IP Library Granted Patent US 10,746,677
Granted Patent B2
US 10,746,677 · App. 16/438,873 · Granted Aug 18, 2020

Optical flash point detection on an automated open cup flash point detector

Inventors: Michael Brosseau (Houston, TX); Thomas Herold (Boxberg-Uiffingen, DE); Simon Blass (Mergetsoechheim, DE); Oezkan Oguz (Lauda-Koenigshofen, DE)
Assignee: Petroleum Analyzer Company, LP
G01N25/50G01N21/33G01N25/52
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Quick Facts
Patent No.
US 10,746,677
App. No.
16/438,873
Granted
Aug 18, 2020
Kind
B2
Abstract

An open cup flash point detector is shown that rapidly increases the temperature of the substance being tested until temperature is close to a theoretical flash point. Thereafter, as temperature is slowly increased, an igniter flame moves in an arc over the upper lip of the test cup while simultaneously a UV sensor senses a wedge-shaped area, also immediately over the upper lip of the test cup. The arc of the igniter flame and the wedge-shaped area do not overlap. By incremental increases in temperature and repeating the arc movement of the igniter flame, the flash point can be detected by the UV sensor.

Claims (46)

1. A flash point detector, comprising:

a stand having an upper surface with an opening in the upper surface;

a test cup located in the opening;

a heater configured to heat the test cup and a substance contained within the test cup, wherein the test cup does not include a lid or cover;

an igniter configured to generate a flame above the test cup, wherein the flame is configured to periodically move within a first area above the test cup;

an ultraviolet (UV) detector located on the upper surface of the stand, wherein the UV detector is configured to:

monitor a second area above the test cup, wherein the second area does not overlap the first area, and

detect when the substance reaches the flash point; and

a chamber housing the entire UV detector, wherein the chamber includes an open area or slot configured to allow the UV detector to detect ultraviolet light from the second area and not from the first area.

2. The flash point detector of claim 1 , wherein the chamber further comprises:

a lens located on a first side of the open area or slot, wherein the lens includes a beam opening configured to allow ultraviolet light from the second area to reach the UV detector.

3. The flash point detector of claim 1 , wherein the igniter comprises:

an igniter motor; and

an igniter arm,

wherein the flame is located at an end of the igniter arm, and

wherein the igniter motor is configured to move the igniter arm within the first area.

4. The flash point detector of claim 3 , wherein the igniter motor is configured to periodically move the igniter arm in an arc above the test cup.

5. The flash point detector of claim 4 , wherein the heater is configured to incrementally increase a temperature of the substance while the igniter arm is periodically moved above the test cup.

6. The flash point detector of claim 3 , further comprising:

a temperature detector configured to measure and record the temperature of the substance in the test cup.

7. The flash point detector of claim 6 , wherein the temperature detector is further configured to record the temperature at which the UV detector detects that the substance reaches the flash point.

8. The flash point detector of claim 1 , wherein the second area comprises a wedge-shaped area.

9. The flash point detector of claim 1 , further comprising:

insulation located in the stand, wherein the insulation is configured to thermally insulate the test cup from the stand.

10. The flash point detector of claim 1 , further comprising:

a test cup holder configured to allow a user to pick up the test cup.

11. A method of determining a flash point of a substance using an open cup, comprising:

placing a substance in a test cup;

inserting the test cup in an upper opening of a stand;

continuously measuring a temperature of the substance in the test cup, wherein the test cup does not include a lid or cover;

increasing the temperature of the substance in the test cup until the substance approaches a flash point;

periodically moving a flame in a first area above the test cup;

monitoring a second area located above the test cup with an ultraviolet (UV) detector, housed entirely in a chamber, to detect when the substance flashes, wherein the second area does not overlap the first area, wherein the monitoring the second area comprises:

detecting ultraviolet light generated in the second area via an opening in the chamber; and

detecting the temperature of the substance when the substance flashes.

12. The method of claim 11 , wherein the periodically moving the flame comprises:

periodically moving the flame in an arc above the test cup, wherein the flame is located at an end of an igniter arm.

13. The method of claim 12 , further comprising:

igniting a gas source to generate the flame.

14. The method of claim 11 , further comprising:

recording the temperature when the substance flashes.

