IP Library Granted Patent US 11,439,981
Granted Patent B2
US 11,439,981 · App. 16/958,428 · Granted Sep 13, 2022

Catalyst for hydrolysis of carbonyl sulfide and method of producing same

Inventors: Katsumi Nochi (Tokyo, JP); Masanao Yonemura (Tokyo, JP); Toshinobu Yasutake (Tokyo, JP); Kaori Yoshida (Tokyo, JP)
Assignee: Mitsubishi Heavy Industries Engineering, Ltd.
B01J21/063B01J23/04B01J27/02B01J37/0018B01J37/08C10K1/004C10K1/34
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Quick Facts
Patent No.
US 11,439,981
App. No.
16/958,428
Granted
Sep 13, 2022
Kind
B2
Abstract

A catalyst for COS hydrolysis includes titanium dioxide and a barium compound supported on the titanium dioxide. The catalyst, when expressing Ba and S in the catalyst in terms of BaO and SO 3 , respectively, has a molar ratio of SO 3 to BaO of at least 1. The catalyst converts COS and H 2 O in a raw material gas to CO 2 and H 2 S.

Claims (14)

1. A catalyst for COS hydrolysis comprising:

a titanium dioxide carrier;

a barium compound supported on the titanium dioxide carrier; and

sulfate ions supported on the titanium dioxide carrier;

wherein, a Ba content and a S content in the catalyst are expressed in terms of BaO and SO 3 , respectively, and a molar ratio of SO 3 to BaO in compounds supported on the titanium dioxide carrier of the catalyst is at least 2.1, and

wherein the catalyst converts COS and H 2 O in a raw material gas to CO 2 and H 2 S.

2. The catalyst for COS hydrolysis according to claim 1 , wherein the barium compound is supported on the titanium dioxide carrier in an amount of 2% by mass or greater and 8% by mass or less in terms of the barium oxide with respect to the catalyst.

3. A method of producing a catalyst for converting COS and H 2 O in a raw material gas to CO 2 and H 2 S by COS hydrolysis, comprising:

adding a barium acetate solution to titanium dioxide containing a sulfate ion and performing kneading to obtain a kneaded product;

extruding the kneaded product to obtain a molded catalyst;

drying the molded catalyst; and

calcining subsequent to the drying to obtain a catalyst of a titanium dioxide carrier supporting a barium compound and a sulfate ion,

wherein, a Ba content and a S content in the catalyst are expressed in terms of BaO and SO 3 , respectively, and a molar ratio of SO 3 to BaO in compounds supported on the titanium dioxide carrier of the catalyst is at least 2.1.

4. The method according to claim 3 , wherein in the kneading to obtain the kneaded product, the barium acetate solution is added in an amount of 2% by mass or more and 8% by mass or less in terms of the barium oxide with respect to the catalyst.

Assignments (3)
CHANGE OF NAME Recorded Dec 14, 2023
From: MITSUBISHI HEAVY INDUSTRIES ENGINEERING, LTD.
To: MHI ENGINEERING, LTD.
Reel/Frame 066014/0774 →
NUNC PRO TUNC ASSIGNMENT Recorded Dec 14, 2023
From: MHI ENGINEERING, LTD.
To: MITSUBISHI HEAVY INDUSTRIES, LTD.
Reel/Frame 066014/0870 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Jul 31, 2020
From: NOCHI, KATSUMI; YONEMURA, MASANAO; YASUTAKE, TOSHINOBU; YOSHIDA, KAORI
To: MITSUBISHI HEAVY INDUSTRIES ENGINEERING, LTD.
Reel/Frame 053366/0955 →