Laser-induced spectroscopy system and process
Specialized linkage assemblies for Laser-Induced Breakdown Spectroscopy (“LIBS”) systems are provided. The linkage assemblies may facilitate the attachment of the laser housing of the LIBS system onto an existing sample supply chamber, such as a volumetric or gravimetric feeder. Generally, the linkage assemblies may comprise a specialized purge head and inert gas assembly that facilitate the attachment of the laser housing and may enhance the functionality of the LIBS system.
1. A linkage assembly for a laser-induced breakdown spectroscopy system, said linkage assembly comprising an inert gas flange assembly, wherein said inert gas flange assembly comprises:
(a) an inert gas flange comprising an inert gas intake for transferring an inert gas into said inert gas flange, wherein said inert gas intake comprises a tube, a pipe, or a borehole; and
(b) a removable lens housing comprising a first lens and a second lens,
wherein said removable lens housing is positioned within said inert gas flange and is in fluid communication with said inert gas intake,
wherein said first lens comprises an aperture allowing the flow of said inert gas from said lens housing to outside of said linkage assembly.
2. The linkage assembly according to claim 1 , wherein said second lens comprises a solid lens.
3. The linkage assembly according to claim 1 , wherein said aperture is positioned in the center of said first lens.
4. The linkage assembly according to claim 3 , wherein said first lens comprises a plurality of additional apertures surrounding said aperture.
5. The linkage assembly according to claim 1 , wherein said inert gas assembly comprises one or more O-rings for positioning said lens housing.
6. The linkage assembly according to claim 1 , wherein said inert gas comprises argon gas.
7. The linkage assembly according to claim 1 , wherein said linkage assembly further comprises a purge head and a leak-resistant valve, wherein said inert gas intake is in fluid communication with said purge head and said leak-resistant valve.
8. A laser-induced breakdown spectroscopy system, said laser-induced breakdown spectroscopy system comprising:
(a) a laser housing comprising a laser source and a spectrometer; and
(b) a linkage assembly for connecting said laser housing to a sample supply chamber, wherein said linkage assembly comprises an inert gas flange assembly, wherein said inert gas flange assembly comprises—
(i) an inert gas flange comprising an inert gas intake for transferring an inert gas into said inert gas flange, wherein said inert gas intake comprises a tube, a pipe, or a borehole; and
(ii) a removable lens housing comprising a first lens and a second lens,
wherein said removable lens housing is positioned within said inert gas flange and is in fluid communication with said inert gas intake,
wherein said first lens comprises an aperture allowing the flow of said inert gas from said lens housing to said sample supply chamber.
9. The laser-induced breakdown spectroscopy system according to claim 8 , wherein said second lens comprises a solid lens.
10. The laser-induced breakdown spectroscopy system according to claim 8 , wherein said aperture is positioned in the center of said first lens.
11. The laser-induced breakdown spectroscopy system according to claim 10 , wherein said first lens comprises a plurality of additional apertures surrounding said aperture.
12. The laser-induced breakdown spectroscopy system according to claim 8 , wherein said inert gas assembly comprises one or more O-rings for positioning said lens housing.
13. The laser-induced breakdown spectroscopy system according to claim 8 , wherein said inert gas comprises argon gas.
14. The laser-induced breakdown spectroscopy system according to claim 8 , wherein said linkage assembly further comprises a purge head and a leak-resistant valve, wherein said inert gas intake is in fluid communication with said purge head and said leak-resistant valve.
15. A method for operating a laser-induced breakdown spectroscopy system, said method comprising:
(a) providing a laser housing comprising a laser source and a spectrometer connected to a sample supply chamber via a linkage assembly, wherein said linkage assembly comprises an inert gas flange assembly, wherein said inert gas flange assembly comprises—
(i) an inert gas flange comprising an inert gas intake for transferring an inert gas into said inert gas flange, wherein said inert gas intake comprises a tube, a pipe, or a borehole; and
(ii) a removable lens housing comprising a first lens and a second lens,
wherein said removable lens housing is positioned within said inert gas flange and is in fluid communication with said inert gas intake,
wherein said first lens comprises an aperture allowing the flow of said inert gas from said lens housing to said sample supply chamber;
(b) contacting said sample with said laser inside said sample supply chamber.
16. The method according to claim 15 , wherein said second lens comprises a solid lens.
17. The method according to claim 15 , wherein said aperture is positioned in the center of said first lens, wherein said first lens comprises a plurality of additional apertures surrounding said aperture.
18. The method according to claim 15 , wherein said inert gas assembly comprises one or more O-rings for positioning said lens housing.
19. The method according to claim 15 , wherein said inert gas comprises argon gas.
20. The method according to claim 15 , wherein said linkage assembly further comprises a purge head and a leak-resistant valve, wherein said inert gas intake is in fluid communication with said purge head and said leak-resistant valve.