IP Library Granted Patent US 11,235,276
Granted Patent B2
US 11,235,276 · App. 16/635,065 · Granted Feb 1, 2022

Process for removal of aerosol droplets

Inventors: Per Aggerholm Sørensen (Kgs. Lyngby, DK); Morten Thellefsen (Hillerød, DK)
Assignee: HALDOR TOPSØE A/S
B01D50/002B01D45/08B01D46/003B01D53/002
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Quick Facts
Patent No.
US 11,235,276
App. No.
16/635,065
Granted
Feb 1, 2022
Kind
B2
Abstract

The present disclosure relates to a process for removal of an aerosol, comprising the steps of directing a process gas comprising an aerosol to contact an inertial demister providing a first demisted process gas, and directing the first demisted process gas to contact a coalescing demister providing a second demisted process gas, characterized in said first inertial demister being more open than said coalescing demister, where more open is defined as having a higher void fraction or a lower density with the associated benefit of such a process providing an efficient removal of a large volume of liquid from the inertial demister, while avoiding flooding of the demister system. It further relates to a process plant for sulfuric acid production employing such a pair of demisters.

Claims (17)

1. A process for removal of an aerosol from a demister system and avoiding flooding of the demister system, comprising:

a. cooling a process gas comprising at least 5,000 ppm wt of a condensable species under condensing conditions to provide a process gas comprising an aerosol,

b. directing said process gas comprising an aerosol to contact an inertial demister providing a first demisted process gas, and

c. directing the first demisted process gas to contact a coalescing demister providing a second demisted process gas, wherein

d. said first inertial demister being more open than said coalescing demister, where more open is defined as having a higher void fraction or a lower density

e. and the process gas entering the demister having an aerosol content being more than 5,000 ppm wt.

2. The process according to claim 1 , wherein said inertial demister has a void fraction of more than 0.90 and a void fraction of less than 0.99.

3. The process according to claim 1 , wherein said coalescing demister has a void fraction of more than 0.60 and a void fraction of less than 0.90.

4. The process according to claim 1 , wherein said inertial demister has a density of more than 30 kg/m 3 and a density of less than 100 kg/m 3 .

5. The process according to claim 1 , wherein said coalescing demister has a density of more than 170 kg/m 3 and a density of less than 300 kg/m 3 .

6. The process according to claim 1 , wherein the inertial demister and coalescing demister both have a dimension in the direction of gas flow, wherein the ratio between the dimension in the direction of gas flow of the inertial demister and the dimension in the direction of gas flow of the coalescing demister is more than 0.5 and less than 10.0.

7. The process according to claim 1 , wherein the gas entering the inertial demister has a superficial velocity more than 1.0 m/s and less than 7.0 m/s.

8. The process according to claim 1 , wherein the difference of the temperature of the process gas entering the demister and the process gas exiting the demister is less than 5° C.

9. The process according to claim 1 , wherein the process gas comprises a sulfuric acid aerosol with a concentration of sulfuric acid in the aerosol droplets at the contact with the inertial demister is above 50 wt % and below 99 wt %.

10. The process according to claim 9 , wherein at least one demister is made from an inorganic material or a polymeric material.

11. The process according to claim 9 , wherein the demister is positioned in a heat and acid resistant vertical tube, in which the process gas flows inside the tube and a cooling medium flow outside the tube.

12. The process according to claim 9 , wherein the temperature of the process gas entering said inertial demister is above 60° C. and below 120° C.

Assignments (2)
CHANGE OF NAME Recorded Oct 30, 2023
From: HALDOR TOPSØE A/S
To: TOPSOE A/S
Reel/Frame 065565/0685 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Mar 10, 2020
From: THELLEFSEN, MORTEN; SØRENSEN, PER AGGERHOLM
To: HALDOR TOPSØE A/S
Reel/Frame 052062/0723 →
Priority Claims (1)
DK PA 2017 00438 · Aug 8, 2017 · national
Continuity (1)
Related Publication 20200246743A1 · Aug 6, 2020