IP Library Granted Patent US 11,718,895
Granted Patent B2
US 11,718,895 · App. 16/635,964 · Granted Aug 8, 2023

Method for dissolving lithium compound, method for manufacturing lithium carbonate, and method for recovering lithium from lithium ion secondary cell scrap

Inventors: Hirotaka Ariyoshi (Hitachi, JP); Isao Tomita (Hitachi, JP); Hiroshi Abe (Hitachi, JP)
Assignee: JX NIPPON MINING & METALS CORPORATION
C22B26/12B09B3/80C01D15/08C22B1/02C22B3/06C22B3/44H01M10/0525H01M10/54C01P2002/72C01P2006/40
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Quick Facts
Patent No.
US 11,718,895
App. No.
16/635,964
Granted
Aug 8, 2023
Kind
B2
Abstract

A method for dissolving a lithium compound according to the present invention includes bringing a lithium compound into contact with water or an acidic solution, and feeding, separately from the lithium compound, a carbonate ion to the water or the acidic solution to produce carbonic acid, and allowing the carbonic acid to react with the lithium compound to produce lithium hydrogen carbonate.

Claims (10)

1. A method for recovering lithium from lithium ion secondary cell scrap, the method comprising: a calcination step of calcining the lithium ion secondary cell scrap; and a lithium dissolving step of bringing cell powder obtained after the calcination step into contact with water or an acidic solution and feeding, separately from the cell powder, a carbonate ion to the water or the acidic solution to dissolve lithium in the cell powder,

wherein the cell powder contains cobalt and aluminum,

wherein a pH of a lithium dissolved solution obtained in the lithium dissolving step is from 7 to 10, and

wherein the cell powder comprises at least one selected from the group consisting of lithium hydroxide, lithium oxide and lithium carbonate.

2. The method for recovering lithium from lithium ion secondary cell scrap according to claim 1 , wherein in the lithium dissolving step, the carbonate ion is fed so as to maintain a saturated state of carbonic acid in the water or the acidic solution.

3. The method for recovering lithium from lithium ion secondary cell scrap according to claim 1 , wherein the feeding of the carbonate ion in the lithium dissolving step is carried out by blowing a carbon dioxide gas into the water or the acidic solution.

4. The method for recovering lithium from lithium ion secondary battery scrap according to claim 1 , further comprising a lithium precipitating step of separating lithium from the lithium dissolved solution obtained in the lithium dissolving step, and precipitating a lithium ion in the lithium dissolved solution as lithium carbonate.

5. The method for recovering lithium from lithium ion secondary battery scrap according to claim 4 , wherein in the lithium precipitating step, the lithium dissolved solution is heated to separate carbonic acid as a carbon dioxide gas from the lithium dissolved solution.

6. The method for recovering lithium from lithium ion secondary battery scrap according to claim 5 , wherein in the lithium precipitating step, the lithium dissolved solution is heated at a temperature of from 50° C. to 90° C.

7. The method for recovering lithium from lithium ion secondary battery scrap according to claim 1 , wherein in the lithium dissolving step, the water or the acidic solution has a temperature of from 5° C. to 25° C.

Assignments (5)
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Sep 23, 2024
From: JX ADVANCED METALS CORPORATION
To: JX METALS CIRCULAR SOLUTIONS CO., LTD.
Reel/Frame 068665/0857 →
CHANGE OF NAME Recorded Jul 29, 2024
From: JX METALS CORPORATION
To: JX ADVANCED METALS CORPORATION
Reel/Frame 068179/0696 →
CHANGE OF NAME Recorded Jun 27, 2024
From: JX NIPPON MINING & METALS CORPORATION
To: JX METALS CORPORATION
Reel/Frame 068050/0527 →
CHANGE OF ADDRESS Recorded May 4, 2023
From: JX NIPPON MINING & METALS CORPORATION
To: JX NIPPON MINING & METALS CORPORATION
Reel/Frame 063545/0343 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Feb 26, 2020
From: ARIYOSHI, HIROTAKA; TOMITA, ISAO; ABE, HIROSHI
To: JX NIPPON MINING & METALS CORPORATION
Reel/Frame 051938/0259 →