IP Library Granted Patent US 11,508,519
Granted Patent B2
US 11,508,519 · App. 16/620,712 · Granted Nov 22, 2022

Continous heat treatment device and method for alloy workpiece or metal workpiece

Inventors: Qingjiang Wang (Fujian Province, CN); Ying Luo (Fujian Province, CN); Jianpeng Wu (Fujian Province, CN)
Assignee: Fujian Changting Golden Dragon Rare-Earth Co., Ltd
H01F41/0253B22F3/24C21D1/613C21D1/773C21D9/0056C21D9/0062C21D9/0068F27B5/02F27B5/04F27B5/18F27B9/028F27D9/00H01F1/0577H01L21/67098H01L21/67173H01L21/67184B22F2003/248B22F2201/10C21D2201/00F27B2005/062F27D2009/0072
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Quick Facts
Patent No.
US 11,508,519
App. No.
16/620,712
Granted
Nov 22, 2022
Kind
B2
Abstract

Disclosed are a continuous heat treatment device and method for a sintered Nd—Fe—B magnet workpiece. The device comprises a first heat treatment chamber, a first cooling chamber, a second heat treatment chamber, and a second cooling chamber continuously disposed in sequence, as well as a transfer system disposed among the chambers to transfer the alloy workpiece or the metal workpiece; both the first cooling chamber and the second cooling chamber adopt a air cooling system, wherein a cooling air temperature of the first cooling chamber is 25° C. or above and differs from a heat treatment temperature of the first heat treatment chamber by at least 450° C.; a cooling air temperature of the second cooling chamber is 25° C. or above and differs from a heat treatment temperature of the second heat treatment chamber by at least 300° C. The continuous heat treatment device and method can improve the cooling rate and production efficiency and improve the properties and consistency of the products.

Claims (45)

1. A continuous heat treatment method for an alloy workpiece or a metal workpiece, comprising:

a first-stage heat treatment performed in a first heat treatment chamber, wherein the first heat treatment chamber is presented as a square structure and comprises two heating regions disposed facing each other on an inner wall of the square structure of the first heat treatment chamber, and the first-stage heat treatment comprises directly placing the alloy workpiece or the metal workpiece on a first material rack at a center of the square structure of the first heat treatment chamber, or first placing the alloy workpiece or the metal workpiece within a first cartridge and then placing the first cartridge on the first material rack at the center of the square structure the first heat treatment chamber,

a first-stage air cooling treatment,

a second-stage heat treatment performed in a second heat treatment chamber, wherein the second heat treatment chamber is presented as a square structure and comprises two heating regions disposed facing each other on an inner wall of the square structure of the second heat treatment chamber, and the second-stage heat treatment comprises directly placing the alloy workpiece or the metal workpiece is on a second material rack at a center of the square structure of the second heat treatment chamber, or first placing the alloy workpiece or the metal workpiece within a second cartridge and then placing the second cartridge on the second material rack at the center of the square structure of the second heat treatment chamber, and

a second-stage air cooling treatment, wherein:

the first-stage heat treatment, the first-stage air cooling treatment, the second-stage heat treatment, and the second-stage air cooling treatment are performed in sequence in air-tight chambers;

a cooling air temperature of the first-stage air cooling treatment is 25° C. or above and lower than a heat treatment temperature of the first-stage heat treatment by at least 450° C.; and a cooling air temperature of the second-stage air cooling treatment is 25° C. or above and lower than a heat treatment temperature of the second-stage heat treatment by at least 300° C.

2. The continuous heat treatment method for an alloy workpiece or a metal workpiece according to claim 1 , wherein the alloy workpiece is a sintered Nd—Fe—B magnet.

3. The continuous heat treatment method for an alloy workpiece or a metal workpiece according to claim 2 , wherein in the second-stage heat treatment, a temperature difference of the alloy workpiece or the metal workpiece in different regions is below ±5° C.

4. The continuous heat treatment method for an alloy workpiece or a metal workpiece according to claim 1 , wherein:

in the first-stage air cooling treatment, an average cooling rate of the alloy workpiece or the metal workpiece in a first 10 minutes is 6° C./min-15° C./min; and

in the second-stage air cooling treatment, an average cooling rate of the alloy workpiece or the metal workpiece in a first 10 minutes is 6° C./min-15° C./min.

