IP Library Granted Patent US 11,583,832
Granted Patent B2
US 11,583,832 · App. 16/780,213 · Granted Feb 21, 2023

Manganese oxide based catalyst and catalyst device for the removal of formaldehyde and volatile organic compounds

Inventors: David Weinberger (Philadelphia, PA); Wolfgang Ruettinger (East Windsor, NJ); Pascaline Tran (Holmdel, NJ); Laif Alden (Feasterville, PA); Ting Gu (Shanghai, CN); Feng Zhao (Shanghai, CN); Anju Shi (Shanghai, CN); Nils Lawrenz (Schifferstadt, DE); Lukas Wengeler (Ludwigshafen, DE)
Assignee: BASF Corporation
B01J23/34B01D53/8668B01D53/8675B01J20/18B01J20/20B01J20/226B01J20/2803B01J21/04B01J35/0033B01J35/04B01J35/1004B01J35/1009B01J35/1014B01J35/1019B01J35/1033B01J35/1038B01J35/1042B01J35/1047B01J37/0009B01J37/0018B01J37/0201B01J37/0215B01J37/0225B01J37/04B01J37/08B01D53/86B01D2255/2065B01D2255/2073B01D2255/20715B01D2257/106B01D2257/502B01D2257/708B01D2258/06B01J21/063B01J21/066B01J21/08B01J21/16B01J21/18B01J23/10B01J35/026
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Quick Facts
Patent No.
US 11,583,832
App. No.
16/780,213
Granted
Feb 21, 2023
Kind
B2
Abstract

Disclosed herein are a catalyst composition, catalyst devices, and methods for removing formaldehyde, volatile organic compounds, and other pollutants from an air flow stream. The catalyst composition including manganese oxide, optionally one or more of alkali metals, alkaline earth metals, zinc, iron, binder, an inorganic oxide, or carbon.

Claims (30)

1. A catalyst composition comprising:

manganese oxide;

bentonite from about 40 wt % to about 50 wt % based on a total weight of the catalyst composition; and

a polymer binder comprising poly(tetrafluoroethylene), acrylic/styrene acrylic copolymer latex, or a combination thereof,

wherein the catalyst composition is disposed on a substrate selected from a polymer substrate, a foam substrate, a paper substrate, a nonwoven filter, a paper filter, a fibrous filter, or a combination thereof, and

wherein the catalyst composition is adapted to remove one or more of formaldehyde, ozone, carbon monoxide, nitrogen oxide, amines, sulfur compounds, thiols, chlorinated hydrocarbons, or volatile organic compounds from an unpurified air supply, and wherein a BJH pore volume of the catalyst composition ranges from about 0.3 mL/g to about 1.5 mL/g.

2. The catalyst composition of claim 1 , wherein the polymer binder further comprises a polymer selected from a group consisting of polyethylene, polypropylene, polyolefin copolymers, polyisoprene, polybutadiene, polybutadiene copolymers, chlorinated rubber, nitrile rubber, polychloroprene, ethylene-propylene-diene elastomers, polystyrene, polyacrylate, polymethacrylate, polyacrylonitrile, poly(vinyl esters), poly(vinyl halides), polyamides, cellulosic polymers, polyimides, acrylics, vinyl acrylics, styrene acrylics, polyvinyl alcohols, thermoplastic polyesters, thermosetting polyesters, poly(phenylene oxide), poly(phenylene sulfide), polyvinylidene fluoride, poly(vinlyfluoride), ethylene chlorotrifluoroethylene copolymer, polyamide, phenolic resins, polyurethane, silicone polymers, and combinations thereof.

3. The catalyst composition of claim 1 , wherein the manganese oxide comprises cryptomelane, birnessite, vernadite, manganese oxide polymorph I, poorly crystalline cryptomelane, amorphous manganese oxide, polymorphs thereof, or mixtures thereof.

4. The catalyst composition of claim 1 , wherein a chloride content of the catalyst composition is less than 1 wt % based on a total weight of the catalyst composition, or wherein a sulfate content of the catalyst composition is less than 1 wt % based on a total weight of the catalyst composition.

5. The catalyst composition of claim 1 , further comprising an inorganic oxide comprising one or more of ceria, zirconia, silica, titania, alumina, iron, lanthanum, praseodymium, samarium.

6. An air filter comprising the catalyst composition of claim 1 , wherein the air filter is adapted for use in a portable air purifier, a heating, ventilation, and air conditioning (HVAC) system, a motor vehicle, a railed vehicle, a watercraft, an aircraft, or a spacecraft.

7. A catalyst device adapted to remove one or more of formaldehyde, ozone, carbon monoxide, nitrogen oxide, amines, sulfur compounds, thiols, chlorinated hydrocarbons, or volatile organic compounds from an unpurified air supply, the catalyst device comprising:

a housing;

a substrate disposed within the housing, wherein the substrate is selected from a polymer substrate, a foam substrate, a paper substrate, a nonwoven filter, a paper filter, a fibrous filter, or a combination thereof; and

a catalyst composition disposed in the housing, wherein the catalyst composition comprises manganese oxide, bentonite from about 40 wt % to about 50 wt % based on a total weight of the catalyst composition, and a polymer binder comprising poly(tetrafluoroethylene), acrylic/styrene acrylic copolymer latex, or a combination thereof, wherein a BJH pore volume of the catalyst composition ranges from about 0.3 mL/g to about 1.5 mL/g.

