IP Library Granted Patent US 11,272,722
Granted Patent B2
US 11,272,722 · App. 16/600,656 · Granted Mar 15, 2022

High pressure processing indicator

Inventor: Alexander Craig Bushman (Loveland, OH)
Assignee: Multi-Color Corporation
A23L3/001A23L3/003A23L3/0155B65D79/008B65D79/02C09B67/0097C09D11/037C09D11/101C09J133/00G01L7/187A23V2002/00B65D2203/12G01L13/028G01N31/22
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Quick Facts
Patent No.
US 11,272,722
App. No.
16/600,656
Granted
Mar 15, 2022
Kind
B2
Abstract

A device for indicating exposure to a pressure. The device may include a base layer, a plurality of microcapsules, and a coating, with the microcapsules being disposed between the base layer and the coating. The microcapsules contain a indicator material that can be released once the microcapsules burst. The microcapsules then have a compressive bursting strength that is chosen or designed to be less than a selected pressure (e.g., the pressure being that to which a particular article may be exposed during high pressure processing). Thus, when the device is subjected to a pressure greater than the compressive bursting strength, at least some microcapsules burst, the indicator material is released from the microcapsules, and the release of the indicator material can be detected by observation of the device. The device may be a label that is associated (such as by being affixed) to the article being subjected to pressure (or multiple labels being associated (such as by being affixed) to multiple articles. Alternatively, the device may be associated with an article or articles without being affixed thereto.

Claims (22)

1. A label for indicating exposure to a pressure, the label comprising:

a base layer, a plurality of microcapsules, and a top layer, the microcapsules being disposed between the base layer and the top layer, the microcapsules containing a indicator material and having a compressive bursting strength less than a selected pressure; and

an adhesive layer disposed adjacent to the base layer such that the base layer is positioned between the adhesive layer and the plurality of microcapsules;

wherein the indicator material includes a UV curable ink;

whereby when the label is subjected to a pressure greater than the compressive bursting strength, at least some microcapsules burst, the indicator material is released from the microcapsules, and the release of the indicator material is detected by observation of the label.

2. The label of claim 1 , wherein at least one of the base layer and the top layer is formed from a material that permits detection of indicator material released from the microcapsules by observation of the label.

3. The label of claim 1 , wherein the base layer includes a material chosen from a film and paper.

4. The label of claim 3 , wherein the base layer includes a film chosen from polypropylene, biaxially-oriented polypropylene, and polyester.

5. The label of claim 4 , wherein the ink can change from a colored ink to a colorless or clear ink when exposed to a temperature equal to or greater than a temperature chosen from 104° F., 120° F., and 150° F.

6. The label of claim 1 , wherein the top layer is chosen from a film and a varnish.

7. The label of claim 6 , wherein the top layer is UV-curable.

8. The label of claim 6 , wherein the top layer is a film and includes polypropylene.

9. The label of claim 1 , wherein the compressive bursting strength is equal to or less than a selected pressure to which the label will be subjected.

10. The label of claim 1 , further comprising an ink layer.

11. The label of claim 10 , wherein the ink layer is disposed between the plurality of microcapsules and the base layer.

12. The label of claim 11 , wherein the adhesive layer includes at least one adhesive that is an acrylic adhesive.

13. The label of claim 1 , wherein the label is a pressure sensitive label, a shrink sleeve label, or an in-mold label.

14. A label for indicating exposure to a pressure, the label comprising:

a base layer, a plurality of microcapsules, and a top layer, the microcapsules being disposed between the base layer and the top layer, the microcapsules containing a indicator material and having a compressive bursting strength less than a selected pressure; and

an adhesive layer disposed adjacent to the base layer such that the base layer is positioned between the adhesive layer and the plurality of microcapsules;

wherein the top layer is chosen from a film and a varnish, and wherein the top layer is UV-curable;

whereby when the label is subjected to a pressure greater than the compressive bursting strength, at least some microcapsules burst, the indicator material is released from the microcapsules, and the release of the indicator material is can be detected by observation of the label.

Assignments (9)
NOTICE AND CONFIRMATION OF GRANT OF SECURITY INTEREST IN PATENTS Recorded May 19, 2026
From: MCC-NORWOOD, LLC; MULTI-COLOR CORPORATION; W/S PACKAGING GROUP, LLC; MCC MANUFACTURING, INC.
To: WILMINGTON TRUST, NATIONAL ASSOCIATION, AS NOTES COLLATERAL AGENT
Reel/Frame 075623/0138 →
RELEASE OF SECURITY INTEREST AT 57973/0614 Recorded May 12, 2026
From: BARCLAYS BANK PLC, AS AGENT
To: MCC-NORWOOD, LLC; MULTI-COLOR CORPORATION; W/S PACKAGING GROUP, LLC (F/K/A W/S PACKAGING GROUP, INC.)
Reel/Frame 075630/0609 →
RELEASE OF SECURITY INTEREST Recorded Oct 17, 2024
From: WILMINGTON TRUST, NATIONAL ASSOCIATION
To: HAMMER PACKAGING CORP.; MCC-NORWOOD LLC; W/S PACKAGING GROUP, INC; MULTI-COLOR CORPORATION
Reel/Frame 069180/0836 →
CASH FLOW SECURITY AGREEMENT Recorded Oct 29, 2021
From: MULTI-COLOR CORPORATION; MCC-NORWOOD, LLC; W/S PACKAGING GROUP, INC.
To: BARCLAYS BANK PLC
Reel/Frame 057973/0625 →
NOTES SECURITY AGREEMENT Recorded Oct 29, 2021
From: MULTI-COLOR CORPORATION; MCC-NORWOOD, LLC; W/S PACKAGING GROUP, INC.
To: WILMINGTON TRUST, NATIONAL ASSOCIATION
Reel/Frame 057973/0739 →
RELEASE OF SECURITY INTEREST Recorded Oct 29, 2021
From: BANK OF AMERICA, N.A.
To: MULTI-COLOR CORPORATION; MCC-NORWOOD, LLC; W/S PACKAGING GROUP, INC.
Reel/Frame 057974/0801 →
ABL SECURITY AGREEMENT Recorded Oct 29, 2021
From: MULTI-COLOR CORPORATION; MCC-NORWOOD, LLC; W/S PACKAGING GROUP, INC.
To: BARCLAYS BANK PLC
Reel/Frame 057973/0614 →
TERM LOAN SECURITY AGREEMENT Recorded Sep 30, 2021
From: W/S PACKAGING GROUP, INC.; MULTI-COLOR CORPORATION; MCC-NORWOOD, LLC
To: BANK OF AMERICA, N.A.
Reel/Frame 057678/0580 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Oct 14, 2019
From: BUSHMAN, ALEXANDER CRAIG
To: MULTI-COLOR CORPORATION
Reel/Frame 050702/0815 →