IP Library Granted Patent US 10,988,460
Granted Patent B2
US 10,988,460 · App. 16/468,446 · Granted Apr 27, 2021

Substituted pyrazole-pyrimidines, variants thereof, and uses therefore

Inventors: Ronald Charles Hawley (San Mateo, CA); Prabha Ibrahim (San Mateo, CA); Anthony P. Ford (Palo Alto, CA); Joel R. Gever (Palo Alto, CA)
Assignee: Afferent Pharmaceuticals, Inc.
C07D403/12
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Quick Facts
Patent No.
US 10,988,460
App. No.
16/468,446
Granted
Apr 27, 2021
Kind
B2
Abstract

Disclosed herein are substituted pyrazole-pyrimidine compounds of Formula (I) and variants thereof for the treatment, for example, of diseases associated with P2X purinergic receptors. In one embodiment, the P2X3 and/or P2X2/3 antagonists disclosed herein are potentially useful, for example, for the treatment of visceral organ, cardiovascular and pain-related diseases, conditions and disorders.

Claims (56)

1. A compound of Formula I:

or a pharmaceutically acceptable salt thereof, wherein:

ring

is selected from the group consisting of:

W is CH 2 , NH, N—C 1-6 alkylene, O or S;

X 6 is CR 3 ; wherein R 3 is hydrogen or C 1-12 alkyl;

Y is hydrogen or —NHR d ; wherein R d is selected from the group consisting of hydrogen, C 1-12 alkyl, C 3-12 cycloalkyl, aryl, and heteroaryl; wherein each of the C 1-12 alkyl, C 3-12 cycloalkyl, aryl, and heteroaryl is optionally substituted with one to three substituents independently selected from halogen, hydroxyl and C 1-6 alkyl;

D is an optional oxygen;

each occurrence of R 1 is independently selected from the group consisting of hydrogen, hydroxyl, C 1-6 alkyl, C 2-6 alkenyl, and C 2-6 alkynyl; wherein each of the C 1-6 alkyl, C 2-6 alkenyl, and C 2-6 alkynyl is optionally substituted with one to three substituents independently selected from halogen and hydroxyl;

each occurrence of R 2 is independently selected from the group consisting of hydrogen, halogen, —NH—R f , —C(O)—NHR f , C 2-12 alkenyl, C 2-12 alkynyl, and —O—C 1-12 alkyl;

each occurrence of R f is independently selected from the group consisting of hydrogen, C 1-12 alkYl, hydroxyl, —SO 2 —NH 2 , and —SO 2 —C 1-6 alkyl; and

R 7 is selected from the group consisting of hydrogen, C 1-12 alkyl, and C 3-12 cycloalkyl.

2. The compound of claim 1 , or a pharmaceutically acceptable salt thereof, wherein:

W is CH 2 or O;

X 6 is CH;

Y is hydrogen or —NHR d ; wherein R d is selected from the group consisting of hydrogen or C 1-6 alkyl; wherein the C 1-6 alkyl is optionally substituted with one to three substituents independently selected from halogen and hydroxyl;

D is absent;

each occurrence of R 1 is independently selected from the group consisting of hydrogen and C 1-6 alkyl;

each occurrence of R 2 is independently selected from the group consisting of hydrogen, halogen, —NH—R f , —C(O)—NHR f , —C(O)—C 1-6 alkyl, C 2-6 alkenyl, and —O—C 1-6 alkyl;

each occurrence of R f is independently selected from the group consisting of hydrogen, C 1-6 alkyl, hydroxyl, —SO 2 —NH 2 , and —SO 2 —C 1-6 alkyl; and

R 7 is selected from the group consisting of hydrogen and C 1-6 alkyl.

3. The compound of claim 1 , or a pharmaceutically acceptable salt thereof, having formulae Ia:

4. The compound of claim 1 having the following formula Ib, or a pharmaceutically acceptable salt thereof:

5. The compound of claim 4 , or a pharmaceutically acceptable salt thereof, wherein:

W is CH 2 or O;

R 1 is selected from the group consisting of hydrogen and C 1-6 alkyl;

R 2 is selected from the group consisting of hydrogen, halogen, —NH 2 ; —C(O)—NH 2 , —C(O)—C 1-6 alkyl, and —O—C 1-6 alkyl; and

R d is selected from the group consisting of hydrogen and C 1-6 alkyl.

