IP Library Granted Patent US 11,499,901
Granted Patent B2
US 11,499,901 · App. 16/643,036 · Granted Nov 15, 2022

Correcting for gravitational force variation in measuring the melt flow index of a polymer

Inventors: John A. Czazasty (Norton, MA); Michael P. Leonardi (Mansfield, MA)
Assignee: Dynisco Instruments LLC
G01N11/02G01N2011/0006
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Quick Facts
Patent No.
US 11,499,901
App. No.
16/643,036
Granted
Nov 15, 2022
Kind
B2
Abstract

Methods and apparatus are disclosed for correcting for gravitational force variation in measuring the melt flow index of a polymer at a location. For example, ample, some embodiments may involve determining a value representing an extent to which gravitational force at the location varies from standard gravity, such as based at least in part upon the latitude of the location. The value may be used in correcting the melt flow index measured for the polymer using a plastometer at the location.

Claims (25)

1. An apparatus, comprising:

instrumentation, adapted to measure a melt flow index for a polymer, at a location; and

a controller, configured to determine a melt flow index for the polymer at standard gravity, wherein the melt flow index for the polymer at standard gravity is determined based at least in part upon the melt flow index measured at the location using the instrumentation, and a value representing an extent to which gravitational force at the location varies from standard gravity.

2. The apparatus of claim 1 , wherein the value representing the extent to which gravitational force at the location varies from standard gravity is determined based at least in part on the latitude of the location.

3. The apparatus of claim 2 , wherein the value representing the extent to which gravitational force at the location varies from standard gravity is calculated as g standard /g, where g standard is standard gravity equal to 9.80665 m/s 2 , and g represents gravitational force at latitude ϕ and is given by g{ϕ}=9.780327 m/s 2 (1+0.00532024 sin 2 ϕ−0.0000058 sin 2 2ϕ).

4. The apparatus of claim 1 , wherein the instrumentation comprises a plastometer.

5. The apparatus of claim 4 , wherein the plastometer is adapted to measure the melt flow index for the polymer in accordance with ASTM D1238.

6. The apparatus of claim 1 , wherein the controller is implemented at least in part via software.

7. A method, comprising acts of:

(A) determining, for a location, a value representing an extent to which gravitational force at the location varies from standard gravity;

(B) employing the value determined in the act (A) to determine a melt flow index for a polymer at standard gravity.

8. The method of claim 7 , wherein the act (A) comprises determining a value representing the extent to which gravitational force at the location varies from standard gravity based at least in part upon the latitude of the location.

9. The method of claim 8 , wherein the act (A) comprises determining the value representing the extent to which gravitational force at the location varies from standard gravity by calculating g standard /g, where g standard is standard gravity equal to 9.80665 m/s 2 , and g represents gravitational force at latitude ϕ and is given by g{ϕ}=9.780327 m/s 2 (1+0.00532024 sin 2 ϕ−0.0000058 sin 2 2ϕ).

10. The method of claim 7 , wherein the act (B) comprises determining a melt flow index for the polymer at the location using a plastometer.

11. The method of claim 10 , wherein the plastometer is adapted to measure the melt flow index for the polymer in accordance with ASTM D1238.

12. The method of claim 7 , wherein the act (B) comprises executing programmed instructions to determine the melt flow index for the polymer at standard gravity.

13. The method of claim 7 , wherein the melt flow index for the polymer is determined using a plastometer comprising a load and piston, and wherein the act (B) comprises employing the value determined in the act (A) in modifying a mass of one or more of the load and piston.

14. The method of claim 7 , wherein the melt flow index for the polymer is determined using a plastometer comprising a scale for measuring a mass of extrudate, and wherein the act (B) comprises employing the value determined in the act (A) in adjusting the scale.

15. At least one computer-readable storage medium having instructions encoded thereon which, when executed by a computing system, cause the computing system to perform a method comprising acts of:

(A) determining, for a location, a value representing an extent to which gravitational force at the location varies from standard gravity;

(B) employing the value determined in the act (A) to determine a melt flow index for a polymer at standard gravity.

16. The at least one computer-readable storage medium of claim 15 , wherein the act (A) comprises determining a value representing the extent to which gravitational force at the location varies from standard gravity based at least in part on the latitude of the location.

