IP Library Granted Patent US 11,358,130
Granted Patent B2
US 11,358,130 · App. 16/917,424 · Granted Jun 14, 2022

Surface-treated silicoaluminophosphate molecular sieve

Inventor: Ivan Petrovic (Princeton, NJ)
Assignee: BASF Corporation
B01J29/85B01D53/9418B01J21/04B01J35/04B01J35/1019B01J37/0244B01J37/0246B01J37/0248B01J37/10B01J37/30C01B39/54F01N3/20F01N3/2066F01N3/2807B01D2255/2092B01D2255/20707B01D2255/20715B01D2255/20761B01D2255/30B01D2255/50B01D2255/9155B01D2255/9207B01J2229/183F01N2330/02F01N2330/30F01N2370/04F01N2610/02F01N2610/1453
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Quick Facts
Patent No.
US 11,358,130
App. No.
16/917,424
Granted
Jun 14, 2022
Kind
B2
Abstract

A catalyst material for abatement of exhaust gas emissions from a lean burn engine is provided, the catalyst material including a metal-exchanged SAPO-34 material, and an oxide layer at least partially covering an outside surface of the SAPO-34 material, wherein the oxide layer is not substantially blocking the pores of the SAPO-34 material.

Claims (27)

1. A catalyst material for abatement of exhaust gas emissions from a lean burn engine, the catalyst material comprising:

a metal-exchanged SAPO-34 material; and

an oxide layer at least partially covering an outside surface of the SAPO-34 material;

wherein the oxide layer is not blocking at least about 70% of the pores of the SAPO-34 material, and

wherein the oxide layer ranges from approximately 0.1 nm to about 50 nm in thickness.

2. The catalyst material of claim 1 , wherein the oxide layer comprises at least one of Al 2 O 3 , SiO 2 , ZrO 2 , and TiO 2 .

3. The catalyst material of claim 1 , wherein the oxide layer ranges from approximately 0.1 nm to 15 nm in thickness.

4. The catalyst material of claim 1 , wherein the metal is chosen from Cu, Fe, Co, Ce, Mn, and Ni.

5. The catalyst material of claim 1 , wherein the metal is Cu present at a loading ranging from 2% and 8% by weight.

6. A catalytic article comprising the catalyst material of claim 1 , in a washcoat deposited on a honeycomb substrate.

7. The catalytic article of claim 6 , wherein the honeycomb substrate comprises a wall flow filter substrate.

8. The catalytic article of claim 7 , wherein the honeycomb substrate comprises a flow through substrate.

9. An exhaust gas treatment system comprising the catalytic article of claim 6 disposed downstream from a diesel engine and a reductant source that adds a reductant to an exhaust gas stream from the engine.

10. A process for modifying a selective catalytic reduction catalyst material comprising a metal-exchanged SAPO-34 material, the process comprising:

using at least one cycle of a surface deposition method to deposit an oxide layer on at least a portion of an exposed outer surface of the SAPO-34 material, wherein the oxide layer does not substantially block the pores of the SAPO-34 material; and

wherein the modified selective catalytic reduction catalyst material is a catalyst material according to claim 1 .

11. The process of claim 10 , wherein the surface deposition method is chosen from-atomic layer deposition (ALD), chemical vapor deposition (CVD), particle vapor deposition (PVD), ion-beam assisted deposition (IBAD), and combinations thereof.

12. The process of claim 10 , wherein at least 60% of the exposed outer surface of the SAPO-34 material is coated with the oxide layer.

13. The process of claim 10 , wherein the oxide layer comprises one or more of Al 2 O 3 , SiO 2 , ZrO 2 , and TiO 2 .

14. The process of claim 10 , wherein the oxide layer deposited in the at least one cycle ranges from approximately 0.1 nm to about 1 nm in thickness.

15. The process of claim 10 , wherein 5 deposition cycles are used to deposit the oxide layer.

16. The process of claim 10 , wherein 10 deposition cycles are used to deposit the oxide layer.

17. The process of claim 10 , wherein the surface deposition method is run at a process temperature ranging from about 100° C. to about 250° C.

18. The process of claim 10 , wherein the surface deposition method is run at a process temperature ranging from about 120° C. to about 180° C.

19. The process of claim 10 , wherein the surface deposition method is run at a process temperature of about 150° C.

20. The process of claim 10 , wherein the metal is chosen from Cu, Fe, Co, Ce, Mn and Ni.

21. The process of claim 10 , wherein the metal is Cu present at a loading ranging from 2% and 8% by weight of the metal-exchanged SAPO-34 material.

Assignments (2)
NUNC PRO TUNC ASSIGNMENT Recorded Aug 8, 2024
From: BASF CORPORATION
To: BASF MOBILE EMISSIONS CATALYSTS LLC
Reel/Frame 068518/0394 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Apr 27, 2022
From: PETROVIC, IVAN
To: BASF CORPORATION
Reel/Frame 059748/0893 →
Continuity (3)
Continuation PCTIB2019050032 · Jan 2, 2019
Provisional Application 62613220 · Jan 3, 2018
Related Publication 20200330966A1 · Oct 22, 2020