IP Library Granted Patent US 11,499,083
Granted Patent B2
US 11,499,083 · App. 16/949,283 · Granted Nov 15, 2022

Method for plugging and abandoning oil and gas wells

Inventors: Eric van Oort (Bee Cave, TX); Michael McDonald (Toronto, CA)
Assignees: Board of Regents, The University of Texas System; PQ LLC
C09K8/426C09K8/46E21B33/14
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Quick Facts
Patent No.
US 11,499,083
App. No.
16/949,283
Granted
Nov 15, 2022
Kind
B2
Abstract

A method and agent to induce accelerated creep deformation of shale rock formations in the annular gap between a shale formation and non-cemented sections of a casing string have been developed. A fluid containing alkali silicate or a modified alkali silicate is added to the annular space between the shale rock formation and the casing string. The alkali silicate promotes creep deformation of the shale rock, effectively closing the annulus surrounding the casing. It has been found lithium silicate provides the strongest shale-casing bond and is the presently preferred material for closing abandoned wells.

Claims (6)

1. A method for promoting creep deformation of shale surrounding a well casing comprising the step of introducing a lithium-based product in aqueous form into an annulus between said shale and said well casing, wherein said lithium-based product is one of lithium hydroxide, lithium carbonate, or lithium chloride, whereby said lithium-based product directly contacts the shale to promote the creep deformation of the shale, thereby sealing the annulus and creating an effective seal between the shale and the well casing.

2. The method of claim 1 wherein said lithium-based product is introduced in aqueous form.

3. The method of claim 1 wherein said lithium-based product further comprises lithium silicate.

4. The method of claim 1 wherein said creep deformation of the shale fully closes said annulus.

5. The method of claim 1 wherein said lithium-based product is added to sodium silicate.

6. The method of claim 5 wherein said lithium-based product further comprises a modified lithium silicate.

Assignments (6)
CHANGE OF NAME Recorded Dec 2, 2021
From: PQ CORPORATION
To: PQ LLC
Reel/Frame 058295/0836 →
PARTIAL RELEASE OF SECURITY INTEREST IN PATENTS RECORDED AT R/F 056539/0903 Recorded Aug 5, 2021
From: CREDIT SUISSE AG, CAYMAN ISLANDS BRANCH, AS ADMINISTRATIVE AGENT
To: PQ CORPORATION
Reel/Frame 057089/0255 →
SECURITY INTEREST Recorded Aug 3, 2021
From: PQ LLC
To: GOLDMAN SACHS BANK USA, AS COLLATERAL AGENT
Reel/Frame 057060/0874 →
TERM LOAN PATENT SECURITY AGREEMENT Recorded Jun 10, 2021
From: PQ CORPORATION
To: CREDIT SUISSE AG, CAYMAN ISLANDS BRANCH, AS AGENT
Reel/Frame 056539/0903 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded May 7, 2021
From: VAN OORT, ERIC
To: BOARD OF REGENTS, THE UNIVERSITY OF TEXAS SYSTEM
Reel/Frame 056167/0936 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded May 7, 2021
From: MCDONALD, MICHAEL J.
To: PQ CORPORATION
Reel/Frame 056168/0326 →