IP Library Granted Patent US 11,131,616
Granted Patent B2
US 11,131,616 · App. 16/629,063 · Granted Sep 28, 2021

Analyzing fluids

Inventors: Chady Stephan (Brampton, CA); David Hilligoss (Venice, FL)
Assignee: PerkinElmer Health Sciences Canada, Inc.
G01N15/14G01N21/73G01N33/2858G01N2015/1486
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Quick Facts
Patent No.
US 11,131,616
App. No.
16/629,063
Granted
Sep 28, 2021
Kind
B2
Abstract

A system and method of using the system for analyzing liquid samples obtain from viscous sources. The system includes a sample delivery system, a particle counter configured to receive a liquid sample from the liquid sample delivery system, a composition analyzer configured to receive the liquid sample from the particle counter, a feed system configured to draw the liquid sample through the particle counter and subsequently inject the liquid sample into the composition analyzer; and a processor to process and analyze data from the particle counter and composition analyzer.

Claims (31)

1. A system for analyzing a liquid sample, the system comprising:

a liquid sample delivery system;

a particle counter configured to receive a liquid sample from the liquid sample delivery system;

a composition analyzer configured to receive the liquid sample from the particle counter;

a feed system configured to draw the liquid sample through the particle counter and subsequently inject the liquid sample into the composition analyzer; and

a processor to process and analyze data from the particle counter and composition analyzer.

2. The system of claim 1 wherein the feed system comprises a syringe and the liquid sample is pulled through the particle counter via the syringe.

3. The system of claim 1 wherein the feed system is configured to inject the liquid sample and a carrier into the composition analyzer.

4. The system of claim 3 wherein the feed system further comprises a pump and a carrier source, wherein the pump is configured to combine the liquid sample with a carrier prior to injecting into the composition analyzer.

5. The system of claim 4 wherein the pump is a peristaltic pump.

6. The system of claim 1 wherein the composition analyzer is an inductively coupled plasma optical emission spectrometry device (ICP-OES).

7. The system of claim 6 wherein the liquid sample is injected into a nebulizer of the ICP-OES.

8. The system of claim 1 further comprising a liquid sample preparation device configured to dilute a viscous source sample to form the liquid sample.

9. The system of claim 8 wherein the liquid sample preparation device dilutes the viscous source sample to a sample:liquid ratio of 1:1 to 1:20.

10. A method for analyzing a liquid sample, the method comprising:

supplying the liquid sample containing particles to a particle counter;

pulling the liquid sample through the particle counter via a feed system;

analyzing the particles of the liquid sample for at least one of number and size;

pulling the liquid sample into a sample loop after analyzing the particles;

injecting the liquid sample from the sample loop into a composition analyzer;

analyzing the liquid sample for its composition; and

processing data from the particle counter and the composition analyzer;

wherein a time period from feeding the liquid sample containing particles into the particle counter through analyzing the liquid sample in the composition analyzer is less than 45 seconds.

11. The method of claim 10 wherein the feed system includes a syringe, the method further comprising pulling the liquid sample through the particle counter via the syringe.

12. The method of claim 10 further comprising injecting the liquid sample and a carrier into the composition analyzer.

13. The method of claim 12 further comprising combining the liquid sample with a carrier prior to injecting the liquid sample into the composition analyzer.

14. The method of claim 13 wherein the feed system further comprises a peristaltic pump, wherein the carrier is pumped via the peristaltic pump into the composition analyzer.

15. The method of claim 10 wherein the composition analyzer is ICP-OES.

16. The method of claim 15 further comprising injecting the liquid sample into a nebulizer of the ICP-OES.

17. The method of claim 10 further comprising diluting a viscous source sample at a ratio of sample:liquid of 1:1 to 1:20 to form the liquid sample.

18. The method of claim 10 further comprising diluting a viscous source sample at a ratio of sample:liquid of 1:5 to 1:15 to form the liquid sample.

Assignments (2)
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Mar 27, 2023
From: PERKINELMER HEALTH SCIENCES CANADA, INC.
To: PERKINELMER SCIENTIFIC CANADA ULC
Reel/Frame 063166/0074 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Jan 28, 2020
From: STEPHAN, CHADY; HILLIGOSS, DAVID
To: PERKINELMER HEALTH SCIENCES CANADA, INC.
Reel/Frame 051642/0263 →