IP Library Granted Patent US 10,730,853
Granted Patent B2
US 10,730,853 · App. 16/793,139 · Granted Aug 4, 2020

Compounds as neuronal histamine receptor-3 antagonists and uses thereof

Inventors: Jia-Ning Xiang (Wuhan, CN); Xuesong Xu (Wuhan, CN); Yi Feng (Wuhan, CN); Wai-Si Eng (Maple Glen, PA)
Assignee: XW LABORATORIES INC.
C07D401/12
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Quick Facts
Patent No.
US 10,730,853
App. No.
16/793,139
Granted
Aug 4, 2020
Kind
B2
Abstract

The present invention relates compounds of Formula (A) as H3R antagonists, as well as their preparation and uses, and further relates pharmaceutical compositions comprising these compounds and their uses as modulators of Histamine 3 Receptor (H3R) functions. The present invention also relates to the uses of the compounds or pharmaceutical compositions in treating or preventing certain disorders and diseases which relate to H3R functions in humans.

Claims (46)

1. A method of treating narcolepsy in a patient comprising administering to a patient in need thereof a therapeutically effective amount of a compound having the structure:

or a pharmaceutically acceptable salt thereof, wherein,

R 1 is selected from hydrogen and C 1-3 alkyl; and

R 2 is selected from hydrogen, hydroxyl, and C 1-3 alkoxy.

2. The method of claim 1 , wherein,

R 1 is selected from hydrogen and methyl; and

R 2 is selected from hydrogen, hydroxyl, and methoxy.

3. The method of claim 1 , wherein,

R 1 is hydrogen; and

R 2 is selected from hydrogen, hydroxyl, and methoxy.

4. The method of claim 1 , wherein,

R 1 is selected from hydrogen and methyl; and

R 2 is hydrogen.

5. The method of claim 1 , wherein the compound is 2-methyl-3-(4-(3-(pyrrolidin-1-yl)propoxy)phenyl)-6-(pentafluorosulfanyl) quinazolin-4(3H)-one (I) or a pharmaceutically acceptable salt thereof:

6. The method of claim 1 , wherein the compound is selected from:

(S)-2-methyl-3-(4-(3-(2-methylpyrrolidin-1-yl)propoxy)phenyl)-6-(pentafluorosulfanyl)quinazolin-4(3H)-one (II);

(R)-2-methyl-3-(4-(3-(2-methylpyrrolidin-1-yl)propoxy)phenyl)-6-(pentafluorosulfanyl)quinazolin-4(3H)-one (IV);

3-(2-methoxy-4-(3-(pyrrolidin-1-yl)propoxy)phenyl)-2-methyl-6-(pentafluorosulfanyl)quinazolin-4(3H)-one (VI);

3-(2-methoxy-4-((1-(tetrahydro-2H-pyran-4-carbonyl)piperidin-4-yl)oxy)phenyl)-2-methyl-6-(pentafluorosulfanyl)quinazolin-4(3H)-one (VIII);

(R)-3-(2-methoxy-4-(3-(2-methylpyrrolidin-1-yl)propoxy)phenyl)-2-methyl-6-(pentafluorosulfanyl)quinazolin-4(3H)-one (X);

3-(2-methoxy-4-(3-(3-methylpyrrolidin-1-yl)propoxy)phenyl)-2-methyl-6-(pentafluorosulfanyl)quinazolin-4(3H)-one (XII); and

(S)-3-(2-methoxy-4-(3-(2-methylpyrrolidin-1-yl)propoxy)phenyl)-2-methyl-6-(pentafluorosulfanyl)quinazolin-4(3H)-one (XIII);

or a pharmaceutically acceptable salt of any of the foregoing.

7. A method of treating narcolepsy in a patient comprising administering to a patient in need thereof a therapeutically effective amount of a pharmaceutical composition comprising a compound having the structure:

or a pharmaceutically acceptable salt thereof, wherein,

R 1 is selected from hydrogen and C 1-3 alkyl; and

R 2 is selected from hydrogen, hydroxyl, and C 1-3 alkoxy.

8. The method of claim 7 , wherein,

R 1 is selected from hydrogen and methyl; and

R 2 is selected from hydrogen, hydroxyl, and methoxy.

9. The method of claim 7 , wherein,

R 1 is hydrogen; and

R 2 is selected from hydrogen, hydroxyl, and methoxy.

10. The method of claim 7 , wherein,

R 1 is selected from hydrogen and methyl; and

R 2 is hydrogen.

11. The method of claim 7 , wherein the compound is 2-methyl-3-(4-(3-(pyrrolidin-1-yl)propoxy)phenyl)-6-(pentafluorosulfanyl) quinazolin-4(3H)-one (I) or a pharmaceutically acceptable salt thereof:

12. The method of claim 7 , wherein the compound is selected from:

(S)-2-methyl-3-(4-(3-(2-methylpyrrolidin-1-yl)propoxy)phenyl)-6-(pentafluorosulfanyl)quinazolin-4(3H)-one (II);

(R)-2-methyl-3-(4-(3-(2-methylpyrrolidin-1-yl)propoxy)phenyl)-6-(pentafluorosulfanyl)quinazolin-4(3H)-one (IV);

3-(2-methoxy-4-(3-(pyrrolidin-1-yl)propoxy)phenyl)-2-methyl-6-(pentafluorosulfanyl)quinazolin-4(3H)-one (VI);

3-(2-methoxy-4-((1-(tetrahydro-2H-pyran-4-carbonyl)piperidin-4-yl)oxy)phenyl)-2-methyl-6-(pentafluorosulfanyl)quinazolin-4(3H)-one (VIII);

(R)-3-(2-methoxy-4-(3-(2-methylpyrrolidin-1-yl)propoxy)phenyl)-2-methyl-6-(pentafluorosulfanyl)quinazolin-4(3H)-one (X);

3-(2-methoxy-4-(3-(3-methylpyrrolidin-1-yl)propoxy)phenyl)-2-methyl-6-(pentafluorosulfanyl)quinazolin-4(3H)-one (XII); and

(S)-3-(2-methoxy-4-(3-(2-methylpyrrolidin-1-yl)propoxy)phenyl)-2-methyl-6-(pentafluorosulfanyl)quinazolin-4(3H)-one (XIII);

or a pharmaceutically acceptable salt of any of the foregoing.

Assignments (2)
CHANGE OF NAME Recorded May 4, 2021
From: XW LABORATORIES INC.
To: XWPHARMA LTD.
Reel/Frame 056177/0619 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Feb 18, 2020
From: XIANG, JIA-NING; XU, XUESONG; FENG, YI; ENG, WAI-SI
To: XW LABORATORIES INC.
Reel/Frame 051849/0134 →
Continuity (3)
Division 16587344 · Sep 30, 2019
Continuation PCTCN2018109115 · Sep 30, 2018
Related Publication 20200181112A1 · Jun 11, 2020
Cited By (13)
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