IP Library Granted Patent US 11,318,338
Granted Patent B2
US 11,318,338 · App. 16/571,936 · Granted May 3, 2022

Azeotrope or azeotrope-like compositions of trifluoroidomethane (CF

Inventors: Christian Jungong (Depew, NY); Daniel C. Merkel (Orchard Park, NY); Haiyou Wang (Amherst, NY); Hang T. Pham (Amherst, NY); Ryan J. Hulse (Getzville, NY)
Assignee: Honeywell International Inc.
A62D1/0057B01D3/36C08J9/146C08J9/147C09K3/30C09K5/044C09K5/048H01B3/56C08J2203/144C08J2203/182C09K2205/122C09K2205/22C09K2205/32
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Quick Facts
Patent No.
US 11,318,338
App. No.
16/571,936
Granted
May 3, 2022
Kind
B2
Abstract

The present disclosure provides azeotrope or azeotrope-like compositions including trifluoroiodomethane (CF 3 I) and 1,1,1,3,3,3-hexafluoropropane (HFC-236fa), and a method of forming an azeotrope or azeotrope-like composition comprising the step of combining 1,1,1,3,3,3-hexafluoropropane (HFC-236fa) and trifluoroiodomethane (CF 3 I) to form an azeotrope or azeotrope-like comprising 1,1,1,3,3,3-hexafluoropropane (HFC-236fa) and trifluoroiodomethane (CF 3 I) having a boiling point of about −22.70° C.±0.30° C. at a pressure of about 14.30 psia±0.30 psia.

Claims (13)

1. A composition comprising an azeotrope composition consisting essentially of from 0.5 wt. % to 10 wt. % 1,1,1,3,3,3-hexafluoropropane (HFC-236fa) and from 90 wt. % to 99.5 wt. % trifluoroiodomethane (CF 3 I), wherein the azeotrope composition has a boiling point of about −22.70° C.±0.30° C. at a pressure of about 14.30 psia±0.30 psia.

2. The composition of claim 1 , wherein the azeotrope composition consists essentially of from 2 wt. % to 10 wt. % 1,1,1,3,3,3-hexafluoropropane (HFC-236fa) and from 90 wt. % to 98 wt. % trifluoroiodomethane (CF 3 I).

3. The composition of claim 1 , wherein the azeotrope composition consists essentially of from about 5 wt. % to about 6 wt. % 1,1,1,3,3,3-hexafluoropropane (HFC-236fa) and from about 94 wt. % to about 95 wt. % trifluoroiodomethane (CF 3 I).

4. The composition of claim 1 , wherein the azeotrope composition consist essentially of about 5.57 wt. % 1,1,1,3,3,3-hexafluoropropane (HFC-236fa) and about 94.43 wt. % trifluoroiodomethane (CF 3 I).

5. The composition of claim 1 , wherein the azeotrope composition consists of from 0.5 wt. % to 10 wt. % 1,1,1,3,3,3-hexafluoropropane (HFC-236fa) and from 90 wt. % to 99.5 wt. % trifluoroiodomethane (CF 3 I).

6. The composition of claim 1 , wherein the azeotrope composition consists of from 2 wt. % 10 wt. % 1,1,1,3,3,3-hexafluoropropane (HFC-236fa) and from 90 wt. % to 98 wt. % trifluoroiodomethane (CF 3 I).

7. The composition of claim 1 , wherein the azeotrope or azeotrope-like composition consists of about 5.57 wt. % 1,1,1,3,3,3-hexafluoropropane (HFC-236fa) and about 94.43 wt. % trifluoroiodomethane (CF 3 I).

8. A method of forming an azeotrope composition comprising the step of combining from 0.5 wt. % to 10 wt. % 1,1,1,3,3,3-hexafluoropropane (HFC-236fa) and from 90 wt. % to 99.5 wt. % trifluoroiodomethane (CF 3 I) to form an azeotrope composition consisting essentially of 1,1,1,3,3,3-hexafluoropropane (HFC-236fa) and trifluoroiodomethane (CF 3 I) having a boiling point of about −22.70° C.±0.30° C. at a pressure of about 14.30 psia±0.30 psia.

9. The composition of claim 8 , wherein the azeotrope composition consists of from 2 wt. % to 10 wt. % 1,1,1,3,3,3-hexafluoropropane (HFC-236fa) and from 90 wt. % to 98 wt. % trifluoroiodomethane (CF 3 I).

10. The method of claim 8 , wherein the combining step comprises combining about 5.57 wt. % 1,1,1,3,3,3-hexafluoropropane (HFC-236fa) and about 94.43 wt. % trifluoroiodomethane (CF 3 I).

11. A method of separating 1,1,1,3,3,3-hexafluoropropane (HFC-236fa) and trifluoroiodomethane (CF 3 I) from a primary composition comprising 1,1,1,3,3,3-hexafluoropropane (HFC-236fa), trifluoroiodomethane (CF 3 I) and at least one impurity, including the steps of:

forming, within the primary composition, a secondary composition which is an azeotrope composition consisting essentially of from 0.5 wt. % to 10 wt. % 1,1,1,3,3,3-hexafluoropropane (HFC-236fa) and from 90 wt. % to 99.5 wt. % trifluoroiodomethane (CF 3 I) having a boiling point of about −22.70° C.±0.30° C. at a pressure of about 14.30 psia±0.30 psia; and

separating the secondary composition from the primary composition and the at least one impurity.

Assignments (3)
NUNC PRO TUNC ASSIGNMENT Recorded Apr 12, 2026
From: HONEYWELL INTERNATIONAL INC.
To: SOLSTICE ADVANCED MATERIALS US, INC.
Reel/Frame 074344/0212 →
SECURITY INTEREST Recorded Jan 12, 2026
From: SOLSTICE ADVANCED MATERIALS US, INC.
To: JPMORGAN CHASE BANK, N.A., AS ADMINISTRATIVE AGENT
Reel/Frame 074569/0260 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Nov 27, 2019
From: JUNGONG, CHRISTIAN; MERKEL, DANIEL C.; WANG, HAIYOU; PHAM, HANG T.; HULSE, RYAN J.
To: HONEYWELL INTERNATIONAL INC.
Reel/Frame 051134/0246 →
Continuity (2)
Provisional Application 62745670 · Oct 15, 2018
Related Publication 20200114188A1 · Apr 16, 2020