IP Library Granted Patent US 11,471,946
Granted Patent B2
US 11,471,946 · App. 16/563,278 · Granted Oct 18, 2022

Additive manufacturing of ferritic/martensitic steel with improved high temperature strength

Inventors: Thomas J. Lienert (Los Alamos, NM); Stuart Andrew Maloy (Los Alamos, NM); Benjamin P. Eftink (Los Alamos, NM); Daniel Vega (Los Alamos, NM)
Assignee: Triad National Security, LLC
B22F12/00B33Y80/00C22F1/00B22F10/10B22F2301/35B33Y10/00B33Y30/00B33Y70/00C21D2211/008
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Quick Facts
Patent No.
US 11,471,946
App. No.
16/563,278
Granted
Oct 18, 2022
Kind
B2
Abstract

Techniques for using additive manufacturing (AM) to fabricate creep resistant ferritic/martensitic steel with improved high temperature strength are described. AM processing may be performed on Grade 91 steel powder. Beam powers from about 221 W to about 270 W may be used. Traverse rates from about 675 mm/s to about 825 mm/s may be used. Heat inputs ranging from about 55.7 J/mm 3 to about 83.2 J/mm 3 may be produced. Creep resistant ferritic/martensitic steel, produced according to the present disclosure, has improved strain yield strength and ductility as compared to wrought steel.

Claims (28)

1. A creep resistant ferritic and martensitic steel produced from powder bed fusion (PBF) additive manufacturing (AM) of steel powder, comprising:

improved ductility as compared to a wrought steel;

wherein the creep resistant ferritic and martensitic steel is produced from PBF AM of Grade 91 steel powder; and

wherein when the creep resistant ferritic and martensitic steel is annealed for about 20 hours at 600° C., the annealed creep resistant ferritic and martensitic steel has a strain yield strength of 870 MPa at room temperature.

2. The creep resistant ferritic and martensitic steel of claim 1 , wherein the creep resistant ferritic and martensitic steel has a strain yield strength of 700 MPa at 600° C.

3. The creep resistant ferritic and martensitic steel of claim 1 , wherein the creep resistant ferritic and martensitic steel has a ductility of 0.09 at room temperature.

4. The creep resistant ferritic and martensitic steel of claim 1 , wherein the creep resistant ferritic and martensitic steel has a ductility of 0.05 at 600° C.

5. The creep resistant ferritic and martensitic steel of claim 1 , wherein:

the annealed creep resistant ferritic and martensitic steel has a ductility of 0.08 at room temperature.

6. The creep resistant ferritic and martensitic steel of claim 1 , wherein:

the annealed creep resistant ferritic and martensitic steel has a ductility of 0.03 at 600° C.

7. A creep resistant ferritic and martensitic steel produced from powder bed fusion (PBF) additive manufacturing (AM) of steel powder, comprising:

improved ductility as compared to a wrought steel;

wherein the creep resistant ferritic and martensitic steel is produced from PBF AM of Grade 91 steel powder; and

wherein when the creep resistant ferritic and martensitic steel is annealed for about 20 hours at 600° C., the annealed creep resistant ferritic and martensitic steel has a strain yield strength of 680 MPa at room temperature.

8. A creep resistant ferritic and martensitic steel produced from powder bed fusion (PBF) additive manufacturing (AM) of steel powder, comprising:

improved ductility as compared to a wrought steel;

wherein the creep resistant ferritic and martensitic steel is produced from PBF AM of Grade 91 steel powder; and

wherein when the creep resistant ferritic and martensitic steel is annealed for about 20 hours at 600° C., the annealed creep resistant ferritic and martensitic steel has a strain yield strength of 835 MPa at room temperature.

9. A method of producing the creep resistant ferritic and martensitic steel according to claim 1 , the method comprising:

obtaining a Grade 91 steel powder; and

performing a powder bed fusion (PBF) additive manufacturing (AM) using the Grade 91 steel powder.

10. The method of claim 9 , wherein the performing comprises using a beam power between about 221 W and about 270 W.

11. The method of claim 9 , wherein the performing comprises using a traverse rate between about 675 mm/s and about 825 mm/s.

12. The method of claim 9 , wherein the performing comprises producing a heat input between about 55.7 J/mm 3 and about 83.2 J/mm 3 .

13. The method of claim 9 , wherein the performing comprises a heat input value of about 68.1 J/mm 3 .

14. The method of claim 9 , wherein the performing comprises rotating a direction of deposition.

15. The method of claim 14 , wherein directions of deposition of adjacent layers of the steel powder are rotated about 67°.

Assignments (2)
CONFIRMATORY LICENSE Recorded Jun 15, 2020
From: TRIAD NATIONAL SECURITY, LLC
To: U.S. DEPARTMENT OF ENERGY
Reel/Frame 052937/0639 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Mar 12, 2020
From: LIENERT, THOMAS J.; MALOY, STUART A.; EFTINK, BENJAMIN P.; VEGA, DANIEL
To: TRIAD NATIONAL SECURITY, LLC
Reel/Frame 052094/0936 →
Continuity (2)
Provisional Application 62727776 · Sep 6, 2018
Related Publication 20200078865A1 · Mar 12, 2020