IP Library Granted Patent US 11,618,238
Granted Patent B2
US 11,618,238 · App. 16/845,887 · Granted Apr 4, 2023

Nonwoven multilayer structures having nanofiber layers

Inventors: Wai-Shing Yung (Pensacola, FL); Albert E. Ortega (Pensacola, FL); Joseph L. Menner (Pinehurst, TX); Vikram Gopal (The Woodlands, TX)
Assignee: Ascend Performance Materials Operations LLC
B32B5/022D04H1/565B32B27/28B32B37/04B32B2307/718B32B2307/732B82Y30/00B82Y40/00
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Quick Facts
Patent No.
US 11,618,238
App. No.
16/845,887
Granted
Apr 4, 2023
Kind
B2
Abstract

Nonwoven multilayer structures having at least two nanofiber layers are described herein. The nonwoven multilayer structure may have two nanofibers layers that have different properties from each other, such as fiber diameter. One nanofiber layer may be produced by an electrospinning process, while another nanofiber layer may be produced by a melt blown process.

Claims (34)

1. A nonwoven multilayer structure comprising:

a first nonwoven layer having melt or solvent electrospun nanofibers, wherein the first nonwoven layer comprises polyamide 66 and has a median pore size from 0.01 microns to 0.414 microns; and

a second nonwoven layer having a first surface and comprising melt blown nanofibers, wherein the second nonwoven layer comprises polyamide 66 and has a median pore size from 1 microns to 5.4 microns, wherein the first layer is adjacent to at least the first surface.

2. The nonwoven multilayer structure of claim 1 , wherein the melt or solvent electrospun nanofibers have an average fiber diameter that is less than or equal to 300 nanometers.

3. The nonwoven multilayer structure of claim 1 , wherein the melt blown nanofibers have an average fiber diameter that is from 250 to 950 nanometers.

4. The nonwoven multilayer structure of claim 1 , wherein the basis weight of the first nonwoven layer is less than second nonwoven layer.

5. The nonwoven multilayer structure of claim 1 , wherein the basis weight of the first nonwoven layer is less than or equal to 25 gsm.

6. The nonwoven multilayer structure of claim 1 , wherein the basis weight of the second nonwoven layer is from 0.9 to 50 gsm.

7. The nonwoven multilayer structure of claim 1 , wherein less than 20% of the electrospun nanofibers have a diameter of greater than 100 nanometers.

8. The nonwoven multilayer structure of claim 1 , wherein no more than 20% of the melt blown nanofibers have a diameter of greater than 700 nanometers.

9. The nonwoven multilayer structure of claim 1 , wherein first nonwoven layer comprises a first polymer and the second nonwoven layer comprises a second polymer.

10. The nonwoven multilayer structure of claim 9 , wherein the second polymer has relative viscosity (RV) from 2 to 330.

11. The nonwoven multilayer structure of claim 1 , wherein the ratio of the median pore size ratio of the first nonwoven layer to the second nonwoven layer is from 1:1 to 1:100.

12. The nonwoven multilayer structure of claim 1 , wherein the second nonwoven layer comprises a second surface, and wherein a scrim layer is adjacent to the second layer.

13. The nonwoven multilayer structure of claim 1 , wherein the second nonwoven layer has an oxidation degradation index (ODI) of less than 200.

14. The nonwoven multilayer structure of claim 1 , wherein the second nonwoven layer has a thermal degradation index (TDI) of less than 4000.

15. A nonwoven multilayer structure comprising:

(a) a first nonwoven layer having first nanofibers having the following first properties (a1) to (a4):

(a1) an average fiber diameter from 1 to 300 nm;

(a2) a basis weight from 0.0001 to 25 gsm;

(a3) a median pore size from 0.01 to 0.414 microns; and

(a4) an average thickness of less than or equal to 30 microns; and

(b) a second nonwoven layer having second nanofibers having the following second properties (b1) to (b7):

(b1) an average fiber diameter from 250 to 950 nm;

(b2) a basis weight from 0.9 to 50 gsm;

(b3) a median pore size from 1 microns to 5.4 microns;

(b4) an average thickness from 5 to 500 microns;

(b5) less than 1 wt. % solvent;

(b6) thermal degradation index of less than 4000; and

(b7) oxidative degradation index of less than 200;

wherein the first property is different from the second property.

16. The nonwoven multilayer structure of claim 15 , wherein the first nonwoven layer comprises a first polymer and the second nonwoven layer comprises a second polymer,

wherein the first polymer comprises polyimide, polyolefin, polyamide, polyester, polystyrene, polyacrylonitrile, polyurethane, polylactic acid, polycaprolactone, polysulfone, fluoropolymer, polyacrylonitrile, polymethyl methacrylate, polystyrene, poly(vinyl chloride), poly(vinyl alcohol), poly(vinyl butylene), poly(vinylidene fluoride), polybutylene terephthalate, cellulose, and copolymers or derivative compounds thereof, and combinations thereof; and

wherein the second polymer polyamide, polyolefin, polyester, polystyrene, polyacrylonitrile, polyurethane, polyimide, polylactic acid, polycaprolactone, polysulfone, fluoropolymer, polyacrylonitrile, polymethyl methacrylate, polystyrene, poly(vinyl chloride), poly(vinyl alcohol), poly(vinyl butylene), poly(vinylidene fluoride), polybutylene terephthalate, cellulose, and copolymers or derivative compounds thereof, and combinations thereof.

Assignments (6)
RELEASE OF SECURITY INTEREST Recorded Dec 23, 2025
From: WILMINGTON SAVINGS FUND SOCIETY, FSB
To: ASCEND PERFORMANCE MATERIALS OPERATIONS LLC
Reel/Frame 074050/0090 →
SECURITY INTEREST Recorded Dec 23, 2025
From: ASCEND PERFORMANCE MATERIALS OPERATIONS LLC
To: WILMINGTON SAVINGS FUND SOCIETY, FSB
Reel/Frame 074056/0183 →
SECURITY INTEREST Recorded Dec 19, 2025
From: ASCEND PERFORMANCE MATERIALS OPERATIONS LLC
To: WELLS FARGO BANK, NATIONAL ASSOCIATION
Reel/Frame 074007/0183 →
SECURITY INTEREST Recorded Apr 10, 2025
From: BANK OF AMERICA, N.A.
To: WILMINGTON SAVINGS FUND SOCIETY, FSB
Reel/Frame 070811/0705 →
SECURITY INTEREST Recorded Dec 8, 2022
From: ASCEND PERFORMANCE MATERIALS OPERATIONS LLC
To: WELLS FARGO CAPITAL FINANCE, LLC
Reel/Frame 062094/0172 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Aug 11, 2020
From: YUNG, WAI-SHING; ORTEGA, ALBERT E.; MENNER, JOSEPH L.; GOPAL, VIKRAM
To: ASCEND PERFORMANCE MATERIALS OPERATIONS LLC
Reel/Frame 053454/0885 →
Continuity (2)
Provisional Application 62833326 · Apr 12, 2019
Related Publication 20200324510A1 · Oct 15, 2020