IP Library Granted Patent US 11,787,152
Granted Patent B2
US 11,787,152 · App. 16/712,448 · Granted Oct 17, 2023

Method of preparing a composite sheet

Inventor: Behnam Pourdeyhimi (Cary, NC)
Assignee: North Carolina State University
B32B5/26B29C48/154B32B5/022B32B37/24D01D4/025D01D5/0985D01F6/625D04H3/011D04H3/013D04H3/08B32B2037/0092B32B2250/02B32B2250/24B32B2262/0276B32B2262/062B32B2305/10B32B2307/538B32B2307/7163B32B2307/726B32B2309/02B32B2309/08B32B2367/00B32B2432/00D10B2201/20D10B2321/021D10B2321/022D10B2321/06D10B2321/08D10B2331/02D10B2331/04D10B2331/041
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Quick Facts
Patent No.
US 11,787,152
App. No.
16/712,448
Granted
Oct 17, 2023
Kind
B2
Abstract

A composite sheet comprising two or more layers is described where the degree of abrasiveness of can be controlled. The sheet can comprise partially or wholly biodegradable or compostable materials or blends thereof. Methods of preparing the composite sheets are also described.

Claims (15)

1. A method of preparing a biodegradable or compostable composite sheet, the method comprising:

providing a base layer, wherein the base layer comprises a polymeric web consisting of a first polymer, wherein the first polymer comprises or consists of cellulose, and

meltblowing a second polymer onto a first surface of the base layer to form a first abrasive layer comprising meltblown fibers of the second polymer, wherein the second polymer is polylactic acid (PLA), wherein the meltblown fibers have a diameter of about 0.3 microns (μm) to about 5 μm, and wherein abrasiveness of the first abrasive layer is controlled by the diameter of the meltblown fibers.

2. The method of claim 1 , wherein the method further comprises meltblowing a third polymer onto a second surface of the base layer to form a second abrasive layer comprising meltblown fibers of the third polymer, wherein the third polymer is the same or different than the second polymer, and wherein the meltblown fibers of the second abrasive layer have a diameter of about 0.3 μm to about 20 μm.

3. The method of claim 2 , wherein the meltblown fibers of the second abrasive layer have a different diameter than the meltblown fibers of the first abrasive layer.

4. The method of claim 1 , wherein the meltblowing is performed using nozzles having a diameter of about 180 μm to about 600 μm and/or a nozzle density of about 10 per inch to about 75 per inch.

5. The method of claim 1 , wherein the meltblowing is performed using a die to collector distance (DCD) of about 50 millimeters (mm) to 300 mm.

6. The method of claim 5 , wherein the meltblowing is performed at a temperature of about 200° C. to about 300° C.

7. The method of claim 1 , wherein the first abrasive layer comprises about 1 grams per square meter (g/m 2 ) to about 30 g/m 2 of the second polymer.

8. The method of claim 7 , wherein the first abrasive layer comprises about 5 g/m 2 to about 15 g/m 2 of the second polymer.

9. The method of claim 1 , wherein the base layer comprises about 10 g/m 2 to about 150 g/m 2 cellulose.

10. The method of claim 9 , wherein the base layer comprises about 25 g/m 2 to about 55 g/m 2 cellulose.

11. The method of claim 1 , wherein the first polymer is cellulose.

12. The method of claim 1 , wherein the cellulose comprises pulp, lyocell, cotton, or a blend thereof.

13. The method of claim 1 , wherein the meltblowing of the second polymer is performed using an air consumption of about 1600 m 3 /m/hr to about 1900 m 3 /m/hr.

Assignments (1)
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Dec 12, 2019
From: POURDEYHIMI, BEHNAM
To: NORTH CAROLINA STATE UNIVERSITY
Reel/Frame 051269/0947 →
Continuity (2)
Provisional Application 62779070 · Dec 13, 2018
Related Publication 20200189230A1 · Jun 18, 2020