IP Library Granted Patent US 11,584,756
Granted Patent B2
US 11,584,756 · App. 16/918,997 · Granted Feb 21, 2023

Heterocyclic compounds as BET inhibitors

Inventors: Son Minh Pham (San Francisco, CA); Sarvajit Chakravarty (Edmond, OK); Jayakanth Kankanala (Plymouth, MN); Jiyun Chen (Moraga, CA); Chris P. Miller (San Mateo, CA); Jeremy D. Pettigrew (Vancouver, CA); Anjan Kumar Nayak (Uttar Pradesh, IN); Anup Barde (Uttar Pradesh, IN)
Assignee: NUVATION BIO INC.
C07D495/04
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Quick Facts
Patent No.
US 11,584,756
App. No.
16/918,997
Granted
Feb 21, 2023
Kind
B2
Abstract

Novel bromodomain and extraterminal domain (BET) inhibitors and to therapeutic methods of treating conditions and diseases using these novel BET inhibitors are provided.

Claims (99)

1. A compound of Formula (J):

or a tautomer or stereoisomer thereof, or a pharmaceutically acceptable salt of any of the foregoing, wherein:

each is independently a single bond or double bond;

X is O or S;

R 1 is hydrogen, C 1 -C 3 alkyl, —(C 1 -C 3 alkylene)OH, C 1 -C 3 haloalkyl, or C 3 -C 4 cycloalkyl;

G 1 is CR a , wherein:

R a is hydrogen, halogen, or C 1 -C 4 alkyl;

Z 1 is C—W 1 —R c ; wherein:

each W 1 is independently —O— or —NR w1 —, wherein:

R w1 is hydrogen, C 3 -C 6 cycloalkyl, or C 1 -C 4 alkyl optionally substituted by oxo, —OH, or halogen, and

R c is independently C 3 -C 6 cycloalkyl, 4- to 6-membered heterocyclyl, C 6 -C 14 aryl, or 5- or 6-membered heteroaryl, each of which is independently optionally substituted by R c1 , wherein each R c1 is independently halogen, C 1 -C 4 alkyl, C 3 -C 6 cycloalkyl, 3- to 6-membered heterocyclyl, cyano, oxo, C 1 -C 4 alkoxy, C 1 -C 4 haloalkoxy, C 1 -C 4 haloalkyl, —OR 10 , —NR 10 R 11 , —C(O)NR 10 R 11 ,

—NR 10 C(O)R 11 , —S(O) 2 R 10 , —NR 10 S(O) 2 R 11 , or —S(O) 2 NR 10 R 11 ;

Z 2 is C—W 2 —R d , wherein:

W 2 is —O—, —NR w2 —, or a bond, wherein:

R w2 is hydrogen, C 3 -C 6 cycloalkyl, or C 1 -C 4 alkyl optionally substituted by oxo, —OH, or halogen, and

R d is independently hydrogen, halogen, cyano, 3- to 6-membered heterocyclyl, or C 1 -C 4 alkyl;

Z 3 is C—R e , wherein:

R e is independently hydrogen, halogen, cyano, 3- to 6-membered heterocyclyl, or C 1 -C 4 alkyl;

M 1 is S or CR 1a ;

M 2 is S or CR 2a , provided that

(1) when M 1 is S, then the adjacent to M 1 is a single bond and the adjacent to M2 is a double bond,

(2) when M 2 is S, then the adjacent to M 2 is a single bond and the adjacent to M 1 is a double bond, and

(3) either M 1 or M 2 is S;

R 1a and R 2a are each independently hydrogen, halogen, C 1 -C 4 alkyl, C 3 -C 6 cycloalkyl, 3- to 6-membered heterocyclyl, 5- to 10-membered heteroaryl, cyano, oxo, C 1 -C 4 haloalkyl, C 1 -C 4 alkoxy, C 1 -C 4 haloalkoxy, —OR 10 , —NR 10 R 11 , —C(O)OR 10 , —C(O)NR 10 R 11 , —NR 10 C(O)R 11 , —S(O) 2 R 10 ,

—NR 10 S(O) 2 R 11 or —S(O) 2 NR 10 R 11 , each of which is independently optionally substituted by R 12 ;

R 2 is hydrogen, halogen, C 1 -C 4 alkyl, C 3 -C 6 cycloalkyl, 3- to 6-membered heterocyclyl, —(C 1 -C 3 alkylene)3- to 6-membered heterocyclyl, 5- to 10-membered heteroaryl, cyano, oxo, C 1 -C 4 haloalkyl, C 1 -C 4 alkoxy, C 1 -C 4 haloalkoxy, —OR 10 , —NR 10 R 11 , —C(O)OR 10 , —C(O)NR 10 R 11 ,

