IP Library Granted Patent US 11,306,199
Granted Patent B2
US 11,306,199 · App. 16/741,037 · Granted Apr 19, 2022

Elastomer formulation using a combination of polymers to create ozone resistance without addition of wax

Inventors: Jeanette Pilarski (Amherst, OH); Joshua R. Goossens (Norwalk, OH)
Assignee: The Pullman Company
C08L23/16C08L7/00C08L9/00C08L23/32C08L81/00C08L2205/03C08L2312/00
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Quick Facts
Patent No.
US 11,306,199
App. No.
16/741,037
Granted
Apr 19, 2022
Kind
B2
Abstract

A shaped article is formed from a cured rubber composition comprising EPDM and a diene rubber. The shaped article exhibits a coefficient of friction greater than 0.1.

Claims (22)

1. A shaped article formed from a cured rubber composition comprising:

ethylene propylene diene monomer (EPDM) having an organic polymer comprising sulfur covalently incorporated therein;

a diene rubber; and

a curing agent that cures the EPDM having the organic polymer comprising sulfur covalently incorporated therein to the diene rubber,

wherein the article has a coefficient of friction greater than 0.1, and

wherein the EPDM having the organic polymer comprising sulfur covalently incorporated therein is present in the cured rubber composition at a concentration of greater than about 5 wt. % and less than about 25 wt. % based on the total weight of the EPDM and the diene rubber.

2. The shaped article according to claim 1 , wherein the article has a coefficient of friction greater than 0.2.

3. The shaped article according to claim 1 , wherein the article has a coefficient of friction greater than 0.5.

4. The shaped article according to claim 1 , wherein the article has a coefficient of friction from 0.5 to 0.8.

5. The shaped article according to claim 4 , giving a pass on an ozone resistance test according to ASTM D-1149 when subjected to 50 pphm ozone for 72 hours at 40° C.

6. The shaped article according to claim 1 , wherein the article has a coefficient of friction from 0.6 to 0.7.

7. The shaped article according to claim 1 , giving a pass on an ozone resistance test according to ASTM D-1149 when subjected to 200 pphm ozone for 24 hours at 40° C.

8. The shaped article according to claim 1 , wherein the article comprises 25 wt. % EPDM and 75 wt. % diene rubber based on the total weight on the EPDM having the organic polymer comprising sulfur covalently incorporated therein and the diene rubber.

9. The shaped article according to claim 1 , wherein the organic polymer comprising sulfur includes a poly(alkyl phenol) disulfide polymer.

10. The shaped article according to claim 1 , wherein the cured rubber composition does not include a wax.

11. A shaped article formed from a cured rubber composition comprising:

a diene; and

an ethylene propylene diene monomer (EPDM) having an organic polymer comprising sulfur covalently incorporated therein,

wherein the diene is cross-linked to the EPDM having the organic polymer comprising sulfur with elemental sulfur.

12. The shaped article according to claim 11 , wherein the EPDM having the organic polymer comprising sulfur covalently incorporated therein is present in the cured rubber composition at a concentration of greater than about 5 wt. % and less than about 25 wt. %.

13. The shaped article according to claim 11 , wherein the organic polymer comprising sulfur includes a poly(alkyl phenol) disulfide polymer.

14. The shaped article according to claim 13 , wherein the shaped article has a coefficient of friction greater than 0.2 and passes an ozone resistance test according to ASTM D-1149 when subjected to 200 pphm ozone for 24 hours at 40° C.

