IP Library Granted Patent US 11,225,571
Granted Patent B2
US 11,225,571 · App. 16/633,362 · Granted Jan 18, 2022

Styrene copolymer composition with improved residual gloss

Inventors: Tobias Schulz (Cologne, DE); Norbert Niessner (Friedelsheim, DE); Eike Jahnke (Aubonne, CH); Hans-Werner Schmidt (Bayreuth, DE); Tristan Kolb (Bayreuth, DE)
Assignee: INEOS STYROLUTION GROUP GMBH
C08L25/14C08K3/32C08L23/0838C08L25/12C08L25/16C08L91/06C08K3/013C08K2003/324C08K2003/325C08L2203/20C08L2205/03
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Quick Facts
Patent No.
US 11,225,571
App. No.
16/633,362
Granted
Jan 18, 2022
Kind
B2
Abstract

Thermoplastic polymer compositions (P) comprising 90 to 99.9 wt.-% of at least one styrene-based copolymer, 0.1 to 10 wt.-% of at least one copolymer at least comprising repeating units derived from at least one α-olefin monomer and at least one vinyl-aromatic monomer, at least one inorganic phosphate compound, at least one polyolefin wax and optionally at least one colorant, dye or pigment, and/or at least one further additive show improved properties with respect to residual gloss after abrasion combined with improved melt flow characteristics while heat resistance is not affected.

Claims (39)

1. A thermoplastic polymer composition (P) comprising:

(A) 90 to 99.9 wt.-%, based on the total weight of the thermoplastic polymer composition (P), of at least one styrene-based copolymer;

(B) 0.1 to 10 wt.-%, based on the total weight of the thermoplastic polymer composition (P), of at least one copolymer composition comprising:

(B-1) 75 to 98 wt.-%, based on the total weight of the copolymer composition (B), of at least one copolymer at least comprising repeating units derived from at least one α-olefin monomer and at least one vinyl-aromatic monomer;

(B-2) 1 to 25 wt.-%, based on the total weight of the copolymer composition (B), of at least one inorganic phosphate compound; and

(B-3) 1 to 22 wt.-%, based on the total weight of the copolymer composition (B), of at least one polyolefin wax;

(C) 0 to 9.9 wt.-%, based on the total weight of the thermoplastic polymer composition (P), of at least one colorant, dye, or pigment; and

(D) 0 to 3 wt.-%, based on the total weight of the thermoplastic polymer composition (P), of at least one further additive.

2. The thermoplastic polymer composition (P) according to claim 1 comprising:

(A) 95 to 99.5 wt.-%, based on the total weight of the thermoplastic polymer composition (P), of at least one styrene-based copolymer;

(B) 0.5 to 5 wt.-%, based on the total weight of the thermoplastic polymer composition (P), of at least one copolymer composition comprising:

(B-1) 75 to 96 wt.-%, based on the total weight of the copolymer composition (B), of at least one copolymer at least comprising repeating units derived from at least one α-olefin monomer and at least one vinyl-aromatic monomer;

(B-2) 3 to 10 wt.-%, based on the total weight of the copolymer composition (B), of at least one inorganic phosphate compound; and

(B-3) 1 to 22 wt.-%, based on the total weight of the copolymer composition (B), of at least one polyolefin wax;

(C) 0 to 4.5 wt.-%, based on the total weight of the thermoplastic polymer composition (P), of at least one colorant, dye, or pigment; and

(D) 0 to 3 wt.-%, based on the total weight of the thermoplastic polymer composition (P), of at least one further additive.

3. The thermoplastic polymer composition (P) according to claim 1 , wherein the at least one inorganic phosphate compound (B-2) comprises at least one alkaline phosphate compound, earth alkaline phosphate compound, or mixtures thereof.

4. The thermoplastic polymer composition (P) according to claim 1 , wherein the thermoplastic polymer composition (P) has a gloss reduction of less than 5% after grid cut test according to norm PV3952.

5. The thermoplastic polymer composition (P) according to claim 1 , wherein the thermoplastic polymer composition (P) has a melt flow rate (MVR, 220/10), which is increased (improved) by a factor of at least 4, whereas VST B50 shows a reduction of less than 5° C.

