IP Library Granted Patent US 11,554,965
Granted Patent B2
US 11,554,965 · App. 16/469,807 · Granted Jan 17, 2023

Method for producing lithium hydroxide from lithium phosphate

Inventors: Kyunghoon Kim (Pohang-si, KR); Sang Min Lee (Pohang-si, KR); Jong-Hak Lee (Pohang-si, KR); Ki Young Kim (Pohang-si, KR); Jae Hyug Choi (Pohang-si, KR); Souhwan Son (Pohang-si, KR)
Assignee: POSCO CO., LTD
C01D15/02C01B25/30C01B25/32C01F11/46
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Quick Facts
Patent No.
US 11,554,965
App. No.
16/469,807
Granted
Jan 17, 2023
Kind
B2
Abstract

The present invention relates to a method of manufacturing lithium hydroxide, which includes adding at least one acid selected from hydrochloric acid, sulfuric acid, and nitric acid into lithium phosphate slurry including a lithium phosphate particle, adding an alkali material to the lithium phosphate slurry including the acid, and converting it into a lithium hydroxide aqueous solution.

Claims (9)

1. A method of manufacturing lithium hydroxide, comprising

adding at least one acid selected from hydrochloric acid, sulfuric acid, and nitric acid into lithium phosphate slurry including a lithium phosphate particle;

adding an alkali material to the lithium phosphate slurry including the acid and converting it into a lithium hydroxide aqueous solution; and

after adding the alkali material to the lithium phosphate slurry including the acid and converting it into the lithium hydroxide aqueous solution, concentrating the lithium hydroxide aqueous solution to prepare the lithium hydroxide,

wherein an amount of the added acid ranges from 0.67 equivalents to 1.0 equivalents based on an amount of the lithium phosphate particle, and

the lithium phosphate slurry including the acid has a lithium concentration of 4,000 mg/L to 2,000 mg/L.

2. The method of manufacturing lithium hydroxide of claim 1 , wherein an amount of the added alkali material may range from 0.8 to 1.5 equivalents based on an amount of the lithium phosphate particle.

3. The method of manufacturing lithium hydroxide of claim 1 , wherein the alkali material is one or more selected from the group consisting of Ca(OH) 2 , NaOH, and CaO.

4. The method of manufacturing lithium hydroxide of claim 1 , wherein in the step of adding the alkali material to the lithium phosphate slurry including the acid and converting it into the lithium hydroxide aqueous solution, gypsum and hydroxyapatite are precipitated.

Assignments (3)
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Oct 26, 2022
From: POSCO HOLDINGS INC.
To: POSCO CO., LTD
Reel/Frame 061774/0129 →
CHANGE OF NAME Recorded Sep 28, 2022
From: POSCO
To: POSCO HOLDINGS INC.
Reel/Frame 061561/0705 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Jun 14, 2019
From: KIM, KYUNGHOON; LEE, SANG MIN; LEE, JONG-HAK; KIM, KI YOUNG; CHOI, JAE HYUG; SON, SOUHWAN
To: POSCO
Reel/Frame 049470/0455 →
Priority Claims (1)
KR 10-2016-0171619 · Dec 15, 2016 · national
Continuity (1)
Related Publication 20200079657A1 · Mar 12, 2020