IP Library Granted Patent US 11,998,956
Granted Patent B2
US 11,998,956 · App. 16/798,792 · Granted Jun 4, 2024

Method of, and an apparatus for, rinsing materialographic samples

Inventors: Thomas Matschofsky (Albertslund, DK); Palle Oppelstrup (Ballerup, DK)
Assignee: Struers APS
B08B3/12B08B3/10G01N1/32G01N1/34H01L21/67057H01L21/68721H01L21/68764H01L21/68771H01L21/68792A47L2601/17
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Quick Facts
Patent No.
US 11,998,956
App. No.
16/798,792
Granted
Jun 4, 2024
Kind
B2
Abstract

The present invention relates to a method of, and an apparatus for rinsing materialographic samples. The apparatus includes a sample holder configured to receive materialographic samples, a rotation head configured to rotate the sample holder and a vessel configured to receive the sample holder and a rinsing liquid. The apparatus also includes means for filling and emptying the vessel with rinsing liquid, means for applying ultrasound to the rinsing liquid and a control means. The control means is configured to control at least one of filling of the vessel with a rinsing liquid by injecting rinsing liquid through an inlet provided in the vessel to submerge the materialographic samples in the rinsing liquid, subjecting the rinsing liquid and the materialographic samples to ultrasound, or rotating the sample holder including the materialographic samples relative to the vessel.

Claims (36)

1. A rinsing apparatus configured to rinse materialographic samples, comprising:

a sample holder configured to receive materialographic samples, wherein the materialographic samples comprise at least one of metal, polymer or ceramic samples that have been cut and subjected to at least one of a grinding or lapping procedure;

a rotation head configured to rotate the sample holder;

a vessel configured to receive the sample holder and a rinsing liquid,

means for filling and emptying the vessel with rinsing liquid;

means for applying ultrasound to the rinsing liquid; and

control means configured to control at least one of:

filling of the vessel with a rinsing liquid by injecting rinsing liquid through an inlet provided in the vessel to submerge the materialographic samples in the rinsing liquid,

subjecting the rinsing liquid and the materialographic samples to ultrasound, or

rotating the sample holder including the materialographic samples relative to the vessel,

wherein the rinsing apparatus further comprises one or more clamps to maintain the materialographic samples in the sample holder during rotation of the sample holder.

2. The rinsing apparatus according to claim 1 , wherein the inlet is located at the bottom of the vessel.

3. A rinsing apparatus configured to rinse materialographic samples, comprising:

a sample holder configured to receive materialographic samples;

a rotation head configured to rotate the sample holder;

a vessel configured to receive the sample holder and a rinsing liquid;

means for filling and emptying the vessel with rinsing liquid;

means for applying ultrasound to the rinsing liquid;

control means configured to control at least one of:

filling of the vessel with a rinsing liquid by injecting rinsing liquid through an inlet provided in the vessel to submerge the samples in the rinsing liquid,

subjecting the rinsing liquid and the materialographic samples to ultrasound, or

rotating the sample holder including the materialographic samples relative to the vessel; and

a retainer plate configured to be arranged on top of the sample holder to maintain the materialographic samples in the sample holder during rotation of the sample holder.

4. The rinsing apparatus according to claim 3 , wherein the retainer plate is made from a flexible material.

5. The rinsing apparatus according to claim 3 , wherein the retainer plate is, on an upper face, provided with fins configured to urge the retainer plate against the sample holder during rotation of the sample holder.

6. The rinsing apparatus according to claim 3 , wherein the retainer plate is, on a face facing the sample holder, provided with means to interlock the retainer plate with respect to the sample holder.

7. A rinsing apparatus configured to rinse materialographic samples, comprising:

a sample holder comprising a plate with a plurality of receptacles, each configured to receive a materialographic sample;

a rotation head configured to rotate the sample holder with said received samples;

a vessel configured to receive the sample holder and a rinsing liquid;

means for filling and emptying the vessel with rinsing liquid;

means for applying ultrasound to the rinsing liquid; and

control means configured to control at least one of:

filling of the vessel with a rinsing liquid by injecting rinsing liquid through an inlet provided in the vessel to submerge the samples in the rinsing liquid,

subjecting the rinsing liquid and the materialographic samples to ultrasound, or

rotating the sample holder including the materialographic samples relative to the vessel.

