IP Library Granted Patent US 10,836,134
Granted Patent B2
US 10,836,134 · App. 16/720,627 · Granted Nov 17, 2020

Low reflection articles and related systems and methods

Inventors: Joshua D. Wiensch (Pasadena, CA); Tina Qin (Van Nuys, CA); Jonathan Seamus Blackley (South Pasadena, CA)
Assignee: Pacific Light & Hologram, Inc.
B32B5/18B32B5/20Y10T428/2495Y10T428/24802Y10T428/24901Y10T428/24917
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Quick Facts
Patent No.
US 10,836,134
App. No.
16/720,627
Granted
Nov 17, 2020
Kind
B2
Abstract

Low reflection articles, and related systems and methods are disclosed. The articles have a surface with primary pores and secondary pores. At least some of the secondary pores contain agent, such, for example, a light absorbing dye.

Claims (53)

1. An article, comprising:

a substrate comprising a metal; and

a light absorbing agent,

wherein:

a surface of the substrate comprises primary pores and secondary pores; and

an average diameter of the primary pores is at least four times greater than an average diameter of the secondary pores.

2. An article, comprising:

a substrate comprising a metal,

wherein:

a surface of the substrate comprises primary pores and secondary pores;

an average diameter of the primary pores is from 500 nm to 15 μm; and

an average diameter of the secondary pores 50 nm to about 250 nm.

3. The article of claim 2 , wherein an average diameter of the primary pores is at least four times greater than an average diameter of the secondary pores.

4. The article of claim 1 , wherein the average diameter of the primary pores is at least five times greater than the average diameter of the secondary pores.

5. The article of claim 1 , wherein the average diameter of the primary pores is at least 500 nm.

6. The article of claim 1 , wherein the average diameter of the primary pores is at least 1 μm.

7. The article of claim 1 , wherein the average diameter of the primary pores is at most 5 μm.

8. The article of claim 1 , wherein the article has a region which comprises the primary pores, and the region of the article has a porosity ratio of at least 0.1.

9. The article of claim 1 , wherein the article has a region which comprises the primary pores, and the region of the article has a porosity ratio of at most 0.3.

10. The article of claim 1 , wherein the average diameter of the secondary pores is at most 250 nm.

11. The article of claim 1 , wherein the average diameter of the secondary pores is at least 50 nm.

12. The article of claim 1 , wherein the secondary pores have an average aspect ratio of at least 10.

13. The article of claim 1 , wherein the secondary pores have an average aspect ratio of at most 40.

14. The article of claim 1 , wherein at least some of the secondary pores comprise the light absorbing agent.

15. The article of claim 14 , wherein the light absorbing agent comprises a visible light absorbing agent.

16. The article of claim 14 , wherein the light absorbing agent comprises a dye.

17. The article of claim 16 , wherein the dye comprises a water-soluble dye.

18. The article of claim 1 , wherein the surface of the article has a fractional reflectance of at most 0.0002 at a wavelength of from 400 nm to 700 nm.

19. The article of claim 1 , wherein:

the surface of the article has a first fractional reflectance at a first wavelength of from 400 nm to 700 nm;

the surface of the article has a second fractional reflectance at a second wavelength of from 400 nm to 700 nm;

the first wavelength is different from the second wavelength; and

the first fractional reflectance is different from the second fractional reflectance.

20. The article of claim 1 , wherein the surface of the article has a fractional reflectance of at most 0.0002 at a wavelength of from 10 nm to 400 nm.

21. The article of claim 1 , wherein the metal comprises a member selected from the group consisting of aluminum, titanium, niobium, tantalum, magnesium and zinc.

22. The article of claim 1 , wherein a portion of the substrate comprises an oxide, and the oxide comprises the metal.

23. The article of claim 22 , wherein the secondary pores are present in the portion of the oxide.

24. The article of claim 1 , wherein the surface of the article comprises a fluoro-aluminate.

25. The article of claim 1 , wherein the surface of the article comprises a hydrated aluminum oxide.

26. The article of claim 2 , wherein the article has a region which comprises the primary pores, and the region of the article has a porosity ratio of at least 0.1.

27. The article of claim 2 , wherein the secondary pores have an average aspect ratio of at least 10.

28. The article of claim 2 , further comprising a light absorbing agent.

29. The article of claim 28 , wherein at least some of the secondary pores comprise the light absorbing agent.

30. The article of claim 29 , wherein the light absorbing agent comprises a visible light absorbing agent.

31. The article of claim 29 , wherein the light absorbing agent comprises a dye.

32. The article of claim 31 , wherein the dye comprises a water-soluble dye.

33. The article of claim 2 , wherein the surface of the article has a fractional reflectance of at most 0.0002 at a wavelength of from 400 nm to 700 nm.

34. The article of claim 2 , wherein the surface of the article has a fractional reflectance of at most 0.0002 at a wavelength of from 10 nm to 400 nm.

35. The article of claim 2 , wherein the metal comprises a member selected from the group consisting of aluminum, titanium, niobium, tantalum, magnesium and zinc.

36. The article of claim 2 , wherein a portion of the substrate comprises an oxide, and the oxide comprises the metal.

37. The article of claim 36 , wherein the secondary pores are present in the portion of the oxide.

38. The article of claim 2 , wherein the surface of the article comprises a fluoro-aluminate.

39. The article of claim 2 , wherein the surface of the article comprises a hydrated aluminum oxide.

Assignments (1)
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Jan 24, 2020
From: WIENSCH, JOSHUA D.; QIN, TINA; BLACKLEY, JONATHAN SEAMUS
To: PACIFIC LIGHT & HOLOGRAM, INC.
Reel/Frame 051693/0844 →
Continuity (3)
Division 16025129 · Jul 2, 2018
Provisional Application 62537147 · Jul 26, 2017
Related Publication 20200124769A1 · Apr 23, 2020