IP Library Granted Patent US 10,729,734
Granted Patent B2
US 10,729,734 · App. 16/429,214 · Granted Aug 4, 2020

Freeze dry process

Inventor: Stephen Goldner (West Bloomfield, MI)
Assignee: PURE GREEN PHARMACEUTICALS, INC.
A61K36/185A61K2236/17A61K2236/37
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Quick Facts
Patent No.
US 10,729,734
App. No.
16/429,214
Granted
Aug 4, 2020
Kind
B2
Abstract

A process includes rupturing plant cells of cannabis by freeze-drying the cannabis at a temperature below 0° C. in order to expose or release one or more chemicals including at least cannabinoids in the plant cells of the cannabis, after rupturing the cannabis plant cells, extracting the one or more chemicals including at least cannabinoids from the cannabis by pressurizing the cannabis in a pressure vessel with along with a solvent, the solvent dissolving the one or more chemicals including at least cannabinoids, followed by depressurizing the cannabis in the pressure vessel, where the depressurizing precipitates the one or more chemicals including at least cannabinoids out of the solvent, and then isolating the one or more chemicals including at least cannabinoids that precipitated from the solvent.

Claims (9)

1. A process consisting essentially of:

drying raw cannabis;

rupturing the cannabis cells in the raw cannabis by freeze-drying the dried raw cannabis at a temperature below 0° C. in order to expose or release one or more cannabinoids in the cells of the cannabis;

after rupturing the cannabis cells, extracting one or more cannabinoids in the cannabis by pressurizing the cannabis in a pressure vessel with along with a solvent, the solvent dissolving the one or more cannabinoids in the cannabis followed by depressurizing the cannabis in the pressure vessel, wherein the depressurizing precipitates the one or more cannabinoids out of the solvent; and

isolating the one or more cannabinoids that precipitated from the solvent, wherein the cannabinoids are selected from the group consisting of tetrahydrocannabinol, cannabidiol, cannabinol, cannabavarin, cannabigerol, cannabichromene, delta-8-THC, cannabicyclol, cannabitriol, and cannabielsoin.

2. The process of claim 1 , wherein the depressurizing is conducted at several pressure intervals.

3. The process of claim 1 , wherein the solvent is carbon dioxide.

4. The process of claim 1 , wherein the solvent is supercritical carbon dioxide.

5. The process of claim 1 , wherein the freeze-drying reduces the size of the cannabis into pieces.

Assignments (3)
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Dec 9, 2021
From: PURE GREEN, LLC
To: PURE GREEN PHARMACEUTICALS, INC.
Reel/Frame 058343/0628 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Aug 26, 2020
From: PURE GREEN PHARMACEUTICALS, INC.
To: PURE GREEN, LLC
Reel/Frame 053600/0876 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Mar 9, 2020
From: GOLDNER, STEPHEN
To: PURE GREEN PHARMACEUTICALS, INC.
Reel/Frame 052054/0048 →
Cited By (1)
US 12,235,043