTHONY JOHN
To: CYNAPSUS THERAPEUTICS INC.
Reel/Frame 051954/0610 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Feb 27, 2020
From: BARNHART, SCOTT DAVID; KOONS, MICHAEL CLINTON
To: ARX, LLC
Reel/Frame 051954/0724 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Feb 27, 2020
From: ARX, LLC
To: CYNAPSUS THERAPEUTICS INC.
Reel/Frame 051954/0792 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Feb 27, 2020
From: SUNOVION CNS DEVELOPMENT CANADA ULC
To: SUNOVION PHARMACEUTICALS INC.
Reel/Frame 051955/0035 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Feb 27, 2020
From: CYNAPSUS THERAPEUTICS INC.
To: PROJECT PEGASUS SUB ACQUISITION ULC
Reel/Frame 052045/0901 →
Continuity (9)
Continuation 15225992 · Aug 2, 2016
Continuation 15014655 · Feb 3, 2016
Continuation 14478975 · Sep 5, 2014
Continuation 13858638 · Apr 8, 2013
Continuation 13445656 · Apr 12, 2012
Continuation PCTUS2011065665 · Dec 16, 2011
Provisional Application 61483864 · May 9, 2011
Provisional Application 61423858 · Dec 16, 2010
Related Publication 20190365661A1 · Dec 5, 2019