17. The at least one computer-readable storage medium of claim 16 , wherein the act (A) comprises determining the value representing the extent to which gravitational force at the location varies from standard gravity by calculating g standard /g, where g standard is standard gravity equal to 9.80665 m/s 2 , and g represents gravitational force at latitude ϕ and is given by g g{ϕ}=9.780327 m/s 2 (1+0.00532024 sin 2 ϕ−0.0000058 sin 2 2ϕ).

18. The at least one computer-readable storage medium of claim 15 , wherein the act (B) comprises determining a melt flow index for the polymer at the location using a plastometer.

19. The at least one computer-readable storage medium of claim 18 , wherein the plastometer is adapted to measure the melt flow index for the polymer in accordance with ASTM D1238.

Assignments (5)
CORRECTIVE ASSIGNMENT TO CORRECT THE PATENT NUMBER PREVIOUSLY RECORDED AT REEL: 61997 FRAME: 614. ASSIGNOR(S) HEREBY CONFIRMS THE SECURITY AGREEMENT. Recorded Nov 13, 2025
From: ALPHA TECHNOLOGIES SERVICES LLC; AMOT CONTROLS LLC; COMPRESSOR CONTROLS LLC; CORNELL PUMP COMPANY LLC; DYNISCO INSTRUMENTS LLC; HANSEN TECHNOLOGIES LLC; METRIX INSTRUMENT CO., L.P.; PETROLEUM ANALYZER COMPANY L.P.; ROPER HOLDINGS, LLC; ROPER INDUSTRIAL PRODUCTS INVESTMENT COMPANY LLC; ROPER PUMP COMPANY LLC; STRUERS LLC; VIA TRAN CORPORATION
To: UBS AG, STAMFORD BRANCH, AS COLLATERAL AGENT
Reel/Frame 073434/0453 →
RELEASE OF SECOND LIEN PATENT SECURITY INTERESTS Recorded May 30, 2025
From: ROYAL BANK OF CANADA
To: AGR INTERNATIONAL, INC.; ALPHA TECHNOLOGIES SERVICES LLC; AMOT CONTROLS LLC; COMPRESSOR CONTROLS LLC; CORNELL PUMP COMPANY LLC; DYNISCO INSTRUMENTS LLC; HANSEN TECHNOLOGIES LLC; METRIX INSTRUMENT CO., L.P.; PETROLEUM ANALYZER COMPANY L.P.; ROPER HOLDINGS, LLC; ROPER INDUSTRIAL PRODUCTS INVESTMENT COMPANY LLC; ROPER PUMP COMPANY LLC; STRUERS LLC; VIATRAN CORPORATION
Reel/Frame 071476/0346 →
SECURITY AGREEMENT (FIRST LIEN) Recorded Nov 28, 2022
From: ALPHA TECHNOLOGIES SERVICES LLC; AMOT CONTROLS LLC; COMPRESSOR CONTROLS LLC; CORNELL PUMP COMPANY LLC; DYNISCO INSTRUMENTS LLC; HANSEN TECHNOLOGIES LLC; METRIX INSTRUMENT CO., L.P.; PETROLEUM ANALYZER COMPANY L.P.; ROPER HOLDINGS, LLC; ROPER INDUSTRIAL PRODUCTS INVESTMENT COMPANY LLC; ROPER PUMP COMPANY LLC; STRUERS LLC; VIATRAN CORPORATION
To: UBS AG, STAMFORD BRANCH, AS COLLATERAL AGENT
Reel/Frame 061997/0614 →
SECURITY AGREEMENT (SECOND LIEN) Recorded Nov 28, 2022
From: ALPHA TECHNOLOGIES SERVICES LLC; AMOT CONTROLS LLC; COMPRESSOR CONTROLS LLC; CORNELL PUMP COMPANY LLC; DYNISCO INSTRUMENTS LLC; HANSEN TECHNOLOGIES LLC; METRIX INSTRUMENT CO., L.P.; PETROLEUM ANALYZER COMPANY L.P.; ROPER HOLDINGS, LLC; ROPER INDUSTRIAL PRODUCTS INVESTMENT COMPANY LLC; ROPER PUMP COMPANY LLC; STRUERS LLC; VIATRAN CORPORATION
To: ROYL BANK OF CANADA, AS COLLATERAL AGENT
Reel/Frame 062003/0566 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Mar 23, 2022
From: CZAZASTY, JOHN A.; LEONARDI, MICHAEL P.
To: DYNISCO INSTRUMENTS LLC
Reel/Frame 059480/0406 →