—NR 10 C(O)R 11 , —S(O) 2 R 10 , —NR 10 S(O) 2 R 11 , or —S(O) 2 NR 10 R 11 , each of which is independently optionally substituted by R 12 ;

R 3 is —(CH 2 ) m NR 13 S(O) 2 R 14 wherein m is 0, 1, 2 or 3; C 3 -C 6 cycloalkyl optionally substituted by halogen, oxo, —CN, or —OH; C 1 -C 4 alkyl substituted by halogen, oxo, —CN, or —OH; or C 2 -C 6 alkenyl;

R 10 and R 11 are each independently hydrogen, C 1 -C 4 alkyl, C 1 -C 4 alkoxy, C 1 -C 4 alkenyl, C 3 -C 6 cycloalkyl, C 6 -C 14 aryl, 3- to 6-membered heterocyclyl, —(C 1 -C 3 alkylene)C 3 -C 6 cycloalkyl, —(C 1 -C 3 alkylene) 3- to 6-membered heterocyclyl, —(C 1 -C 3 alkylene) C 6 -C 14 aryl, —NR 15 R 16 , or —C(O)R 12 , wherein each of R 10 and R 11 is independently optionally substituted by halogen, oxo, —CN, —CF 3 ,

—OH, —NR 13 R 14 , —C(O)NR 13 R 14 , or C 1 -C 4 alkyl optionally substituted by halogen, oxo, —CN, —CF 3 , or —OH,

or R 10 and R 11 are taken together with the atom or atoms to which they are attached to form a 3- to 6-membered heterocyclyl ring optionally substituted by halogen, oxo, —CN, —CF 3 , —OH, or C 1 -C 4 alkyl optionally substituted by halogen, oxo, —CN, or —OH;

each R 12 is independently halogen, cyano, C 1 -C 4 haloalkyl, C 1 -C 4 alkoxy, C 1 -C 4 haloalkoxy, —OR 15 , —NR 15 R 16 , —C(O)NR 15 R 16 , —NR 15 C(O)R 16 , —S(O) 2 R 15 , —NR 15 S(O) 2 R 16 , —S(O) 2 NR 15 R 16 , C 3 -C 6 cycloalkyl, 3- to 6-membered heterocyclyl, or C 1 -C 4 alkyl, each of which is independently optionally substituted by halogen, oxo, —CF 3 , —CN, —OH, —NR 13 R 14 , or —NR 13 C(O)R 14 ;

R 13 and R 14 are independently hydrogen, C 1 -C 4 alkyl C 3 -C 6 cycloalkyl, or 3- to 6-membered heterocyclyl, each of which is independently optionally substituted by halogen, oxo, —CN, or —OH,

or R 13 and R 14 are taken together with the atom or atoms to which they are attached to form a 3- to 6-membered heterocyclyl ring optionally substituted by halogen, oxo, —CN, —OH, or C 1 -C 4 alkyl optionally substituted by halogen, oxo, —CN, or —OH; and

each R 15 and R 16 are independently hydrogen, C 1 -C 4 alkyl, C 3 -C 6 cycloalkyl, or 3- to 6-membered heterocyclyl, each of which is independently optionally substituted by halogen, oxo, —CN, or —OH,

or R 15 and R 16 are taken together with the atoms to which they are attached to form a 3- to 6-membered heterocyclyl ring optionally substituted by halogen, oxo, —CN, —OH, or C 1 -C 4 alkyl optionally substituted by halogen, oxo, —CN, or —OH.

2. The compound of claim 1 , wherein the compound is a compound of Formula (I):

or a tautomer or stereoisomer thereof, or a pharmaceutically acceptable salt of any of the foregoing, wherein:

each is independently a single bond or double bond;

X is O or S;

R 1 is hydrogen, C 1 -C 3 alkyl, —(C 1 -C 3 alkylene)OH, C 1 -C 3 haloalkyl, or C 3 -C 4 cycloalkyl;

G 1 is CR a , wherein:

R a is hydrogen, halogen, or C 1 -C 4 alkyl;

Z 1 is C—W 1 —R c ; wherein:

each W 1 is independently —O— or —NR w1 —, wherein:

R w1 is hydrogen, C 3 -C 6 cycloalkyl, or C 1 -C 4 alkyl optionally substituted by oxo, —OH, or halogen, and

