IP Library Granted Patent US 11,235,435
Granted Patent B1
US 11,235,435 · App. 16/566,435 · Granted Feb 1, 2022

Methods of fabricating polycrystalline diamond elements

Inventors: Brandon Paul Linford (Draper, UT); Cody William Knuteson (Salem, UT)
Assignee: US SYNTHETIC CORPORATION
B24D3/10B24D18/0009E21B10/46E21B10/55E21B10/567
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Quick Facts
Patent No.
US 11,235,435
App. No.
16/566,435
Granted
Feb 1, 2022
Kind
B1
Abstract

Embodiments relate to polycrystalline diamond compacts (“PDCs”) including a polycrystalline diamond (“PCD”) table having a diamond grain size distribution selected for improving leachability. In an embodiment, a PDC includes a PCD table bonded to a substrate. The PCD table includes diamond grains exhibiting diamond-to-diamond bonding therebetween. The diamond grains includes a first amount being about 30 to about 65 volume % of the diamond grains and a second amount being about 18 to about 65 volume % of the diamond grains. The first amount exhibits a first average grain size of about 8 μm to about 22 μm. The second amount exhibits a second average grain size that is greater than the first average grain size and is about 15 μm to about 50 μm. Other embodiments are directed methods of forming PDCs, and various applications for such PDCs in rotary drill bits, bearing apparatuses, and wire-drawing dies.

Claims (34)

1. A rotary drill bit, comprising:

a bit body including a leading end structure configured to facilitate drilling a subterranean formation and having one or more blades; and

at least one cutting element mounted to the bit body, the at least one cutting element including:

a substrate; and

a polycrystalline diamond table bonded to the substrate, the polycrystalline diamond table including a plurality of diamond grains exhibiting diamond-to-diamond bonding therebetween, the plurality of diamond grains including:

a first amount being about 55 weight % to about 65 weight % of the plurality of diamond grains, the first amount exhibiting a first average grain size of about 8 μm to about 14 μm;

a second amount being about 35 weight % to about 45 weight % of the plurality of diamond grains, the second amount exhibiting a second average grain size that is greater than the first average grain size and is about 15 μm to about 55 μm; and

a third amount being greater than 0 weight % to about 40 weight % of the plurality of diamond grains that exhibits a third average grain size of about 18 μm and 22 μm that is greater than the first average grain size and less than the second average grain size.

2. The rotary drill bit of claim 1 , wherein the first average grain size is about 10 μm to about 12 μm and the second average grain size is about 18 μm to about 22 μm.

3. The rotary drill bit of claim 1 , wherein the first amount is about 58 weight % to about 62 weight % and the second amount is about 38 weight % to about 42 weight %.

4. The rotary drill bit of claim 3 , wherein the first average grain size is about 10 μm to about 12 μm and the second average grain size is about 18 μm to about 22 μm.

5. The rotary drill bit of claim 1 , wherein the polycrystalline diamond table includes one or more of niobium, molybdenum, tantalum, tungsten, rhenium, hafnium, or alloys thereof in a range from greater than 0 weight % to about 5 weight % of the polycrystalline diamond table.

6. The rotary drill bit of claim 1 , wherein the polycrystalline diamond table includes boron in a range from greater than 0 weight % to about 0.2 weight % of the polycrystalline diamond table.

7. The rotary drill bit of claim 1 , wherein the polycrystalline diamond table is integrally formed with the substrate.

8. The rotary drill bit of claim 1 , wherein the polycrystalline diamond table includes at least one exterior surface and a leached region extending inwardly from the at least one exterior surface to a depth of at least 250 μm.

9. The rotary drill bit of claim 1 , wherein the polycrystalline diamond table includes at least one exterior surface and a leached region extending inwardly from the at least one exterior surface to a depth of about 400 μm to about 600 μm.

10. The rotary drill bit of claim 1 , wherein the polycrystalline diamond table includes at least one exterior surface and a leached region extending inwardly from the at least one exterior surface to a depth of about 600 μm to about 800 μm.

11. The rotary drill bit of claim 1 , wherein the at least one cutting element exhibits a G ratio of about 2.5×10 7 to about 3.5×10 7 .