6. The compound of claim 1 having one of the following formulae Ic and Id, or a pharmaceutically acceptable salt thereof:

7. The compound of claim 6 having the following formula Ie, or a pharmaceutically acceptable salt thereof:

8. The compound of claim 6 having the following formula If, or a pharmaceutically acceptable salt thereof:

9. The compound of claim 7 , or a pharmaceutically acceptable salt thereof, wherein:

W is CH 2 or O;

R 1 is selected from the group consisting of hydrogen and C 1-6 alkyl;

R 2 is selected from the group consisting of hydrogen, halogen, —NH 2 , —C(O)—NH 2 , —C(O)—C 1-6 alkyl, and —O—C 1-6 alkyl; and

R d is selected from the group consisting of hydrogen and C 1-6 alkyl.

10. The compound of claim 1 , wherein W is O, or a pharmaceutically acceptable salt thereof.

11. The compound of claim 1 , wherein W is CH 2 , or a pharmaceutically acceptable salt thereof.

12. A compound selected from the group consisting of:

or a pharmaceutically acceptable salt thereof.

13. A composition which comprises an inert carrier and a compound of claim 1 or a pharmaceutically acceptable salt thereof.

14. A method for slowing or interrupting the progression of a P2X3 and/or P2X2/3 associated disease or disorder, wherein the disorder is pain, comprising administering to a subject in need thereof an effective amount of a compound of claim 1 , or a pharmaceutically acceptable salt thereof.

15. The compound of claim 3 , wherein:

W is CH 2 or O;

R 1 is selected from the group consisting of hydrogen and C 1-6 alkyl;

R 2 is selected from the group consisting of hydrogen, halogen, —NH 2 ; —C(O)—NH 2 , —C(O)—C 1-6 alkyl, and —O—C 1-6 alkyl; and

R d is selected from the group consisting of hydrogen and C 1-6 alkyl;

or a pharmaceutically acceptable salt thereof.

16. The compound of claim 15 , wherein W is CH 2 , or a pharmaceutically acceptable salt thereof.

17. The compound of claim 8 , wherein:

W is CH 2 or O;

R 1 is selected from the group consisting of hydrogen and C 1-6 alkyl;

R 2 is selected from the group consisting of hydrogen, halogen, —NH 2 , —C(O)—NH 2 , —C(O)—C 1-6 alkyl, and —O—C 1-6 alkyl; and

R d is selected from the group consisting of hydrogen and C 1-6 alkyl;

or a pharmaceutically acceptable salt thereof.

18. The compound of claim 17 , wherein W is O, or a pharmaceutically acceptable salt thereof.

Assignments (3)
CORRECTIVE ASSIGNMENT TO CORRECT THE APPLICATION NUMBER 17197705 PREVIOUSLY RECORDED AT REEL: 061574 FRAME: 0579. ASSIGNOR(S) HEREBY CONFIRMS THE ASSIGNMENT . Recorded Dec 1, 2022
From: AFFERENT PHARMACEUTICALS, INC.
To: AFFERENT PHARMACEUTICALS, INC.
Reel/Frame 062036/0001 →
CHANGE OF ADDRESS Recorded Sep 30, 2022
From: AFFERENT PHARMACEUTICALS, INC.
To: AFFERENT PHARMACEUTICALS, INC.
Reel/Frame 061574/0579 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Jun 11, 2019
From: HAWLEY, RONALD CHARLES; IBRAHIM, PRABHA; FORD, ANTHONY P; GEVER, JOEL R
To: AFFERENT PHARMACEUTICALS, INC.
Reel/Frame 049433/0769 →
Continuity (2)
Provisional Application 62434513 · Dec 15, 2016
Related Publication 20200239451A1 · Jul 30, 2020