IP Library Granted Patent US 11,607,727
Granted Patent B2
US 11,607,727 · App. 16/412,801 · Granted Mar 21, 2023

Metal powder manufacture using a liquid metal ejector

Inventors: Scott J Vader (Pittsford, NY); Zachary S Vader (Pittsford, NY); Chu-Heng Liu (Penfield, NY)
Assignee: Xerox Corporation
B22F1/065B22F9/06B22F2999/00
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Quick Facts
Patent No.
US 11,607,727
App. No.
16/412,801
Granted
Mar 21, 2023
Kind
B2
Abstract

An ejector of liquid material to form spherical particles includes a crucible for retaining liquid material, an orifice area defining at least one orifice, and an actuator responsive to a voltage signal for causing material to be ejected from the crucible through the orifice. A method comprises applying a voltage signal of a first type and a second type to the actuator, causing a material droplet of a first size and a second size to be ejected through the orifice. Alternately or in addition, the orifice area defines a first orifice having a first diameter and a second orifice having a second diameter different from the first diameter, whereby a signal causes a material droplet of a first size to be ejected through the first orifice and a material droplet of a second size to be ejected through the second orifice.

Claims (23)

1. A method of operating an ejector to form solid spherical particles of a metal powder, the ejector having a crucible configured to retain molten metal material, structure associated with the crucible including a single orifice area defining one or more orifices, and an electrical coil responsive to a voltage signal to produce Lorentz forces in a portion of the molten metal material to be ejected from the crucible, comprising:

applying a voltage signal of a first type to the electrical coil to produce Lorentz forces in the portion of the molten metal material and eject droplets of a first predetermined size from the crucible through the one or more orifices of the single orifice area;

applying a voltage signal of a second type to the electrical coil to produce Lorentz forces in the portion of the molten metal material and eject droplets of a second predetermined size from the crucible through the one or more orifices of the single orifice area, the first predetermined size being different than the second predetermined size; and

catching in a same receptacle solid spherical particles having different diameters that were formed by the molten material droplets of the first predetermined size and the second predetermined size after the molten metal material droplets of the first predetermined size and the second predetermined size have solidified by traveling a predetermined distance from the single orifice area, the caught solid spherical particles forming the metal powder in the same receptacle.

2. The method of claim 1 , the voltage signal of the first type and the voltage signal of the second type differing by at least one of amplitude and duration.

3. The method of claim 1 , each of the voltage signal of the first type and the voltage signal of the second type include a quiet period adequate to provide time for a meniscus in the one or more orifices of the single orifice area to settle.

4. The method of claim 1 , further comprising:

receiving a request, prior to operation of the electrical coil, for the ejector to create a predetermined amount of a mixture of droplets of the first predetermined size and the second predetermined size.

5. The method of claim 4 , further comprising:

calculating how many voltage signals of the first type and voltage signals of the second type are required to create the predetermined amount of the mixture of droplets.

6. The method of claim 1 , further comprising:

applying the calculated number of the voltage signal of the first type to the electrical coil during a first duration; and

applying the calculated number of the voltage signal of the second type to the electrical coil during a second duration, the first duration being different than the second duration.

7. The method of claim 6 , further comprising:

applying each voltage signal of the first type to the electrical coil during the first duration sequentially;

applying the voltage signal of the second type to the electrical coil during the second duration sequentially; and

repeating the application of the calculated number of the voltage signal of the first type to the electrical coil sequentially followed by the application of the calculated number of the voltage signal of the second type to the electrical coil sequentially.

8. The method of claim 1 , wherein the single orifice area defines the one or more orifices as a plurality of orifices, whereby the application of the voltage signal of the first type and the application of the voltage signal of the second type causes ejection of at least one molten metal material droplet from each orifice in the plurality of orifices.

9. The method of claim 8 , wherein the single orifice area defines at least one orifice in the plurality of orifices with a first diameter at an end of the at least one orifice from which the molten metal material droplet is ejected and the single orifice area defines at least one other orifice in the plurality of orifices with a second diameter at an end of the at least one other orifice from which the molten metal material droplet is ejected, the first diameter being different than the second diameter.

10. The method of claim 1 , the molten metal material comprising molten pure metal.

11. The method of claim 1 , the molten metal material comprising a molten metal alloy.

12. The method of claim 1 , further comprising:

causing the molten metal material droplet to be ejected into pure inert gas as the molten metal material droplet travels at least a portion of the predetermined distance.

Assignments (5)
TERMINATION AND RELEASE OF SECURITY INTEREST IN PATENTS RECORDED AT RF 064760/0389 Recorded Feb 13, 2024
From: CITIBANK, N.A., AS COLLATERAL AGENT
To: XEROX CORPORATION
Reel/Frame 068261/0001 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Dec 1, 2023
From: XEROX CORPORATION
To: ELEM ADDITIVE, LLC
Reel/Frame 065734/0413 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Dec 1, 2023
From: ELEM ADDITIVE, LLC
To: ADDITIVE TECHNOLOGIES LLC
Reel/Frame 065743/0267 →
SECURITY INTEREST Recorded Jun 22, 2023
From: XEROX CORPORATION
To: CITIBANK, N.A., AS COLLATERAL AGENT
Reel/Frame 064760/0389 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded May 15, 2019
From: VADER, SCOTT J, ,; VADER, ZACHARY S, ,; LIU, CHU-HENG , ,
To: XEROX CORPORATION
Reel/Frame 049184/0928 →
Continuity (2)
Provisional Application 62672302 · May 16, 2018
Related Publication 20190351488A1 · Nov 21, 2019