R c is independently 4- to 6-membered heterocyclyl, C 6 -C 14 aryl, or 5- or 6-membered heteroaryl, each of which is independently optionally substituted by R c1 , wherein each R c1 is independently halogen, C 1 -C 4 alkyl, C 3 -C 6 cycloalkyl, 3- to 6-membered heterocyclyl, cyano, oxo, C 1 -C 4 alkoxy, C 1 -C 4 haloalkoxy, C 1 -C 4 haloalkyl, —OR 10 , —NR 10 R 11 , —C(O)NR 10 R 11 , —NR 10 C(O)R 11 , —S(O) 2 R 10 , —NR 10 S(O) 2 R 11 , or —S(O) 2 NR 10 R 11 ;

Z 2 is C—W 2 —R d , wherein:

W 2 is —O—, —NR w2 —, or a bond, wherein:

R w2 is hydrogen, C 3 -C 6 cycloalkyl, or C 1 -C 4 alkyl optionally substituted by oxo, —OH, or halogen, and

R d is independently hydrogen, halogen, cyano, 3- to 6-membered heterocyclyl, or C 1 -C 4 alkyl;

Z 3 is C—R e , wherein:

R e is independently hydrogen, halogen, cyano, 3- to 6-membered heterocyclyl, or C 1 -C 4 alkyl;

M 1 is S or CR 1a ;

M 2 is S or CR 2a , provided that

(1) when M 1 is S, then the adjacent to M 1 is a single bond and the adjacent to M 2 is a double bond,

(2) when M 2 is S, then the adjacent to M 2 is a single bond and the adjacent to M 1 is a double bond, and

(3) at least one of M 1 and M 2 is not S;

R 1a and R 2a are each independently hydrogen, halogen, C 1 -C 4 alkyl, C 3 -C 6 cycloalkyl, 3- to 6-membered heterocyclyl, 5- to 10-membered heteroaryl, cyano, oxo, C 1 -C 4 haloalkyl, C 1 -C 4 alkoxy, C 1 -C 4 haloalkoxy, —OR 10 , —NR 10 R 11 , —C(O)OR 10 , —C(O)NR 10 R 11 , —NR 10 C(O)R 11 , —S(O) 2 R 10 ,

—NR 10 S(O) 2 R 11 or —S(O) 2 NR 10 R 11 , each of which is independently optionally substituted by R 12 ;

R 2 is halogen, C 1 -C 4 alkyl, C 3 -C 6 cycloalkyl, 3- to 6-membered heterocyclyl, —(C 1 -C 3 alkylene)3- to 6-membered heterocyclyl, 5- to 10-membered heteroaryl, cyano, oxo, C 1 -C 4 haloalkyl, C 1 -C 4 alkoxy, C 1 -C 4 haloalkoxy, —OR 10 , —NR 10 R 11 , —C(O)OR 10 , —C(O)NR 10 R 11 , —NR 10 C(O)R 11 , —S(O) 2 R 10 , —NR 10 S(O) 2 R 11 , or —S(O) 2 NR 10 R 11 , each of which is independently optionally substituted by R 12 ;

R 3 is —(CH 2 ) m NR 13 S(O) 2 R 14 , C 3 -C 6 cycloalkyl, or C 1 -C 4 alkyl substituted by halogen, oxo, —CN, or —OH, wherein m is 0, 1, 2 or 3;

R 10 and R 11 are each independently hydrogen, C 1 -C 4 alkyl, C 1 -C 4 alkoxy, C 1 -C 4 alkenyl, C 3 -C 6 cycloalkyl, 3- to 6-membered heterocyclyl, —(C 1 -C 3 alkylene)C 3 -C 6 cycloalkyl, —(C 1 -C 3 alkylene) 3- to 6-membered heterocyclyl, —NR 15 R 16 , or —C(O)R 12 , wherein each of R 10 and R 11 is independently optionally substituted by halogen, oxo, —CN, —CF 3 , —OH, —NR 13 R 14 , —C(O)NR 13 R 14 , or C 1 -C 4 alkyl optionally substituted by halogen, oxo, —CN, —CF 3 , or —OH,

or R 10 and R 11 are taken together with the atom or atoms to which they are attached to form a 3- to 6-membered heterocyclyl ring optionally substituted by halogen, oxo, —CN, —CF 3 , —OH, or C 1 -C 4 alkyl optionally substituted by halogen, oxo, —CN, or —OH;

each R 12 is independently halogen, cyano, C 1 -C 4 haloalkyl, C 1 -C 4 alkoxy, C 1 -C 4 haloalkoxy, —OR 15 , —NR 15 R 16 , —C(O)NR 15 R 16 , —NR 15 C(O)R 16 , —S(O) 2 R 15 , —NR 15 S(O) 2 R 16 , —S(O) 2 NR 15 R 16 , C 3 -C 6 cycloalkyl, 3- to 6-membered heterocyclyl, or C 1 -C 4 alkyl, each of which is independently optionally substituted by halogen, oxo, —CF 3 , —CN, —OH, —NR 13 R 14 , or —NR 13 C(O)R 14 ;