6. A process for the preparation of the thermoplastic polymer composition (P) according to claim 1 , wherein the process comprises at least the following steps:

a) providing the components (A) and (B), and, when present, (C) and/or (D), in the predetermined amounts to an optionally heatable mixing device; and

b) blending the components (A) and (B), and, when present, (C) and/or (D), in the optionally heatable mixing device at temperatures above the glass transition temperature of the components (A) and (B), and, when present, (C) and/or (D), to obtain the thermoplastic polymer composition (P);

or wherein the process comprises at least the following steps:

a) providing the components (A), (B-1), and (B-2), and, when present, (B-3), (C), and/or (D), in the predetermined amounts to an optionally heatable mixing device; and

b) blending the components (A), (B-1), and (B-2), and, when present, (B-3), (C), and/or (D), in the optionally heatable mixing device at temperatures above the glass transition temperature of the components A), (B-1), and (B-2), and, when present, (B-3), (C), and/or (D), to obtain the thermoplastic polymer composition (P).

7. A molded article, prepared from the thermoplastic polymer composition (P) according to claim 1 .

8. A method of making components or articles for electronic devices, household goods, and automotive parts, comprising the thermoplastic polymer composition (P) according to claim 1 .

9. The thermoplastic polymer composition (P) according to claim 1 , wherein the copolymer composition (B) comprises as constituent (B-1) 77 to 92 wt.-%, based on the total weight of the copolymer composition (B), of at least one copolymer at least comprising repeating units derived from at least one a-olefin monomer and at least one vinyl-aromatic monomer.

10. The thermoplastic polymer composition (P) according to claim 1 , wherein copolymer composition (B) comprises as constituent (B-2) 3 to 10 wt.-%, based on the total weight of the copolymer composition (B), of at least one inorganic phosphate compound.

11. The thermoplastic polymer composition (P) according to claim 1 , wherein copolymer composition (B) comprises as constituent (B-3) 5 to 20 wt.-%, based on the total weight of the copolymer composition (B), of at least one polyolefin wax.

12. The thermoplastic polymer composition (P) according to claim 1 wherein the thermoplastic polymer composition (P) has a residual gloss of ≥25% after abrasion was effected according to norm PV3975 compared to the surface of the non-abraded thermoplastic polymer composition (P).

13. The thermoplastic polymer composition (P) according to claim 1 , wherein the thermoplastic polymer composition (P) has a residual gloss of ≥30% after abrasion was effected according to norm PV3975 compared to the surface of the non-abraded thermoplastic polymer composition (P).

14. The thermoplastic polymer composition (P) according to claim 4 , wherein the thermoplastic polymer composition (P) has a gloss reduction of less than 3% after grid cut test according to norm PV3952.

15. The thermoplastic polymer composition (P) according to claim 4 , wherein the thermoplastic polymer composition (P) has a gloss reduction of less than 1% after grid cut test according to norm PV3952.

16. The thermoplastic polymer composition (P) according to claim 5 , wherein the thermoplastic polymer composition (P) has a melt flow rate (MVR, 220/10), which is increased (improved) by a factor of at least 6.

17. The thermoplastic polymer composition (P) according to claim 5 , wherein VST B50 shows a reduction of less 3° C.

18. The thermoplastic polymer composition (P) according to claim 5 , wherein VST B50 shows a reduction of less 1° C.

19. A method of making components or articles for electronic devices, household goods, and automotive parts, comprising the molded article according to claim 7 .

20. The molded article according to claim 7 , wherein the molded article is a component or article for electronic devices, household goods, and automotive parts.

Assignments (2)
FIRST LIEN INTELLECTUAL PROPERTY SECURITY AGREEMENT Recorded Apr 30, 2021
From: INEOS STYROLUTION GROUP GMBH
To: HSBC CORPORATE TRUSTEE COMPANY (UK) LIMITED
Reel/Frame 056103/0236 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Apr 14, 2021
From: SCHULZ, TOBIAS; NIESSNER, NORBERT; JAHNKE, EIKE; SCHMIDT, HANS-WERNER; KOLB, TRISTAN
To: INEOS STYROLUTION GROUP GMBH
Reel/Frame 055913/0733 →
Continuity (1)
Related Publication 20210155787A1 · May 27, 2021