IP Library Granted Patent US 11,186,657
Granted Patent B2
US 11,186,657 · App. 16/445,599 · Granted Nov 30, 2021

Hyperbranched polymer, metal recovery agent, metal recovery method, and catalytic activity inhibitor

Inventors: Naoki Usuki (Mishima-gun, JP); Akiko Kito (Takatsuki, JP); Atsushi Yusa (Nagaokakyo, JP)
Assignee: MAXELL, LTD.
C08F12/30B01J20/261B01J20/3214B01J20/3276C08F8/30C08F212/36C08F220/56C08F293/00C22B11/00C22B11/04C23C18/18
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Quick Facts
Patent No.
US 11,186,657
App. No.
16/445,599
Granted
Nov 30, 2021
Kind
B2
Abstract

There is provided a hyper-branched polymer represented by the following formula (1) and having a weight-average molecular weight in a range of 1,000 to 1,000,000. In the formula (1), A 1 is a group containing an aromatic ring, A 2 is a group containing an amide group, A 3 is a group containing sulfur, R 0 is hydrogen or a substituted or unsubstituted hydrocarbon group having 1 to 10 carbon atoms, ml is in a range of 0.5 to 11, and n1 is in a range of 5 to 100.

Claims (20)

1. A hyper-branched polymer represented by the following formula (1) and having a weight-average molecular weight in a range of 1,000 to 1,000,000:

wherein in the formula (1), A 1 is a group containing an aromatic ring, A 2 is a group containing an amide group, A 3 is a group containing sulfur, R 0 is hydrogen or a substituted or unsubstituted hydrocarbon group having 1 to 10 carbon atoms, ml is in a range of 0.5 to 11, and n1 is in a range of 5 to 100.

2. The hyper-branched polymer according to claim 1 , wherein in the formula (1), A 1 is a group represented by the following formula (2), and A 3 is a dithiocarbamate group.

3. The hyper-branched polymer according to claim 1 , wherein in the formula (1), A 2 is a group represented by the following formula (3):

in the formula (3), R 1 is a single bond or a substituted or unsubstituted alkylene group having 1 to 5 carbon atoms, and R 2 and R 3 are each hydrogen or a substituted or unsubstituted alkyl group having 1 to 10 carbon atoms.

4. The hyper-branched polymer according to claim 3 , wherein in the formula (3), R 1 is the single bond, R 2 is the hydrogen, and R 3 is an isopropyl group.

5. The hyper-branched polymer according to claim 1 , wherein in the formula (1), A 3 is a group represented by the following formula (4):

in the formula (4), R 4 and R 5 are each hydrogen or a substituted or unsubstituted alkyl group having 1 to 5 carbon atoms.

6. The hyper-branched polymer according to claim 5 , wherein in the formula (4), R 4 and R 5 are each an ethyl group.

7. The hyper-branched polymer according to claim 1 , wherein in the formula (1), a ratio of a total molar number of the amide group contained in A 2 to a molar number of A 3 which is the group containing sulfur is in a range of not less than 0.5 to less than 1.5.

8. The hyper-branched polymer according to claim 1 , wherein in the formula (1), A 3 is a dithiocarbamate group; and

a ratio of a total molar number of the amide group contained in A 2 to a molar number of A 3 which is the group containing sulfur is in a range of 0.5 to 1.5.

9. The hyper-branched polymer according to claim 1 , wherein in the formula (1), R 0 is a vinyl group.

10. The hyper-branched polymer according to claim 1 , wherein the hyper-branched polymer is a mixture of a hyper-branched polymer in which the R 0 in the formula (1) is a vinyl group and a hyper-branched polymer in which the R 0 in the formula (1) is an ethyl group.

11. A metal recovery agent recovering a metal in a liquid in which the metal is dissolved, comprising the hyper-branched polymer as defined in claim 1 .

12. A metal-recovering method of recovering a metal in a liquid in which the metal is dissolved, the method comprising:

preparing a solution of a hyper-branched polymer by dissolving the hyper-branched polymer as defined in claim 1 in a solvent;

applying the solution of the hyper-branched polymer onto a substrate so as to form a hyper-branched polymer layer; and

causing the liquid to make contact with the hyper-branched polymer layer to thereby make the metal in the liquid to adsorb to the hyper-branched polymer layer and to recover the metal.

13. A catalytic activity inhibitor inhibiting catalytic activity of an electroless plating catalyst, the catalytic activity inhibitor comprising the hyper-branched polymer as defined in claim 1 .

Assignments (2)
CHANGE OF NAME Recorded Dec 3, 2021
From: MAXELL HOLDINGS, LTD.
To: MAXELL, LTD.
Reel/Frame 058301/0318 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Jun 19, 2019
From: USUKI, NAOKI; KITO, AKIKO; YUSA, ATSUSHI
To: MAXELL HOLDINGS, LTD.
Reel/Frame 049518/0446 →
Priority Claims (1)
JP JP2017-004296 · Jan 13, 2017 · national
Continuity (2)
Continuation PCTJP2017047054 · Dec 27, 2017
Related Publication 20190309104A1 · Oct 10, 2019