R 13 and R 14 are independently hydrogen, C 1 -C 4 alkyl C 3 -C 6 cycloalkyl, or 3- to 6-membered heterocyclyl, each of which is independently optionally substituted by halogen, oxo, —CN, or —OH,

or R 13 and R 14 are taken together with the atom or atoms to which they are attached to form a 3- to 6-membered heterocyclyl ring optionally substituted by halogen, oxo, —CN, —OH, or C 1 -C 4 alkyl optionally substituted by halogen, oxo, —CN, or —OH; and

each R 15 and R 16 are independently hydrogen, C 1 -C 4 alkyl, C 3 -C 6 cycloalkyl, or 3- to 6-membered heterocyclyl, each of which is independently optionally substituted by halogen, oxo, —CN, or —OH,

or R 15 and R 16 are taken together with the atoms to which they are attached to form a 3- to 6-membered heterocyclyl ring optionally substituted by halogen, oxo, —CN, —OH, or C 1 -C 4 alkyl optionally substituted by halogen, oxo, —CN, or —OH.

3. The compound of claim 1 , or a tautomer or stereoisomer thereof, or a pharmaceutically acceptable salt of any of the foregoing, wherein the compound is of Formula (II),

4. The compound of claim 1 , or a tautomer or stereoisomer thereof, or a pharmaceutically acceptable salt of any of the foregoing, wherein the compound is of Formula (III),

5. The compound of claim 1 , or a tautomer or stereoisomer thereof, or a pharmaceutically acceptable salt of any of the foregoing, wherein X is O.

6. The compound of claim 1 , or a tautomer or stereoisomer thereof, or a pharmaceutically acceptable salt of any of the foregoing, wherein G 1 is CH.

7. The compound of claim 1 , or a tautomer or stereoisomer thereof, or a pharmaceutically acceptable salt of any of the foregoing, wherein Z 1 is C—W 1 —R c and R c is C 6 -C 14 aryl optionally substituted by R c1 .

8. The compound of claim 7 , or a tautomer or stereoisomer thereof, or a pharmaceutically acceptable salt of any of the foregoing, wherein R′ is phenyl optionally substituted by halogen or C 1 -C 4 alkyl.

9. The compound of claim 1 , or a tautomer or stereoisomer thereof, or a pharmaceutically acceptable salt of any of the foregoing, wherein Z 2 is CH.

10. The compound of claim 1 , or a tautomer or stereoisomer thereof, or a pharmaceutically acceptable salt of any of the foregoing, wherein Z 3 is CH.

11. The compound of claim 1 , or a tautomer or stereoisomer thereof, or a pharmaceutically acceptable salt of any of the foregoing, wherein R 1 is C 1 -C 3 alkyl.

12. The compound of claim 1 , or a tautomer or stereoisomer thereof, or a pharmaceutically acceptable salt of any of the foregoing, wherein R 2 is —C(O)NR 10 R 11 , 5- to 10-membered heteroaryl, —(C 1 -C 3 alkylene)3- to 6-membered heterocyclyl, or C 1 -C 4 alkyl, each of which is independently optionally substituted by R 12 .

13. The compound of claim 12 , or a tautomer or stereoisomer thereof, or a pharmaceutically acceptable salt of any of the foregoing, wherein R 2 is —C(O)NR 10 R 11 which is optionally substituted by R 12 , wherein R 10 and R 11 are each independently hydrogen, C 1 -C 4 alkyl, or C 3 -C 6 cycloalkyl, or R 10 and R 11 are taken together with the atom or atoms to which they are attached to form a 3- to 6-membered heterocyclyl ring optionally substituted by halogen.

14. The compound of claim 12 , or a tautomer or stereoisomer thereof, or a pharmaceutically acceptable salt of any of the foregoing, wherein R 2 is 5- to 10-membered heteroaryl optionally substituted by R 12 .

15. The compound of claim 1 , or a tautomer or stereoisomer thereof, or a pharmaceutically acceptable salt of any of the foregoing, wherein R 3 is —(CH 2 ) m NR 13 S(O) 2 R 14 or C 1 -C 4 alkyl substituted by halogen, oxo, —CN, or —OH.

