IP Library Granted Patent US 11,168,350
Granted Patent B2
US 11,168,350 · App. 16/442,349 · Granted Nov 9, 2021

Highly-multiplexed fluorescent imaging

Inventors: Garry P. Nolan (Redwood City, CA); Nikolay Samusik (Mountain View, CA); Julia Kennedy-Darling (Stanford, CA); Yury Goltsev (Stanford, CA)
Assignee: The Board of Trustees of the Leland Stanford Junior University
C12Q1/6804C12Q1/6813G01N1/30G01N33/5308G01N33/54306G01N33/554G01N2001/302G01N2458/10
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Quick Facts
Patent No.
US 11,168,350
App. No.
16/442,349
Granted
Nov 9, 2021
Kind
B2
Abstract

Provided herein is a method and system for analyzing a sample. In some embodiments the method makes use of a plurality of capture agents that are each linked to a different oligonucleotide and a corresponding plurality of labeled nucleic acid probes, wherein each of the labeled nucleic acid probes specifically hybridizes with only one of the oligonucleotides. The sample is labeled with the capture agents en masse, and sub-sets of the capture agents are detected using iterative cycles using corresponding subsets of the labeled nucleic acid probes.

Claims (22)

1. A composition comprising:

(a) a sample comprising fixed cells;

(b) a plurality of capture agents that are each linked to a different oligonucleotide;

(c) a corresponding plurality of labeled nucleic acid probes, wherein each of the labeled nucleic acid probes specifically hybridizes with only one of the oligonucleotides of (b); and

(d) a chemical denaturant, wherein the chemical denaturant comprises a compound selected from the group consisting of urea, DMSO, formamide, and a chaotropic agent;

wherein the sample is labeled with the plurality of capture agents.

2. The composition of claim 1 , wherein the capture agent comprises an antibody or an aptamer.

3. The composition of claim 2 , wherein each capture agent is covalently linked to the different oligonucleotide.

4. The composition of claim 3 , wherein each capture agent is covalently linked to the different oligonucleotide by a linkage selected from the group consisting of a maleimide group, or a cysteine-reactive group.

5. The composition of claim 3 , comprising a plurality of antibodies covalently linked to different nucleotides.

6. The composition of claim 1 , wherein the composition comprises at least 30% of the chemical denaturant.

7. The composition of claim 6 , wherein the chemical denaturant is at least 30% formamide.

8. The composition of claim 1 , wherein the nucleic acid probes are hybridized to the different oligonucleotides.

9. The composition of claim 1 , wherein the nucleic acid probes are not hybridized to the different oligonucleotides.

10. The composition of claim 1 , wherein one or more of the plurality of nucleic acid probes are removed in the presence of the chemical denaturant.

11. The composition of claim 1 , wherein the composition does not comprise displacement probes.

12. The composition of claim 1 , wherein the nucleic acid probe comprises a detectable label selected from the group consisting of a fluorophore, a fluorescent protein, a visible stain, a polychromatic barcode, a mass tag, a structural tag, a radio sensitive tag, a radioactive tag, or an absorbance tag.

13. The composition of claim 12 , further comprising an enzyme that amplifies signal of the detectable label.

14. The composition of claim 1 , wherein the chemical denaturant comprises a chaotropic agent.

15. The composition of claim 14 , wherein the chaotropic agent is guanidinium chloride.

16. The composition of claim 2 , wherein each capture agent is non-covalently linked to the different oligonucleotide.

17. The composition of claim 16 , wherein each capture agent is non-covalently linked to the different oligonucleotide by a streptavidin-biotin linkage.

Assignments (3)
RELEASE OF SECURITY INTEREST Recorded Jul 11, 2025
From: MIDCAP FINANCIAL TRUST
To: AKOYA BIOSCIENCES, INC.
Reel/Frame 071893/0033 →
SECURITY INTEREST Recorded Jun 4, 2025
From: AKOYA BIOSCIENCES, INC.
To: MIDCAP FINANCIAL TRUST
Reel/Frame 071484/0056 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Jun 18, 2019
From: NOLAN, GARRY P.; SAMUSIK, NIKOLAY; KENNEDY-DARLING, JULIA; GOLTSEV, YURY
To: THE BOARD OF TRUSTEES OF THE LELAND STANFORD JUNIOR UNIVERSITY
Reel/Frame 049502/0942 →