8. The catalyst device of claim 7 , wherein the polymer binder further comprises a polymer selected from a group consisting of polyethylene, polypropylene, polyolefin copolymers, polyisoprene, polybutadiene, polybutadiene copolymers, chlorinated rubber, nitrile rubber, polychloroprene, ethylene-propylene-diene elastomers, polystyrene, polyacrylate, polymethacrylate, polyacrylonitrile, poly(vinyl esters), poly(vinyl halides), polyamides, cellulosic polymers, polyimides, acrylics, vinyl acrylics, styrene acrylics, polyvinyl alcohols, thermoplastic polyesters, thermosetting polyesters, poly(phenylene oxide), poly(phenylene sulfide), polyvinylidene fluoride, poly(vinlyfluoride), ethylene chlorotrifluoroethylene copolymer, polyamide, phenolic resins, polyurethane, silicone polymers, and combinations thereof.

9. The catalyst device of claim 7 , wherein the manganese oxide comprises cryptomelane, birnessite, vernadite, manganese oxide polymorph I, poorly crystalline cryptomelane, amorphous manganese oxide, polymorphs thereof, or mixtures thereof.

10. The catalyst device of claim 7 , wherein a chloride content of the catalyst composition is less than 1 wt % based on a total weight of the catalyst composition, or wherein a sulfate content of the catalyst composition is less than 1 wt % based on a total weight of the catalyst composition.

11. The catalyst device of claim 7 , further comprising an inorganic oxide comprising one or more of ceria, zirconia, silica, titania, alumina, iron, lanthanum, praseodymium, samarium.

12. The catalyst device of claim 7 , wherein the catalyst device is incorporated into an air filter of a device selected from a group consisting of: a portable air purifier, a heating, ventilation, and air conditioning (HVAC) system, a motor vehicle, a railed vehicle, a watercraft, an aircraft, and a spacecraft.

13. A method of preparing a catalyst coating, the method comprising:

mixing manganese oxide, bentonite, and a polymer binder in water to form a slurry, the polymer binder comprising poly(tetrafluoroethylene), acrylic/styrene acrylic copolymer latex, or a combination thereof; and

depositing the slurry onto a substrate to form the catalyst coating on the substrate, wherein the substrate selected from a polymer substrate, a foam substrate, a paper substrate, a nonwoven filter, a paper filter, a fibrous filter, or a combination thereof, wherein a BJH pore volume of the catalyst coating ranges from about 0.3 mL/g to about 1.5 mL/g, wherein the bentonite is present from about 40 wt % to about 50 wt % based on a total weight of the catalyst coating.

14. The method of claim 13 , wherein the polymer binder further comprises a polymer selected from a group consisting of polyethylene, polypropylene, polyolefin copolymers, polyisoprene, polybutadiene, polybutadiene copolymers, chlorinated rubber, nitrile rubber, polychloroprene, ethylene-propylene-diene elastomers, polystyrene, polyacrylate, polymethacrylate, polyacrylonitrile, poly(vinyl esters), poly(vinyl halides), polyamides, cellulosic polymers, polyimides, acrylics, vinyl acrylics, styrene acrylics, polyvinyl alcohols, thermoplastic polyesters, thermosetting polyesters, poly(phenylene oxide), poly(phenylene sulfide), polyvinylidene fluoride, poly(vinlyfluoride), ethylene chlorotrifluoroethylene copolymer, polyamide, phenolic resins, polyurethane, silicone polymers, and combinations thereof.

15. The method of claim 13 , wherein the manganese oxide comprises cryptomelane, birnessite, vernadite, manganese oxide polymorph I, poorly crystalline cryptomelane, amorphous manganese oxide, polymorphs thereof, or mixtures thereof.

16. A catalyst composition comprising:

manganese oxide comprising cryptomelane;

bentonite from about 40 wt % to about 50 wt % based on a total weight of the catalyst composition; and

a polymer binder, wherein the catalyst composition is adapted to remove one or more of formaldehyde, ozone, carbon monoxide, nitrogen oxide, amines, sulfur compounds, thiols, chlorinated hydrocarbons, or volatile organic compounds from an unpurified air supply, and wherein a BJH pore volume of the catalyst composition ranges from about 0.3 mL/g to about 1.5 mL/g,

wherein the catalyst composition is disposed on a substrate selected from a polymer substrate, a foam substrate, a paper substrate, a nonwoven filter, a paper filter, a fibrous filter, or a combination thereof.

Assignments (6)
NUNC PRO TUNC ASSIGNMENT Recorded Aug 8, 2024
From: BASF CORPORATION
To: BASF MOBILE EMISSIONS CATALYSTS LLC
Reel/Frame 068518/0394 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Sep 8, 2020
From: BASF SE
To: BASF CORPORATION
Reel/Frame 053714/0553 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Sep 2, 2020
From: BASF CATALYSTS (SHANGHAI) CO., LTD.
To: BASF CORPORATION
Reel/Frame 053677/0249 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Aug 21, 2020
From: LAWRENZ, NILS; WENGELER, LUKAS
To: BASF SE
Reel/Frame 053558/0436 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Aug 19, 2020
From: GU, TING; ZHAO, FENG; SHI, ANJU
To: BASF CATALYSTS (SHANGHAI) CO., LTD.
Reel/Frame 053538/0682 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Aug 17, 2020
From: WEINBERGER, DAVID S.; RUETTINGER, WOLFGANG; TRAN, PASCALINE; ALDEN, LAIF R.
To: BASF CORPORATION
Reel/Frame 053507/0622 →
Continuity (4)
Continuation 16309666
Provisional Application 62509633 · May 22, 2017
Provisional Application 62357007 · Jun 30, 2016
Related Publication 20200171464A1 · Jun 4, 2020