IP Library Granted Patent US 11,768,198
Granted Patent B2
US 11,768,198 · App. 16/795,467 · Granted Sep 26, 2023

Compositions and methods for molecular labeling

Inventors: Michael L. Samuels (Windham, NH); Jeffrey Charles Olson (Chelmsford, MA); Andrew Watson (Bedford, MA); Keith Brown (Carlsbad, CA); Darren R. Link (Lexington, MA)
Assignee: BIO-RAD LABORATORIES, INC.
G01N33/53C12N15/1075C12Q1/6804C12Q1/6806C12Q1/6874C40B50/08G01N33/532G01N33/5436G01N33/58C12Q2521/10C12Q2563/179C12Q2565/30G01N2458/10
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Quick Facts
Patent No.
US 11,768,198
App. No.
16/795,467
Granted
Sep 26, 2023
Kind
B2
Abstract

The invention provides barcode libraries and methods of making and using them including obtaining a plurality of nucleic acid constructs in which each construct comprises a unique N-mer and a functional N-mer and segregating the constructs into a fluid compartments such that each compartment contains one or more copies of a unique construct. The invention further provides methods for digital PCR and for use of barcode libraries in digital PCR.

Claims (14)

1. A method for protein detection, the method comprising:

introducing a protein-specific binding reagent linked to an oligonucleotide barcode to a sample comprising a population of cells;

encapsulating the cells in sample droplets such that each sample droplet comprises a single cell and said protein-specific binding reagent by merging droplets containing said cells and said protein-specific binding reagents; and

determining the presence of proteins of said cells that are bound to said protein-specific binding reagents.

2. The method of claim 1 , further comprising the step of lysing said cells.

3. The method of claim 1 , wherein said protein-specific binding reagent is selected from an antibody, an aptamer, a nucleic acid-labeled protein.

4. The method of claim 1 , wherein the protein-specific binding reagents are coupled to beads.

5. The method of claim 1 , wherein the protein-specific binding reagents are cleavable from the proteins to which they bind.

6. The method of claim 1 , wherein the proteins are cell-surface proteins.

7. The method of claim 1 , wherein the encapsulating step comprises loading the cells into a microfluidic chip.

8. The method of claim 1 , wherein the protein-specific binding reagents further comprise a universal binding site.

9. The method of claim 1 , further comprising quantifying the proteins.

10. The method of claim 1 , wherein the oligonucleotide barcodes linked to the protein-specific binding reagents have ligation-competent ends and the method includes ligating copies of droplet-identifying barcodes to the oligonucleotide barcodes linked to said protein-specific binding reagents.

11. The method of claim 2 , wherein lysing occurs within said droplets.

Assignments (2)
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded May 18, 2020
From: SAMUELS, MICHAEL; OLSON, JEFFREY CHARLES; WATSON, ANDREW; BROWN, KEITH; LINK, DARREN ROY
To: RAINDANCE TECHNOLOGIES, INC.
Reel/Frame 052682/0456 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded May 18, 2020
From: RAINDANCE TECHNOLOGIES, INC.
To: BIO-RAD LABORATORIES, INC.
Reel/Frame 052682/0470 →
Cited By (1)
US 12,461,094