Assignments (7)
CHANGE OF NAME Recorded Aug 20, 2025
From: THE PULLMAN COMPANY
To: THE PULLMAN COMPANY LLC
Reel/Frame 072553/0230 →
PATENT SECURITY AGREEMENT (ABL) Recorded Apr 7, 2023
From: TENNECO INC.; DRIV AUTOMOTIVE INC.; FEDERAL-MOGUL CHASSIS LLC; FEDERAL-MOGUL IGNITION LLC; FEDERAL-MOGUL MOTORPARTS LLC; FEDERAL-MOGUL POWERTRAIN LLC; FEDERAL-MOGUL WORLD WIDE LLC; TENNECO AUTOMOTIVE OPERATING COMPANY INC.; THE PULLMAN COMPANY
To: CITIBANK, N.A., AS COLLATERAL AGENT
Reel/Frame 063268/0506 →
NOTICE OF GRANT OF SECURITY INTEREST IN PATENTS (FIRST LIEN) Recorded Nov 22, 2022
From: DRIV AUTOMOTIVE INC.; FEDERAL-MOGUL CHASSIS LLC; FEDERAL-MOGUL IGNITION LLC; FEDERAL-MOGUL MOTORPARTS LLC; FEDERAL-MOGUL POWERTRAIN LLC; FEDERAL-MOGUL WORLD WIDE LLC; TENNECO AUTOMOTIVE OPERATING COMPANY INC.; TENNECO INC.; THE PULLMAN COMPANY
To: CITIBANK, N.A., AS COLLATERAL AGENT
Reel/Frame 061989/0689 →
RELEASE OF SECURITY INTEREST Recorded Nov 19, 2022
From: WILMINGTON TRUST, NATIONAL ASSOCIATION
To: TENNECO INC.; TENNECO AUTOMOTIVE OPERATING COMPANY INC.; THE PULLMAN COMPANY; FEDERAL-MOGUL IGNITION LLC; FEDERAL-MOGUL POWERTRAIN LLC; FEDERAL-MOGUL PRODUCTS US LLC; FEDERAL-MOGUL MOTORPARTS LLC; FEDERAL-MOGUL WORLD WIDE LLC; FEDERAL-MOGUL CHASSIS LLC; DRIV AUTOMOTIVE INC.
Reel/Frame 061971/0156 →
RELEASE OF SECURITY INTEREST Recorded Nov 19, 2022
From: WILMINGTON TRUST, NATIONAL ASSOCIATION
To: TENNECO INC.; TENNECO AUTOMOTIVE OPERATING COMPANY INC.; THE PULLMAN COMPANY; FEDERAL-MOGUL IGNITION LLC; FEDERAL-MOGUL POWERTRAIN LLC; FEDERAL-MOGUL PRODUCTS US LLC; FEDERAL-MOGUL WORLD WIDE LLC; FEDERAL-MOGUL CHASSIS LLC; DRIV AUTOMOTIVE INC.
Reel/Frame 061975/0031 →
SECURITY AGREEMENT Recorded Mar 17, 2021
From: TENNECO INC.; TENNECO AUTOMOTIVE OPERATING COMPANY INC.; THE PULLMAN COMPANY; FEDERAL-MOGUL IGNITION LLC; FEDERAL-MOGUL POWERTRAIN LLC; FEDERAL-MOGUL PRODUCTS US LLC; FEDERAL-MOGUL WORLD WIDE LLC; FEDERAL-MOGUL CHASSIS LLC; DRIV AUTOMOTIVE INC.
To: WILMINGTON TRUST, NATIONAL ASSOCIATION
Reel/Frame 055626/0065 →
SECURITY AGREEMENT Recorded Dec 1, 2020
From: TENNECO INC.; THE PULLMAN COMPANY; FEDERAL-MOGUL IGNITION LLC; FEDERAL-MOGUL POWERTRAIN LLC; FEDERAL-MOGUL PRODUCTS US LLC; FEDERAL-MOGUL MOTORPARTS LLC; FEDERAL-MOGUL WORLD WIDE LLC; FEDERAL-MOGUL CHASSIS LLC; DRIV AUTOMOTIVE INC.; TENNECO AUTOMOTIVE OPERATING COMPANY INC.
To: WILMINGTON TRUST, NATIONAL ASSOCIATION
Reel/Frame 054555/0592 →