16. The compound of claim 1 , or a tautomer or stereoisomer thereof, or a pharmaceutically acceptable salt of any of the foregoing, wherein R 3 is —(CH 2 ) m NR 13 S(O) 2 R 14 .

17. The compound of claim 1 , or a tautomer or stereoisomer thereof, or a pharmaceutically acceptable salt of any of the foregoing, wherein R 3 is

18. The compound of claim 1 , or a tautomer or stereoisomer thereof, or a pharmaceutically acceptable salt of any of the foregoing, wherein R 3 is C 1 -C 4 alkyl substituted by —OH.

19. The compound of claim 18 , or a tautomer or stereoisomer thereof, or a pharmaceutically acceptable salt of any of the foregoing, wherein R 3 is

20. The compound of claim 1 , or a tautomer or stereoisomer thereof, or a pharmaceutically acceptable salt of any of the foregoing, wherein R 1a is hydrogen.

21. The compound of claim 1 , or a tautomer or stereoisomer thereof, or a pharmaceutically acceptable salt of any of the foregoing, wherein R 2a is hydrogen.

22. The compound of claim 1 , wherein the compound is selected from the group consisting of:

or a pharmaceutically acceptable salt of any of the foregoing.

23. A pharmaceutical composition comprising the compound of claim 1 , or a tautomer or stereoisomer thereof, or a pharmaceutically acceptable salt of any of the foregoing, and a pharmaceutically acceptable carrier.

24. A kit comprising the compound of claim 1 , or a tautomer or stereoisomer thereof, or a pharmaceutically acceptable salt of any of the foregoing.

25. The compound of claim 22 , or a pharmaceutically acceptable salt thereof, wherein the compound is

26. The compound of claim 22 , or a pharmaceutically acceptable salt thereof, wherein the compound is

27. The compound of claim 22 , or a pharmaceutically acceptable salt thereof, wherein the compound is

28. The compound of claim 22 , or a pharmaceutically acceptable salt thereof, wherein the compound is

29. The compound of claim 22 , or a pharmaceutically acceptable salt thereof, wherein the compound is

30. The compound of claim 22 , or a pharmaceutically acceptable salt thereof, wherein the compound is

31. The compound of claim 22 , or a pharmaceutically acceptable salt thereof, wherein the compound is

Assignments (10)
RELEASE OF SECURITY INTEREST Recorded Jul 6, 2026
From: SAGARD HOLDINGS MANAGER LP, AS ADMINISTRATIVE AGENT
To: NUVATION BIO INC.
Reel/Frame 075179/0564 →
SECURITY INTEREST Recorded Mar 4, 2025
From: NUVATION BIO INC.
To: SAGARD HOLDINGS MANAGER LP, AS ADMINISTRATIVE AGENT
Reel/Frame 070400/0200 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded May 3, 2022
From: SPARCBIO LLC
To: GIRAFPHARMA LLC
Reel/Frame 059798/0172 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded May 3, 2022
From: GIRAFPHARMA LLC
To: NUVATION BIO OPERATING COMPANY INC.
Reel/Frame 059798/0175 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded May 3, 2022
From: NUVATION BIO OPERATING COMPANY LLC
To: NUVATION BIO INC.
Reel/Frame 059798/0204 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded May 3, 2022
From: PHAM, SON MINH; CHAKRAVARTY, SARVAJIT; KANKANALA, JAYAKANTH; CHEN, JIYUN; PETTIGREW, JEREMY D.
To: SPARCBIO LLC
Reel/Frame 059798/0090 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded May 3, 2022
From: INTEGRAL BIOSCIENCES PVT. LTD.
To: SPARCBIO LLC
Reel/Frame 059848/0491 →
CHANGE OF NAME Recorded May 3, 2022
From: NUVATION BIO OPERATING COMPANY INC.
To: NUVATION BIO OPERATING COMPANY LLC
Reel/Frame 059848/0494 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded May 3, 2022
From: NAYAK, ANJAN KUMAR; BARDE, ANUP
To: INTEGRAL BIOSCIENCES PVT. LTD.
Reel/Frame 059848/0432 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded May 3, 2022
From: MILLER, CHRIS P.
To: NUVATION BIO OPERATING COMPANY INC.
Reel/Frame 059798/0107 →
Continuity (3)
Provisional Application 62870020 · Jul 2, 2019
Provisional Application 63017547 · Apr 29, 2020
Related Publication 20210002293A1 · Jan 7, 2021