IP Library Granted Patent US 11,286,601
Granted Patent B2
US 11,286,601 · App. 16/806,255 · Granted Mar 29, 2022

Processing of chemically modified cellulosic fibres

Inventors: Wayne Lee Bonnefin (Flintshire, GB); Lucy Louisa Ballamy (Flintshire, GB); Sarah Wroe (Flintshire, GB); David Parsons (Flintshire, GB); Garry Storey (Flintshire, GB); Joseph Thompson (Flintshire, GB)
Assignee: CONVATEC TECHNOLOGIES, INC.
D06B1/00A61F13/00012A61F13/00063A61F13/0276A61L15/28A61L15/42B65B55/02D01F2/24D01G15/00D04H1/4258D04H1/46D06M11/38D06M13/21D06M13/278D21H13/02A61F2013/0091A61F2013/00936D06M2101/06
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Quick Facts
Patent No.
US 11,286,601
App. No.
16/806,255
Granted
Mar 29, 2022
Kind
B2
Abstract

A chemically modified cellulosic fibre or filament having a moisture content of at least 7% by weight obtained by a process comprising the steps of (i) obtaining cellulosic fibres or filament and chemically modifying the cellulose by substitution to increase its absorbency; (ii) washing the fibres after step (i) in a mixture comprising water and up to 99% by weight of water-miscible organic solvent; (iii) drying the fibres to a moisture content of at least 7% by weight.

Claims (28)

1. A process for processing a cellulosic fibre or a cellulosic filament, the process comprising:

chemically modifying the cellulose of the cellulosic fibre or the cellulosic filament by substitution to increase absorbency;

washing the chemically modified cellulosic fibre or chemically modified cellulosic filament in a wash solution comprising up to 99% by weight of an organic solvent and at least 95% by weight of the organic solvent; and

adjusting the washed fibre or washed filament to a moisture content of at least 7% by weight.

2. The process of claim 1 , wherein the washed fibre or washed filament is dried to a moisture content from 11% to 18% by weight.

3. The process of claim 1 , wherein the adjusting step comprises drying the washed fibre or washed filament.

4. The process of claim 3 , further comprising carding the dried fibre or dried filament to make a nonwoven web of fibre.

5. The process of claim 4 , further comprising needling the nonwoven web of fibre to form a wound dressing.

6. The process of claim 5 , further comprising sealing the wound dressing in a pouch that maintains the moisture content of the wound dressing in a sterile environment.

7. The process of claim 1 , wherein the adjusting step comprises conditioning the washed fibre or washed filament in an atmosphere having a relative humidity of at least 40%.

8. The process of claim 7 , wherein the relative humidity is from 45% to 85%.

9. The process of claim 7 , further comprising carding the conditioned fibre or filament to produce a non-woven web of chemically modified cellulosic fibre.

10. A process for producing a non-woven web of chemically modified cellulosic fibres, the process comprising:

neutralizing chemically modified cellulosic fibres;

finishing the chemically modified cellulosic fibres with a solution comprising less than 99% by weight of an organic solvent to produce finished chemically modified cellulosic fibres;

adjusting the moisture content of the finished chemically modified cellulosic fibres to a moisture content from 11% to 20% by weight;

processing the finished chemically modified cellulosic fibres into the non-woven web of chemically modified cellulosic fibres, and wherein the moisture content of the non-woven web of chemically modified cellulosic fibres is from 11% to 20% by weight; and

packaging the non-woven web of chemically modified cellulosic fibres in a pouch that maintains the moisture content of the non-woven web of chemically modified cellulosic fibres in a sterile environment, and wherein the packaged non-woven web of chemically modified cellulosic fibres has a tensile strength of at least 3N per cm,

wherein the solution comprises at least 95% by weight of the organic solvent.

11. The process of claim 10 , wherein the solution comprises less than 95% by weight of an organic solvent.

12. The process of claim 10 , wherein the adjusting step comprises drying the finished chemically modified cellulosic fibres to achieve the moisture content from 11% to 20% by weight.

13. The process of claim 10 , wherein the adjusting step comprises conditioning the finished chemically modified cellulosic fibres in air having a relative humidity of at least 40% to achieve the moisture content from 11% to 20% by weight.

14. The process of claim 13 , wherein the relative humidity is from 45% to 85%.

15. The process of claim 10 , wherein the adjusting step comprises drying the finished chemically modified cellulosic fibres in air having a relative humidity of at least 40% to achieve the moisture content from 11% to 20% by weight.

16. A non-woven web of chemically modified cellulosic fibres produced by the process of claim 10 .

17. The non-woven web of chemically modified cellulosic fibres of claim 16 , wherein the non-woven web of chemically modified cellulosic fibres has a tensile strength from 3N/cm to 25N/cm.

18. The non-woven web of chemically modified cellulosic fibres of claim 16 , wherein the non-woven web of chemically modified cellulosic fibres has a basis weight from 80 gsm to 120 gsm.

19. The non-woven web of chemically modified cellulosic fibres of claim 16 , wherein the tensile strength is in a cross-direction.

Assignments (3)
CORRECTIVE ASSIGNMENT TO CORRECT THE APPLICATION NO. 16/816,255 PREVIOUSLY RECORDED ON REEL 064125 FRAME 0565. ASSIGNOR(S) HEREBY CONFIRMS THE ASSIGNMENT. Recorded Jan 11, 2024
From: BONNEFIN, WAYNE LEE; BALLAMY, LUCY LOUISA; WROE, SARAH; PARSONS, DAVID; STOREY, GARRY; THOMPSON, JOSEPH
To: CONVATEC TECHNOLOGIES INC.
Reel/Frame 066275/0019 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Jul 5, 2023
From: BONNEFIN, WAYNE LEE; BALLAMY, LUCY LOUISA; WROE, SARAH; PARSONS, DAVID; STOREY, GARRY; THOMPSON, JOSEPH
To: CONVATEC TECHNOLOGIES INC.
Reel/Frame 064150/0059 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Jun 30, 2023
From: BONNEFIN, WAYNE LEE; BALLAMY, LUCY LOUISA; WROE, SARAH; PARSONS, DAVID; STOREY, GARRY; THOMPSON, JOSEPH
To: CONVATEC TECHNOLOGIES INC.
Reel/Frame 064125/0565 →