12. A rotary drill bit, comprising:

a bit body including a leading end structure configured to facilitate drilling a subterranean formation and having one or more blades; and

at least one cutting element mounted to the bit body, the at least one cutting element including:

a substrate; and

a polycrystalline diamond table bonded to the substrate, the polycrystalline diamond table including a plurality of diamond grains exhibiting diamond-to-diamond bonding therebetween, the plurality of diamond grains including:

a first amount being about 30 weight % to about 65 weight % of the plurality of diamond grains, the first amount exhibiting a first average grain size of about 8 μm to about 22 μm;

a second amount being about 18 weight % to about 65 weight % of the plurality of diamond grains, the second amount exhibiting a second average grain size that is greater than the first average grain size and is about 15 μm to about 50 μm; and

a third amount being greater than 0 weight % to about 40 weight % of the plurality of diamond grains that exhibits a third average grain size of about 15 μm and 22 μm that is greater than the first average grain size and less than the second average grain size.

13. The rotary drill bit of claim 12 , wherein the first amount is about 58 weight % to about 62 weight % and the second amount is about 38 weight % to about 42 weight %.

14. The rotary drill bit of claim 12 , wherein the polycrystalline diamond table includes one or more of boron, niobium, molybdenum, tantalum, tungsten, rhenium, hafnium, or alloys thereof in a range from greater than 0 weight % to about 5 weight % of the polycrystalline diamond table.

15. The rotary drill bit of claim 12 , wherein the polycrystalline diamond table includes boron in a range from greater than 0 weight % to about 0.2 weight % of the polycrystalline diamond table.

16. The rotary drill bit of claim 12 , wherein the polycrystalline diamond table is integrally formed with the substrate.

17. The rotary drill bit of claim 12 , wherein the polycrystalline diamond table includes at least one exterior surface and a leached region extending inwardly from the at least one exterior surface to a depth of at least 250 μm.

18. The rotary drill bit of claim 12 , wherein the polycrystalline diamond table includes at least one exterior surface and a leached region extending inwardly from the at least one exterior surface to a depth of about 400 μm to about 600 μm.

19. The rotary drill bit of claim 12 , wherein the polycrystalline diamond table includes at least one exterior surface and a leached region extending inwardly from the at least one exterior surface to a depth of about 600 μm to about 800 μm.

20. The rotary drill bit of claim 12 , wherein the at least one cutting element exhibits a G ratio of about 2.5×10 7 to about 3.5×10 7 .

Assignments (5)
SECURITY INTEREST Recorded Jul 18, 2025
From: US SYNTHETIC CORPORATION
To: KEYBANK NATIONAL ASSOCIATION
Reel/Frame 074973/0089 →
RELEASE OF SECURITY INTEREST IN PATENTS Recorded Jul 17, 2025
From: JPMORGAN CHASE BANK, N.A.
To: CHAMPIONX LLC; APERGY ESP SYSTEMS, LLC; APERGY BMCS ACQUISITION CORP; HARBISON-FISCHER, INC.; NORRIS RODS, INC.,; NORRIS RODS, INC.,; NORRISEAL-WELLMARK, INC.; PCS FERGUSON, INC.; QUARTZDYNE, INC.; US SYNTHETIC CORPORATION
Reel/Frame 072004/0019 →
RELEASE OF SECURITY INTEREST Recorded Jun 7, 2022
From: BANK OF AMERICA, N.A.
To: ACE DOWNHOLE, LLC; HARBISON-FISCHER, INC.; NORRIS RODS, INC.; PCS FERGUSON, INC.; QUARTZDYNE, INC.; SPIRIT GLOBAL ENERGY SOLUTIONS, INC.; THETA OILFIELD SERVICES, INC.; APERGY BMCS ACQUISITION CORP.; NORRISEAL-WELLMARK, INC.; US SYNTHETIC CORPORATION; WINDROCK, INC.
Reel/Frame 060305/0001 →
SECURITY INTEREST Recorded Jun 5, 2020
From: ACE DOWNHOLE, LLC; APERGY BMCS ACQUISITION CORP.; HARBISON-FISCHER, INC.; NORRIS RODS, INC.; NORRISEAL-WELLMARK, INC.; PCS FERGUSON, INC.; QUARTZDYNE, INC.; SPIRIT GLOBAL ENERGY SOLUTIONS, INC.; THETA OILFIELD SERVICES, INC.; US SYNTHETIC CORPORATION; WINDROCK, INC.
To: BANK OF AMERICA, N.A.
Reel/Frame 053790/0001 →
SECURITY AGREEMENT Recorded Nov 6, 2019
From: APERGY ESP SYSTEMS, LLC; APERGY BMCS ACQUISITION CORP.; PCS FERGUSON, INC.; QUARTZDYNE, INC.; THETA OILFIELD SERVICES, INC.; US SYNTHETIC CORPORATION; WINDROCK, INC.
To: JPMORGAN CHASE BANK, N.A.
Reel/Frame 050941/0695 →