5. A continuous heat treatment device for an alloy workpiece or a metal workpiece, comprising:

a first heat treatment chamber,

a first cooling chamber,

a second heat treatment chamber,

a second cooling chamber, wherein the first heat treatment chamber, the first cooling chamber, the second heat treatment chamber, and the second cooling chamber are disposed in sequence by means of airtight devices, and

a transfer system disposed among the first heat treatment chamber, the first cooling chamber, the second heat treatment chamber, and the second cooling chamber to transfer the alloy workpiece or the metal workpiece, wherein:

both the first cooling chamber and the second cooling chamber adopt an air cooling system;

a cooling air temperature of the first cooling chamber is 25° C. or above and lower than a heat treatment temperature of the first heat treatment chamber by at least 450° C.;

a cooling air temperature of the second cooling chamber is 25° C. or above and lower than a heat treatment temperature of the second heat treatment chamber by at least 300° C.;

a pressure of the first cooling chamber and a pressure of the second cooling chamber are 50 kPa-100 kPa;

the first heat treatment chamber is presented as a square structure and comprises two heating regions disposed facing each other on an inner wall of the square structure of the first heat treatment chamber;

the alloy workpiece or the metal workpiece is placed directly on a first material rack at a center of the square structure of the first heat treatment chamber, or the alloy workpiece or the metal workpiece is first placed within a first cartridge and the first cartridge is then placed on the first material rack at the center of the square structure the first heat treatment chamber;

the second heat treatment chamber is presented as a square structure and comprises two heating regions disposed facing each other on an inner wall of the square structure of the second heat treatment chamber;

the alloy workpiece or the metal workpiece is placed directly on a second material rack at a center of the square structure of the second heat treatment chamber, or the alloy workpiece or the metal workpiece is first placed within a second cartridge and the second cartridge is then placed on the second material rack at the center of the square structure of; and the transfer system is used to transfer at least one of the first material rack or the second material rack between any two or more of the first heat treatment chamber, the first cooling chamber, the second heat treatment chamber, and the second cooling chamber.

6. The continuous heat treatment device for an alloy workpiece or a metal workpiece according to claim 5 , wherein the alloy workpiece is a sintered Nd—Fe—B magnet.

7. The continuous heat treatment device for an alloy workpiece or a metal workpiece according to claim 5 , wherein the air cooling system is an air cooling system adopting an inert gas.

8. The continuous heat treatment device for an alloy workpiece or a metal workpiece according to claim 7 , wherein:

the heat treatment temperature of the first heat treatment chamber is 800° C.-950° C.;

the cooling air temperature of the first cooling chamber is 25° C.-150° C.;

the heat treatment temperature of the second heat treatment chamber is 400° C.-650° C.;

the cooling air temperature of the second cooling chamber is 25° C.-100° C.;

in a first-stage air cooling treatment performed in the first cooling chamber, an average cooling rate of the alloy workpiece or the metal workpiece in a first 10 minutes of the first-stage air cooling treatment is 6° C./min-15° C./min; and

in a second-stage air cooling treatment performed in the second cooling chamber, an average cooling rate of the alloy workpiece or the metal workpiece in a first 10 minutes of the second-stage air cooling treatment is 6° C./min-15° C./min.

9. The continuous heat treatment device for an alloy workpiece or a metal workpiece according to claim 5 , wherein:

an area of the two heating regions of the first heat treatment chamber exceeds a longitudinal-sectional area of the first material rack; and

an area of the two heating regions of the second heat treatment chamber exceeds a longitudinal-sectional area of the second material rack.

10. The continuous heat treatment device for an alloy workpiece or a metal workpiece according to claim 5 , wherein:

in the first heat treatment chamber, distances from the first cartridge, the alloy workpiece, or the metal workpiece to the two heating regions of the first heat treatment chamber disposed facing each other are the same, ranging from 5 cm to 20 cm; and

in the second heat treatment chamber, distances from the second cartridge, the alloy workpiece, or the metal workpiece to the two heating regions of the second heat treatment chamber disposed facing each other are the same, ranging from 5 cm to 20 cm, and a temperature difference of the alloy workpiece or the metal workpiece in different regions is below ±5° C.

11. The continuous heat treatment device for an alloy workpiece or a metal workpiece according to claim 10 , wherein:

wherein the alloy workpiece is a sintered Nd—Fe—B magnet; and

the sintered Nd—Fe—B magnet is a Nd—Fe—B magnet having a total rare earth (TRE) of 28.8 wt %-30.5 wt %.

12. The continuous heat treatment device for an alloy workpiece or a metal workpiece according to claim 5 , wherein the first material rack and the second material rack are a same material rack.

Assignments (2)
CHANGE OF NAME Recorded Dec 20, 2023
From: FUJIAN CHANGTING GOLDEN DRAGON RARE-EARTH CO., LTD.
To: FUJIAN GOLDEN DRAGON RARE-EARTH CO., LTD.
Reel/Frame 066124/0473 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Dec 9, 2019
From: WANG, QINGJIANG; LUO, YING; WU, JIANPENG
To: FUJIAN CHANGTING GOLDEN DRAGON RARE-EARTH CO., LTD.
Reel/Frame 051218/0949 →
Priority Claims (2)
CN 201810100874.2 · Feb 1, 2018 · national
CN 201810307941.8 · Apr 8, 2018 · national
Continuity (1)
Related Publication 20210142943A1 · May 13, 2021