ECAE materials for high strength aluminum alloys
A method of forming a high strength aluminum alloy. The method comprises subjecting an aluminum material containing at least one of magnesium, manganese, silicon, copper, and zinc at a concentration of at least 0.1% by weight to an equal channel angular extrusion (ECAE) process. The method produces a high strength aluminum alloy having an average grain size from about 0.2 μm to about 0.8 μm and a yield strength from about 300 MPa to about 650 MPa.
1. A method of forming a high strength aluminum alloy, the method comprising:
heating an aluminum material containing aluminum as a primary component and at least one of magnesium, manganese, silicon, copper, and zinc as a secondary component at a concentration of at least 0.1% by weight to a temperature from about 400° C. to about 550° C. to form a heated aluminum material;
quenching the heated aluminum material to room temperature to form a cooled aluminum material;
aging the cooled aluminum material by heating to form aged aluminum material; and
subjecting the aged aluminum material to an equal channel angular extrusion (ECAE) process while maintaining the aged aluminum material at a temperature from about 0° C. to about 200° C. to form a high strength aluminum alloy, wherein the high strength aluminum alloy has an average grain size from about 0.2 μm to about 0.8 μm in diameter and a yield strength from about 300 MPa to about 650 MPa;
wherein aging the cooled aluminum material by heating includes a first heating step followed by a second heating step, the first heating step at a temperature from about 80° C. to about 100° C. for from about 1 hour to about 50 hours and the second heating step at a temperature from about 100° C. to about 170° C. for from about 20 hours to about 100 hours.
2. The method of claim 1 , wherein aging the cooled aluminum material by heating includes a first heating step followed by a second heating step, the first heating step at a temperature from about 85° C. to about 95° C. for from about 8 hours to about 40 hours and the second heating step a temperature from about 100° C. to about 160° C. for from about 35 hours to about 60 hours.
3. The method of claim 2 , wherein the aged aluminum material is subjected to the ECAE process while maintaining the aged aluminum material at a temperature from about 20° C. to about 125° C.
4. The method of claim 2 , wherein the aged aluminum material is subjected to the ECAE process while maintaining the aged aluminum material at a temperature from about 20° C. to about 35° C.
5. The method of claim 1 , wherein aging the cooled aluminum material by heating includes a first heating step followed by a second heating step, the first heating step at a temperature from about 88° C. to about 92° C. for from about 8 hours to about 20 hours and the second heating step a temperature from about 110° C. to about 160° C. for from about 40 hours to about 45 hours.
6. The method of claim 5 , wherein the aged aluminum material is subjected to the ECAE process while maintaining the aged aluminum material at a temperature from about 20° C. to about 125° C.
7. The method of claim 5 , wherein the aged aluminum material is subjected to the ECAE process while maintaining the aged aluminum material at a temperature from about 20° C. to about 35° C.
8. The method of claim 1 , wherein the aged aluminum material is subjected to the ECAE process while maintaining the aged aluminum material at a temperature from about 20° C. to about 125° C.
9. The method of claim 1 , wherein the aged aluminum material is subjected to the ECAE process while maintaining the aged aluminum material at a temperature from about 20° C. to about 35° C.