IP Library Granted Patent US 11,591,553
Granted Patent B2
US 11,591,553 · App. 16/936,956 · Granted Feb 28, 2023

Method for producing a washing agent portion unit with improved optical and rheological properties

Inventors: Frank Meier (Duesseldorf, DE); Peter Schmiedel (Duesseldorf, DE); Daniel Thomas Piorkowski (Fairfield, CT)
Assignee: Henkel AG & Co. KGaA
C11D17/043C11D1/83C11D3/046C11D3/2075C11D3/43C11D11/0017C11D1/72
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Quick Facts
Patent No.
US 11,591,553
App. No.
16/936,956
Granted
Feb 28, 2023
Kind
B2
Abstract

A method for producing a washing agent portion unit having at least one receiving chamber surrounded by a water-soluble film, including the steps of: a) transporting a first water-soluble film in the direction of a dosing station; b) molding the first water-soluble film into the cavities of a deep-drawing die located below the water-soluble film, forming at least one cavity in the direction of travel of the film; c) filling the cavity by way of the dosing station with a first flowable washing agent preparation containing, based on its total weight, i) 20 to 80 wt. % surfactant; ii) 2 to 15 wt. % fatty acid; iii) 0.3 to 8 wt. % of the salt of a divalent cation; iv) 8 to 35 wt. % solvent; d) transporting the filled cavity in the direction of a sealing station; e) sealing the filled cavity with a second water-soluble film, and the washing agent portion.

Claims (46)

1. A method for producing an opacified washing agent portion unit having at least one filled receiving chamber surrounded by a water-soluble film, comprising the steps of:

a) transporting a first water-soluble film in the direction of a dosing station at a speed above 0.04 m/s;

b) molding the first water-soluble film into cavities of a deep-drawing die located below the water-soluble film, so as to form at least one cavity having a maximum diameter in the direction of travel of the film of between 3 and 75 mm;

c) filling the cavity by means of the dosing station with a first flowable washing agent preparation containing, based on its total weight,

i) 20 to 80 wt. % surfactant consisting of anionic surfactant and non-ionic surfactant;

ii) 2 to 15 wt. % fatty acid;

iii) 0.4 to 6 wt. % of a salt of a divalent cation;

iv) 8 to 35 wt. % solvent;

v) 0.5 to 4 wt. % of a salt of a monovalent metal cation; and

vi) 0.3 to 5 wt. % of a co-surfactant that differs from the non-ionic surfactant and is selected from the group consisting of, aliphatic C 6 -C 14 alcohols, aromatic C 6 -C 14 alcohols, aliphatic C 6 -C 12 dialcohols, monoglycerides of C 12 -C 18 fatty acids, and monoglycerol ethers of C 8 -C 18 fatty alcohols;

d) further transporting the filled cavity in the direction of a sealing station at a speed above 0.04 m/s;

e) sealing the filled cavity with a second water-soluble film;

wherein the first flowable washing agent preparation has a turbidity above 60 NTU and is free from enzymes.

2. The method according to claim 1 , wherein the water-soluble film is continuously transported from step a) to step e).

3. The method according to claim 1 , wherein the first water-soluble film is transported at a speed from 0.08 to 0.3 m/s in step a).

4. The method according to claim 3 , wherein the first water-soluble film is transported at a speed from 0.1 to 0.2 m/s.

5. The method according to claim 1 , wherein the cavity formed in step b) has a maximum diameter in the direction of travel of the film between 3 and 40 mm.

6. The method according to claim 5 , wherein the cavity has a maximum diameter in the direction of travel of the film between 3 and 20 mm.

7. The method according to claim 5 , wherein the cavity has a maximum diameter in the direction of travel of the film between 3 and 15 mm.

8. The method according to claim 1 , wherein the first flowable washing agent preparation contains, based on its total weight,

i) 20 to 80 wt. % surfactant, wherein the anionic surfactant is present in an amount from 20 to 50 wt. %;

ii) 4 to 12 wt. % of the fatty acid;

iii) 0.5 to 4 wt. % of the salt of a divalent metal cation.

9. The method according to claim 1 , wherein the first flowable washing agent preparation contains, based on its total weight,

i) 32.3 to 80 wt. % of the surfactant, wherein the anionic surfactant is present in an amount from 20 to 50 wt. % and the nonionic surfactant is present in an amount from 12 to 30 wt. %;

ii) 4 to 12 wt. % of the fatty acid;

iii) 0.5 to 4 wt. % of the salt of a divalent cation.

10. The method according to claim 1 , wherein the first water-soluble film is transported at a speed from 0.08 to 0.3 m/s in step d).

11. The method according to claim 10 , wherein the first water-soluble film is transported at a speed from 0.1 to 0.2 m/s.

12. The method according to claim 1 , wherein the washing agent portion unit has at least two receiving chambers which enclose one another at least in part.

13. The method according to claim 1 , wherein the first water-soluble film is transported in the direction of a dosing station at a speed of 0.08 m/s.

14. The method according to claim 1 , wherein the filled cavity is further transported in the direction of a sealing station at a speed of 0.08 m/s.

15. A method for producing a washing agent portion unit having at least one filled receiving chamber surrounded by a water-soluble film, comprising the steps of:

a) transporting a first water-soluble film in the direction of a dosing station at a speed above 0.04 m/s;

b) molding the first water-soluble film into cavities of a deep-drawing die located below the water-soluble film, so as to form at least one cavity having a maximum diameter in the direction of travel of the film of between 3 and 75 mm;

c) filling the cavity by means of the dosing station with a first opacified flowable washing agent preparation free of amphoteric surfactant and containing, based on its total weight,

i) 20 to 80 wt. % surfactant containing anionic surfactant and non-ionic surfactant,

ii) 2 to 15 wt. % fatty acid;

iii) 0.5 to 4 wt. % of the salt of a divalent cation;

iv) 8 to 35 wt. % solvent;

v) 0.5 to 4 wt. % of a salt of a monovalent metal cation; and

vi) 0.3 to 5 wt. % of a co-surfactant that differs from the non-ionic surfactant and is selected from the group consisting of aliphatic C 6 -C 14 alcohols, aromatic C 6 -C 14 alcohols, aliphatic C 6 -C 12 dialcohols, monoglycerides of C 12 -C 18 fatty acids, and monoglycerol ethers of C 8 -C 18 fatty alcohols;

d) further transporting the filled cavity in the direction of a sealing station at a speed above 0.04 m/s; and

e) sealing the filled cavity with a second water-soluble film.

16. The method according to claim 15 , wherein the water-soluble film is continuously transported from step a) to step e).

17. The method according to claim 15 , wherein the first water-soluble film is transported at a speed from 0.08 to 0.3 m/s in steps a) and d).

Assignments (3)
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Feb 22, 2022
From: HENKEL IP & HOLDING GMBH
To: HENKEL AG & CO. KGAA
Reel/Frame 059207/0627 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded May 28, 2021
From: MEIER, FRANK; SCHMIEDEL, PETER
To: HENKEL AG & CO. KGAA
Reel/Frame 056382/0642 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded May 28, 2021
From: PIORKOWSKI, DANIEL THOMAS
To: HENKEL IP & HOLDING GMBH
Reel/Frame 056382/0675 →