Method of making a tobacco extract
Embodiments described herein include a method of making a tobacco extract comprising; (a) providing tobacco and an entrapment solvent in a partitioned vessel, wherein the tobacco and entrapment solvent are separated by the partition, and the vessel is configured such that the tobacco and entrapment solvent cannot contact each other; (b) flowing a supercritical extraction solvent through the vessel, wherein the extraction solvent and any dissolved substances can pass through the partition; whereby tobacco components are extracted from the tobacco into the extraction solvent and carried across the partition, wherein the extraction solvent contacts the entrapment solvent and tobacco components are transferred from the supercritical extraction solvent into the entrapment solvent.
1. A method of making a tobacco extract, the method comprising:
(a) providing tobacco and an entrapment solvent in a partitioned vessel, wherein the tobacco and entrapment solvent are separated by a partition, and the vessel is configured such that the tobacco and entrapment solvent cannot contact each other;
(b) flowing a supercritical extraction solvent into the vessel, wherein the extraction solvent and any dissolved substances can pass through the partition; whereby tobacco components are extracted from the tobacco into the extraction solvent and carried across the partition, wherein the extraction solvent contacts the entrapment solvent and the tobacco components are transferred from the extraction solvent into the entrapment solvent,
wherein the method further comprises the step of providing the entrapment solvent containing dissolved tobacco components in a cartridge, wherein the cartridge is configured for use in a smoking article.
2. The method of claim 1 , wherein the partition is selected from the group consisting of: a bubble cap tray, a sieve plate, a valve plate, a sinter plate, and a very fine mesh.
3. The method of claim 1 , further comprising:
(c) altering the conditions in the vessel so that the extraction solvent is subcritical, thereby separating the extraction solvent and any remaining dissolved tobacco components, at least some of which are subsequently dissolved in the entrapment solvent.
4. The method according to claim 1 , wherein the extraction solvent comprises carbon dioxide.
5. The method according to claim 4 wherein, during (a) and (b), the temperature is in the range of about 308-473K, and the pressure is in the range of about 8-85 MPa.
6. The method according to claim 1 , wherein the entrapment solvent comprises an aerosol generating agent.
7. The method according to claim 6 , wherein the entrapment solvent comprises a polyol.
8. The method according to claim 1 , wherein the tobacco components include one or more of nicotine and tobacco aromas and flavors.
9. The method according to claim 1 , wherein the entrapment solvent is provided in an upper portion of the vessel, above the tobacco in a lower portion, and the partition is selected from the group consisting of a bubble cap tray, a sieve plate, and a valve plate.
10. The method according to claim 1 , wherein the entrapment solvent is provided in a lower portion of the vessel, below the tobacco in an upper portion, and the partition is selected from the group consisting of a sinter plate and a very fine mesh.
11. The method according to claim 1 , wherein the method comprises an initial step of adding water to the tobacco.
12. The method of using the tobacco extract obtainable by the method according to claim 1 , comprising generating an inhalable aerosol from the tobacco extract.
13. The method of using the tobacco extract according to claim 12 , wherein the tobacco extract is used in a smoking article.
14. The method according to claim 11 , wherein the amount of water added to the tobacco is from about 2% to 20% based on the dry weight of the tobacco.
15. The method according to claim 11 , wherein the tobacco has a particle size range of from 355 μm to 3.5 mm.
16. The method according to claim 15 , wherein the tobacco is ground Virginia tobacco leaf.