15. The method of claim 11 , wherein the opening comprises an opening in a lens located at one end of the chamber.

16. The method of claim 11 , wherein the monitoring an area comprises monitoring a wedge-shaped area above the test cup.

17. The method of claim 11 , wherein the increasing the temperature comprises;

increasing the temperature at a first rate until an estimated flash point is reached, and increasing the temperature at a second rate after the estimated flash point is reached, wherein the first rate is greater than the second rate.

18. The method of claim 11 , wherein the increasing the temperature comprises increasing the temperature while an igniter arm is moving the flame above the test cup.

Assignments (6)
CORRECTIVE ASSIGNMENT TO CORRECT THE PATENT NUMBER PREVIOUSLY RECORDED AT REEL: 61997 FRAME: 614. ASSIGNOR(S) HEREBY CONFIRMS THE SECURITY AGREEMENT. Recorded Nov 13, 2025
From: ALPHA TECHNOLOGIES SERVICES LLC; AMOT CONTROLS LLC; COMPRESSOR CONTROLS LLC; CORNELL PUMP COMPANY LLC; DYNISCO INSTRUMENTS LLC; HANSEN TECHNOLOGIES LLC; METRIX INSTRUMENT CO., L.P.; PETROLEUM ANALYZER COMPANY L.P.; ROPER HOLDINGS, LLC; ROPER INDUSTRIAL PRODUCTS INVESTMENT COMPANY LLC; ROPER PUMP COMPANY LLC; STRUERS LLC; VIA TRAN CORPORATION
To: UBS AG, STAMFORD BRANCH, AS COLLATERAL AGENT
Reel/Frame 073434/0453 →
RELEASE OF SECOND LIEN PATENT SECURITY INTERESTS Recorded May 30, 2025
From: ROYAL BANK OF CANADA
To: AGR INTERNATIONAL, INC.; ALPHA TECHNOLOGIES SERVICES LLC; AMOT CONTROLS LLC; COMPRESSOR CONTROLS LLC; CORNELL PUMP COMPANY LLC; DYNISCO INSTRUMENTS LLC; HANSEN TECHNOLOGIES LLC; METRIX INSTRUMENT CO., L.P.; PETROLEUM ANALYZER COMPANY L.P.; ROPER HOLDINGS, LLC; ROPER INDUSTRIAL PRODUCTS INVESTMENT COMPANY LLC; ROPER PUMP COMPANY LLC; STRUERS LLC; VIATRAN CORPORATION
Reel/Frame 071476/0346 →
CHANGE OF NAME Recorded Apr 25, 2025
From: PETROLEUM ANALYZER COMPANY L.P.
To: PRECISION ANALYZER COMPANY L.P.
Reel/Frame 071058/0188 →
SECURITY AGREEMENT (FIRST LIEN) Recorded Nov 28, 2022
From: ALPHA TECHNOLOGIES SERVICES LLC; AMOT CONTROLS LLC; COMPRESSOR CONTROLS LLC; CORNELL PUMP COMPANY LLC; DYNISCO INSTRUMENTS LLC; HANSEN TECHNOLOGIES LLC; METRIX INSTRUMENT CO., L.P.; PETROLEUM ANALYZER COMPANY L.P.; ROPER HOLDINGS, LLC; ROPER INDUSTRIAL PRODUCTS INVESTMENT COMPANY LLC; ROPER PUMP COMPANY LLC; STRUERS LLC; VIATRAN CORPORATION
To: UBS AG, STAMFORD BRANCH, AS COLLATERAL AGENT
Reel/Frame 061997/0614 →
SECURITY AGREEMENT (SECOND LIEN) Recorded Nov 28, 2022
From: ALPHA TECHNOLOGIES SERVICES LLC; AMOT CONTROLS LLC; COMPRESSOR CONTROLS LLC; CORNELL PUMP COMPANY LLC; DYNISCO INSTRUMENTS LLC; HANSEN TECHNOLOGIES LLC; METRIX INSTRUMENT CO., L.P.; PETROLEUM ANALYZER COMPANY L.P.; ROPER HOLDINGS, LLC; ROPER INDUSTRIAL PRODUCTS INVESTMENT COMPANY LLC; ROPER PUMP COMPANY LLC; STRUERS LLC; VIATRAN CORPORATION
To: ROYL BANK OF CANADA, AS COLLATERAL AGENT
Reel/Frame 062003/0566 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Jun 12, 2019
From: BROSSEAU, MICHAEL; HEROLD, THOMAS; BLASS, SIMON; OGUZ, OEZKAN
To: PETROLEUM ANALYZER COMPANY, LP
Reel/Frame 049447/0055 →