IP Library Granted Patent US 11,945,997
Granted Patent B2
US 11,945,997 · App. 16/823,025 · Granted Apr 2, 2024

Composition useful in sulfate scale removal

Inventors: Clay Purdy (Medicine Hat, CA); Markus Weissenberger (Calgary, CA); Stig Magnor Nordaa (Sandnes, NO); Adrienne Lee (Calgary, CA)
Assignee: DORF KETAL CHEMICALS FZE
C09K8/528C02F5/125C02F2101/101C02F2103/08C02F2103/10E21B37/06
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Quick Facts
Patent No.
US 11,945,997
App. No.
16/823,025
Granted
Apr 2, 2024
Kind
B2
Abstract

The present invention discloses a novel aqueous composition for use in removing petroleum-contaminated barium sulfate scale from a surface contaminated with such, said composition comprising: a chelating agent and a counterion component selected from the group consisting of: Li 5 DTPA; Na 5 DTPA; K 5 DTPA; Cs 5 DTPA; Na 4 EDTA; K 4 EDTA; TEAH 4 DTPA; and TBAH 5 DTPA; a scale removal enhancer; and a non-ionic surfactant. There is also disclosed methods to use such compositions.

Claims (19)

1. An aqueous composition for use in removing petroleum-contaminated barium sulfate scale from a surface contaminated with such, said composition consisting of:

a chelating agent having chelating agent components, said chelating agent components including Ethylenediaminetetraacetic acid (EDTA), diethylenetriaminepentaacetic acid (DTPA), Tetraethylammonium hydroxide (TEAR), and Tetrabutylammonium hydroxide (TBAH)

said chelating agent and a counterion component selected from the group consisting of: Na 5 DTPA; K 5 DTPA; Cs 5 DTPA; Na 4 EDTA; K 4 EDTA; TEAH 4 DTPA; and TBAH 5 DTPA;

a scale removal enhancer;

a non-ionic surfactant;

distilled water;

potassium hydroxide; and

wherein the non-ionic surfactant is a linear alcohol ethoxylate surfactant having a chain length of at least 6 carbon atoms and wherein said aqueous composition has a pH ranging from 10 to 11.

2. The aqueous composition according to claim 1 , wherein the scale removal enhancer is selected from the group consisting of: potassium carbonate; potassium formate; cesium formate and cesium carbonate and combinations thereof.

3. The aqueous composition according to claim 1 where the non-ionic surfactant is a linear alcohol ethoxylate surfactant selected from the group consisting of: alcohol ethoxylate surfactants having a chain length of at least 8 carbon atoms.

4. The aqueous composition according to claim 1 where the non-ionic surfactant is an alcohol ethoxylate surfactant selected from the group consisting of: alcohol ethoxylate surfactants having a minimum degree of ethoxylation of 9 or higher.

5. The aqueous composition according to claim 1 where the non-ionic surfactant is an alcohol ethoxylate surfactant selected from the group consisting of: alcohol ethoxylate surfactants having a HLB value of 13 or higher.

6. The aqueous composition according to claim 1 , wherein the scale removal enhancer is present in the composition in an amount ranging from 5 to 20 wt % of the composition.

7. The aqueous composition according to claim 1 , wherein the scale removal enhancer is present in the composition in an amount ranging from 10 to 15 wt % of the composition.

8. The aqueous composition according to claim 1 , wherein the scale removal enhancer is present in the composition in an amount of approximately 10 wt % of the composition.

9. The aqueous composition according to claim 1 , wherein the chelating agent and counterion are present in the composition in an amount ranging from 5 to 40 wt % of the composition.

10. The aqueous composition according to claim 1 , wherein the chelating agent and counterion are present in the composition in an amount ranging from 10 to 30 wt % of the composition.

11. The aqueous composition according to claim 1 , wherein the chelating agent and counterion are present in the composition in an amount ranging from 10 to 20 wt % of the composition.

12. The aqueous composition according to claim 1 , wherein the scale removal enhancer is selected from the group consisting of: K 2 CO 3 ; KOOCH; CsCO 3 ; CsCOOH.

Assignments (4)
SECURITY INTEREST Recorded Dec 12, 2023
From: DORF KETAL CHEMICALS FZE
To: HSBC BANK MIDDLE EAST LIMITED
Reel/Frame 065878/0104 →
CORRECTIVE ASSIGNMENT TO CORRECT THE PRIOR ERRONEOUS RECORDATION OF ASSIGNMENT APPLICATION NUMBERS: 15614284, 17148881 PREVIOUSLY RECORDED ON REEL 063118 FRAME 0689. ASSIGNOR(S) HEREBY CONFIRMS THE ASSIGNMENT. Recorded May 17, 2023
From: FLUID ENERGY GROUP LTD.
To: DORF KETAL CHEMICALS FZE
Reel/Frame 063695/0522 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Mar 20, 2023
From: FLUID ENERGY GROUP LTD.
To: DORF KETAL CHEMICALS FZE
Reel/Frame 063118/0689 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Feb 4, 2022
From: PURDY, CLAY; WEISSENBERGER, MARKUS; NORDAA, STIG; LEE, ADRIENNE
To: FLUID ENERGY GROUP LTD
Reel/Frame 058892/0365 →
Priority Claims (1)
CA CA 3038556 · Apr 1, 2019 · national
Continuity (1)
Related Publication 20200308472A1 · Oct 1, 2020