IP Library Granted Patent US 11,579,134
Granted Patent B2
US 11,579,134 · App. 16/786,930 · Granted Feb 14, 2023

Sampling for monitoring per- and polyfluoroalkyl substances (PFAS) in surface water, groundwater and pore water

Inventors: Eliza M. Kaltenberg (Quincy, MA); Franco Pala (Rockland, MA); Kavitha Dasu (Hanover, MA); Fred Griesemer (Columbus, OH); Bradley Westlake (Columbus, OH); George Nanes (Columbus, OH)
Assignee: Battelle Memorial Institute
G01N33/1826B01J20/262B01J20/2805B01J20/28045C08L75/06C08L75/08G01N1/10G01N1/405G01N2001/1031
View Patent ↗
Loading inventors, assignments & file history…
Monitor This Case
Get email alerts when status or documents change.
Order Certified Copies
Most orders are placed with the USPTO same day — all within 24 business hours.
Order via The Patent Place →
Pre-filled with this patent's details
Quick Facts
Patent No.
US 11,579,134
App. No.
16/786,930
Granted
Feb 14, 2023
Kind
B2
Abstract

Methods of passively sampling PFAS in the environment, PFAS sorbents, apparatus and systems (apparatus plus conditions) for sampling groundwater, porewater, and surface water are described.

Claims (20)

1. A PFAS groundwater sampler, comprising:

a housing comprising a wall or walls that define an internal cross-sectional area;

a PFAS sorbent material disposed within the housing;

wherein the sampler has a mass of at least 0.05 grams and a ratio of sorbent mass to housing internal cross-sectional area of no more than 3 g/10 cm 2 ; and wherein the sorbent has a log K d of 10 or less for each of PFOA and PFOS and PFBS.

2. The sampler of claim 1 wherein the sorbent is a polymer.

3. A PFAS sampler, comprising:

a PFAS sorbent film or foam that is covered by a copper mesh.

4. The PFAS sampler of claim 3 comprising five layers wherein the PFAS sorbent film or foam is sandwiched between two pieces of copper mesh and two pieces of stainless steel mesh such that the sampler comprises layers of the orders: stainless steel:copper:PFAS sorbent:copper:stainless steel.

5. The PFAS groundwater sampler of claim 1 wherein the sampler has a ratio of sorbent mass to housing internal cross-sectional area of no more than 1 g/10 cm 2 .

6. The PFAS groundwater sampler of claim 1 wherein the sorbent is a polymeric foam.

7. A PFAS groundwater sampler, comprising:

a housing comprising a wall or walls that define an internal cross-sectional area;

a PFAS sorbent material disposed within the housing;

wherein the sampler has a mass of at least 0.05 grams and a ratio of sorbent mass to housing internal cross-sectional area of no more than 3 g/10 cm 2 ; wherein the sorbent is a polymeric foam and wherein the foam comprises two types of polyurethane.

8. The PFAS groundwater sampler of claim 7 wherein the two types are ether-polyurethane and ester-polyurethane.

9. A PFAS groundwater sampler, comprising:

a housing comprising a wall or walls that define an internal cross-sectional area;

a PFAS sorbent material disposed within the housing;

wherein the sampler has a mass of at least 0.05 grams and a ratio of sorbent mass to housing internal cross-sectional area of no more than 3 g/10 cm 2 ; wherein the sorbent is a polymeric foam and wherein the polymeric foam is further characterizable by at least one of the parameters shown in Table 2, 4, or 5 and having a value of ±50% of that parameter as shown in Table 2, 4, or 5.

10. The PFAS groundwater sampler of claim 6 wherein the sorbent is a single material.

Assignments (1)
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Aug 23, 2022
From: KALTENBERG, ELIZA M.; PALA, FRANCO; DASU, KAVITHA; GRIESEMER, FRED; WESTLAKE, BRADLEY; NANES, GEORGE
To: BATTELLE MEMORIAL INSTITUTE
Reel/Frame 060875/0122 →
Continuity (4)
Provisional Application 62900109 · Sep 13, 2019
Provisional Application 62869623 · Jul 2, 2019
Provisional Application 62803581 · Feb 10, 2019
Related Publication 20200292516A1 · Sep 17, 2020
Cited By (8)
US 12,275,661 US 12,304,850 US 12,351,498 US 12,473,222 US 12,515,974 US 12,534,390 US 12,545,601 US 12,655,051