Assignments (6)
CORRECTIVE ASSIGNMENT TO CORRECT THE PATENT NUMBER PREVIOUSLY RECORDED AT REEL: 61997 FRAME: 614. ASSIGNOR(S) HEREBY CONFIRMS THE SECURITY AGREEMENT. Recorded Nov 13, 2025
From: ALPHA TECHNOLOGIES SERVICES LLC; AMOT CONTROLS LLC; COMPRESSOR CONTROLS LLC; CORNELL PUMP COMPANY LLC; DYNISCO INSTRUMENTS LLC; HANSEN TECHNOLOGIES LLC; METRIX INSTRUMENT CO., L.P.; PETROLEUM ANALYZER COMPANY L.P.; ROPER HOLDINGS, LLC; ROPER INDUSTRIAL PRODUCTS INVESTMENT COMPANY LLC; ROPER PUMP COMPANY LLC; STRUERS LLC; VIA TRAN CORPORATION
To: UBS AG, STAMFORD BRANCH, AS COLLATERAL AGENT
Reel/Frame 073434/0453 →
RELEASE OF SECOND LIEN PATENT SECURITY INTERESTS Recorded May 30, 2025
From: ROYAL BANK OF CANADA
To: AGR INTERNATIONAL, INC.; ALPHA TECHNOLOGIES SERVICES LLC; AMOT CONTROLS LLC; COMPRESSOR CONTROLS LLC; CORNELL PUMP COMPANY LLC; DYNISCO INSTRUMENTS LLC; HANSEN TECHNOLOGIES LLC; METRIX INSTRUMENT CO., L.P.; PETROLEUM ANALYZER COMPANY L.P.; ROPER HOLDINGS, LLC; ROPER INDUSTRIAL PRODUCTS INVESTMENT COMPANY LLC; ROPER PUMP COMPANY LLC; STRUERS LLC; VIATRAN CORPORATION
Reel/Frame 071476/0346 →
SECURITY AGREEMENT (FIRST LIEN) Recorded Nov 28, 2022
From: ALPHA TECHNOLOGIES SERVICES LLC; AMOT CONTROLS LLC; COMPRESSOR CONTROLS LLC; CORNELL PUMP COMPANY LLC; DYNISCO INSTRUMENTS LLC; HANSEN TECHNOLOGIES LLC; METRIX INSTRUMENT CO., L.P.; PETROLEUM ANALYZER COMPANY L.P.; ROPER HOLDINGS, LLC; ROPER INDUSTRIAL PRODUCTS INVESTMENT COMPANY LLC; ROPER PUMP COMPANY LLC; STRUERS LLC; VIATRAN CORPORATION
To: UBS AG, STAMFORD BRANCH, AS COLLATERAL AGENT
Reel/Frame 061997/0614 →
SECURITY AGREEMENT (SECOND LIEN) Recorded Nov 28, 2022
From: ALPHA TECHNOLOGIES SERVICES LLC; AMOT CONTROLS LLC; COMPRESSOR CONTROLS LLC; CORNELL PUMP COMPANY LLC; DYNISCO INSTRUMENTS LLC; HANSEN TECHNOLOGIES LLC; METRIX INSTRUMENT CO., L.P.; PETROLEUM ANALYZER COMPANY L.P.; ROPER HOLDINGS, LLC; ROPER INDUSTRIAL PRODUCTS INVESTMENT COMPANY LLC; ROPER PUMP COMPANY LLC; STRUERS LLC; VIATRAN CORPORATION
To: ROYL BANK OF CANADA, AS COLLATERAL AGENT
Reel/Frame 062003/0566 →
CHANGE OF NAME Recorded May 31, 2022
From: STRUERS, INC.
To: STRUERS, LLC
Reel/Frame 060220/0894 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Feb 24, 2020
From: MATSCHOFSKY, THOMAS; OPPELSTRUP, PALLE
To: STRUERS APS
Reel/Frame 051901/0731 →